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91 RSR011 SEVERN TRENT LABORATORIES, INC. Run Date: 9/22/06 SAMPLE CONFIRMATION REPORT Page : 1 Time : 8:06: The following samples have been received by Severn Trent Laboratories, Inc. at West Sacramento, California. Please verify that the sample ID's and the requested tests are correct. Contact the STL project manager listed below to resolve any discrepancies Report to: Bill to: SUSAN CARSTENN Accounts Payable Tetra Tech Inc Tetra Tech Inc 180 Howard Street 180 Howard Street Suite 250 Suite 250 San Francisco, CA94105 San Francisco, CA Client STL Project : Makua Military Reservation Date Rec: 9/21/06 Number : Quote No: Manager : SUSAN CARSTENN Manager : Robert Hrabak Due Dates Preliminary: 10/09/06 Hard Copy : 10/12/06 Analytical TAT: Client ID: 2FD Date Sampled: 8/03/06 Time Sampled: :00 LAB ID: G6I Matrix: BIOLOGICAL Parameter Method BIOLOGIC, 8330, Special List SW BIOLOGIC, 8290, Dioxins/Furans SW Rep Client ID: NW1FD Date Sampled: 8/05/06 Time Sampled: :00 LAB ID: G6I Matrix: BIOLOGICAL Parameter Method BIOLOGIC, 8330, Special List SW BIOLOGIC, 8290, Dioxins/Furans SW Rep Client ID: NW2FD Date Sampled: 8/19/06 Time Sampled: :00 LAB ID: G6I Matrix: BIOLOGICAL Parameter Method BIOLOGIC, 8330, Special List SW BIOLOGIC, 8290, Dioxins/Furans SW Rep Client ID: NW1SW1-1FD Date Sampled: 8/09/06 Time Sampled: :00 LAB ID: G6I Matrix: BIOLOGICAL Parameter Method BIOLOGIC, 8330, Special List SW BIOLOGIC, 8290, Dioxins/Furans SW Rep STL Sacramento is a part of Severn Trent Laboratories, Inc.
92 RSR011 SEVERN TRENT LABORATORIES, INC. Run Date: 9/22/06 SAMPLE CONFIRMATION REPORT Page : 2 Time : 8:06:14 Client STL Project : Makua Military Reservation Date Rec: 9/21/06 Number : Quote No: Manager : SUSAN CARSTENN Manager : Robert Hrabak Due Dates Preliminary: 10/09/06 Hard Copy : 10/12/06 Analytical TAT: Client ID: 9AFD AND 10A COMP Date Sampled: 8/03/06 Time Sampled: :00 LAB ID: G6I Matrix: BIOLOGICAL Parameter Method BIOLOGIC, 8330, Special List SW BIOLOGIC, 8290, Dioxins/Furans SW Rep STL Sacramento is a part of Severn Trent Laboratories, Inc.
