APPENDIX H CHEMICAL TESTING
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1 APPENDIX H CHEMICAL TESTING
2 APPENDIX H CHEMICAL TESTING TABLE OF CONTENTS ATTACHMENTS AETL Report B-10 and B-11for Disposal (16 pages) Disposal Manifest Form (3 pages) R1-AH/wp/ADY H-i
3 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Attention: Dean Francuch Number of Pages 12 Date Received 08/23/2012 Date Reported 09/04/2012 Job Number Order Date Client Site: San Pedro, CA Enclosed please find results of analyses of 2 soil samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call. Checked By: Approved By: Cyrus Razmara, Ph.D. Laboratory Director
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5 1 A Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Attention: Dean Francuch Date Received 08/23/2012 Date Reported 09/04/2012 Job Number Order Date Client CERTIFICATE OF ANALYSIS CASE NARRATIVE AETL received 2 samples with the following specification on 08/23/2012. Lab ID Sample ID Sample Date Matrix QTY of Containers B-10 08/22/2012 