93 SEVERN TRENT LABORATORIES, INC. PRELIMINARY DATA SUMMARY The results shown below may still require additional laboratory review and are subject to change. Actions taken based on these results are the responsibility of the data user Tetra Tech Inc PAGE 1 Lot #: G6I Makua Military Reservation Date Reported: 10/11/06 REPORTING ANALYTICAL PARAMETER RESULT LIMIT UNITS METHOD Client Sample ID: 2fd Sample #: 001 Date Sampled: 08/03/06 Date Received: 09/21/06 Matrix: BIOLOGIC Nitroaromatics and Nitramines by HPLC 2,4-Dinitrotoluene ND 0.25 mg/kg SW Nitroglycerin 0.69 AA 0.50 mg/kg SW RDX ND 0.25 mg/kg SW Reviewed AA=see case narrative Dibenzodioxins and Dibenzofurans, HRGC/HRMS 2,3,7,8-TCDD ND 0.33 pg/g SW Total TCDD ND 0.33 pg/g SW ,2,3,7,8-PeCDD ND 0.79 pg/g SW Total PeCDD ND 0.79 pg/g SW ,2,3,4,7,8-HxCDD ND 0.54 pg/g SW ,2,3,6,7,8-HxCDD ND 0.52 pg/g SW ,2,3,7,8,9-HxCDD ND 0.51 pg/g SW Total HxCDD ND 0.54 pg/g SW ,2,3,4,6,7,8-HpCDD ND 1.7 pg/g SW Total HpCDD ND 1.7 pg/g SW OCDD 8.7 J pg/g SW ,3,7,8-TCDF 0.59 J,CON pg/g SW Total TCDF 0.59 pg/g SW ,2,3,7,8-PeCDF ND 0.49 pg/g SW ,3,4,7,8-PeCDF ND 0.49 pg/g SW Total PeCDF ND 1.2 pg/g SW ,2,3,4,7,8-HxCDF ND 0.51 pg/g SW ,2,3,6,7,8-HxCDF ND 0.37 pg/g SW ,3,4,6,7,8-HxCDF ND 0.41 pg/g SW ,2,3,7,8,9-HxCDF ND 0.45 pg/g SW Total HxCDF ND 0.51 pg/g SW ,2,3,4,6,7,8-HpCDF ND 1.3 pg/g SW ,2,3,4,7,8,9-HpCDF ND 0.43 pg/g SW Total HpCDF ND 1.3 pg/g SW OCDF ND 1.1 pg/g SW Reviewed J Estimated result. Result is less than the reporting limit. CON Confirmation analysis. (Continued on next page) STL Sacramento is a part of Severn Trent Laboratories, Inc.
94 SEVERN TRENT LABORATORIES, INC. PRELIMINARY DATA SUMMARY The results shown below may still require additional laboratory review and are subject to change. Actions taken based on these results are the responsibility of the data user Tetra Tech Inc PAGE 2 Lot #: G6I Makua Military Reservation Date Reported: 10/11/06 REPORTING ANALYTICAL PARAMETER RESULT LIMIT UNITS METHOD Client Sample ID: NW1fd Sample #: 002 Date Sampled: 08/05/06 Date Received: 09/21/06 Matrix: BIOLOGIC Nitroaromatics and Nitramines by HPLC 2,4-Dinitrotoluene ND 0.25 mg/kg SW Nitroglycerin 0.33 J 0.50 mg/kg SW RDX J 0.25 mg/kg SW Reviewed J Estimated result. Result is less than RL. Dibenzodioxins and Dibenzofurans, HRGC/HRMS 2,3,7,8-TCDD ND 0.41 pg/g SW Total TCDD ND 0.41 pg/g SW ,2,3,7,8-PeCDD ND 0.77 pg/g SW Total PeCDD ND 0.77 pg/g SW ,2,3,4,7,8-HxCDD ND 0.46 pg/g SW ,2,3,6,7,8-HxCDD ND 0.44 pg/g SW ,2,3,7,8,9-HxCDD ND 0.43 pg/g SW Total HxCDD ND 0.46 pg/g SW ,2,3,4,6,7,8-HpCDD ND 0.82 pg/g SW Total HpCDD ND 0.82 pg/g SW OCDD ND 3.3 pg/g SW ,3,7,8-TCDF ND 0.41 pg/g SW Total TCDF ND 0.41 pg/g SW ,2,3,7,8-PeCDF ND 0.51 pg/g SW ,3,4,7,8-PeCDF ND 0.51 pg/g SW Total PeCDF ND 0.51 pg/g SW ,2,3,4,7,8-HxCDF ND 0.36 pg/g SW ,2,3,6,7,8-HxCDF ND 0.34 pg/g SW ,3,4,6,7,8-HxCDF ND 0.37 pg/g SW ,2,3,7,8,9-HxCDF ND 0.41 pg/g SW Total HxCDF ND 0.41 pg/g SW ,2,3,4,6,7,8-HpCDF ND 1.2 pg/g SW ,2,3,4,7,8,9-HpCDF ND 0.44 pg/g SW Total HpCDF ND 1.2 pg/g SW OCDF ND 0.87 pg/g SW Reviewed (Continued on next page) STL Sacramento is a part of Severn Trent Laboratories, Inc.
95 SEVERN TRENT LABORATORIES, INC. PRELIMINARY DATA SUMMARY The results shown below may still require additional laboratory review and are subject to change. Actions taken based on these results are the responsibility of the data user Tetra Tech Inc PAGE 3 Lot #: G6I Makua Military Reservation Date Reported: 10/11/06 REPORTING ANALYTICAL PARAMETER RESULT LIMIT UNITS METHOD Client Sample ID: NW2fd Sample #: 003 Date Sampled: 08/19/06 Date Received: 09/21/06 Matrix: BIOLOGIC Nitroaromatics and Nitramines by HPLC 2,4-Dinitrotoluene ND 0.25 mg/kg SW Nitroglycerin ND 0.50 mg/kg SW RDX ND 0.25 mg/kg SW Dibenzodioxins and Dibenzofurans, HRGC/HRMS 2,3,7,8-TCDD ND 0.34 pg/g SW Total TCDD ND 0.34 pg/g SW ,2,3,7,8-PeCDD ND 0.69 pg/g SW Total PeCDD ND 0.69 pg/g SW ,2,3,4,7,8-HxCDD ND 0.49 pg/g SW ,2,3,6,7,8-HxCDD ND 0.48 pg/g SW ,2,3,7,8,9-HxCDD ND 0.46 pg/g SW Total HxCDD ND 0.49 pg/g SW ,2,3,4,6,7,8-HpCDD ND 0.48 pg/g SW Total HpCDD ND 0.48 pg/g SW OCDD ND 1.3 pg/g SW ,3,7,8-TCDF ND 0.22 pg/g SW Total TCDF ND 0.22 pg/g SW ,2,3,7,8-PeCDF ND 0.48 pg/g SW ,3,4,7,8-PeCDF ND 0.47 pg/g SW Total PeCDF ND 0.48 pg/g SW ,2,3,4,7,8-HxCDF ND 0.32 pg/g SW ,2,3,6,7,8-HxCDF ND 0.30 pg/g SW ,3,4,6,7,8-HxCDF ND 0.34 pg/g SW ,2,3,7,8,9-HxCDF ND 0.37 pg/g SW Total HxCDF ND 0.34 pg/g SW ,2,3,4,6,7,8-HpCDF ND 0.48 pg/g SW ,2,3,4,7,8,9-HpCDF ND 0.41 pg/g SW Total HpCDF ND 0.48 pg/g SW OCDF ND 0.68 pg/g SW Reviewed Reviewed Client Sample ID: NW1SW1-1fd Sample #: 004 Date Sampled: 08/09/06 Date Received: 09/21/06 Matrix: BIOLOGIC (Continued on next page) STL Sacramento is a part of Severn Trent Laboratories, Inc.
96 SEVERN TRENT LABORATORIES, INC. PRELIMINARY DATA SUMMARY The results shown below may still require additional laboratory review and are subject to change. Actions taken based on these results are the responsibility of the data user Tetra Tech Inc PAGE 4 Lot #: G6I Makua Military Reservation Date Reported: 10/11/06 REPORTING ANALYTICAL PARAMETER RESULT LIMIT UNITS METHOD Client Sample ID: NW1SW1-1fd Sample #: 004 Date Sampled: 08/09/06 Date Received: 09/21/06 Matrix: BIOLOGIC Nitroaromatics and Nitramines by HPLC 2,4-Dinitrotoluene ND 0.25 mg/kg SW Nitroglycerin ND 0.50 mg/kg SW RDX 0.38 PG 0.25 mg/kg SW Reviewed PG The percent difference between the original and confirmation analyses is greater than 40%. Dibenzodioxins and Dibenzofurans, HRGC/HRMS 2,3,7,8-TCDD ND 0.37 pg/g SW Total TCDD ND 0.37 pg/g SW ,2,3,7,8-PeCDD ND 0.55 pg/g SW Total PeCDD ND 0.55 pg/g SW ,2,3,4,7,8-HxCDD ND 0.42 pg/g SW ,2,3,6,7,8-HxCDD ND 0.41 pg/g SW ,2,3,7,8,9-HxCDD ND 0.39 pg/g SW Total HxCDD ND 0.42 pg/g SW ,2,3,4,6,7,8-HpCDD ND 0.42 pg/g SW Total HpCDD ND 0.42 pg/g SW OCDD ND 0.55 pg/g SW ,3,7,8-TCDF ND 0.21 pg/g SW Total TCDF ND 0.21 pg/g SW ,2,3,7,8-PeCDF ND 0.42 pg/g SW ,3,4,7,8-PeCDF ND 0.42 pg/g SW Total PeCDF ND 0.42 pg/g SW ,2,3,4,7,8-HxCDF ND 0.26 pg/g SW ,2,3,6,7,8-HxCDF ND 0.24 pg/g SW ,3,4,6,7,8-HxCDF ND 0.27 pg/g SW ,2,3,7,8,9-HxCDF ND 0.29 pg/g SW Total HxCDF ND 0.29 pg/g SW ,2,3,4,6,7,8-HpCDF ND 0.30 pg/g SW ,2,3,4,7,8,9-HpCDF ND 0.34 pg/g SW Total HpCDF ND 0.34 pg/g SW OCDF ND 0.59 pg/g SW Reviewed (Continued on next page) STL Sacramento is a part of Severn Trent Laboratories, Inc.
97 SEVERN TRENT LABORATORIES, INC. PRELIMINARY DATA SUMMARY The results shown below may still require additional laboratory review and are subject to change. Actions taken based on these results are the responsibility of the data user Tetra Tech Inc PAGE 5 Lot #: G6I Makua Military Reservation Date Reported: 10/11/06 REPORTING ANALYTICAL PARAMETER RESULT LIMIT UNITS METHOD Client Sample ID: 9afd and 10a Comp Sample #: 005 Date Sampled: 08/03/06 Date Received: 09/21/06 Matrix: BIOLOGIC Nitroaromatics and Nitramines by HPLC 2,4-Dinitrotoluene ND 0.25 mg/kg SW Nitroglycerin 0.95 PG 0.50 mg/kg SW RDX ND 0.25 mg/kg SW Reviewed PG The percent difference between the original and confirmation analyses is greater than 40%. Dibenzodioxins and Dibenzofurans, HRGC/HRMS 2,3,7,8-TCDD ND 0.39 pg/g SW Total TCDD ND 0.39 pg/g SW ,2,3,7,8-PeCDD ND 0.79 pg/g SW Total PeCDD ND 1.2 pg/g SW ,2,3,4,7,8-HxCDD ND 0.63 pg/g SW ,2,3,6,7,8-HxCDD ND 0.61 pg/g SW ,2,3,7,8,9-HxCDD ND 0.58 pg/g SW Total HxCDD ND 0.63 pg/g SW ,2,3,4,6,7,8-HpCDD ND 1.5 pg/g SW Total HpCDD ND 1.5 pg/g SW OCDD 6.9 J pg/g SW ,3,7,8-TCDF ND 0.26 pg/g SW Total TCDF ND 0.26 pg/g SW ,2,3,7,8-PeCDF ND 0.61 pg/g SW ,3,4,7,8-PeCDF ND 0.60 pg/g SW Total PeCDF ND 0.61 pg/g SW ,2,3,4,7,8-HxCDF ND 0.34 pg/g SW ,2,3,6,7,8-HxCDF ND 0.32 pg/g SW ,3,4,6,7,8-HxCDF ND 0.36 pg/g SW ,2,3,7,8,9-HxCDF ND 0.40 pg/g SW Total HxCDF ND 0.40 pg/g SW ,2,3,4,6,7,8-HpCDF ND 0.63 pg/g SW ,2,3,4,7,8,9-HpCDF ND 0.49 pg/g SW Total HpCDF ND 0.63 pg/g SW OCDF ND 0.82 pg/g SW Reviewed J Estimated result. Result is less than the reporting limit. STL Sacramento is a part of Severn Trent Laboratories, Inc.
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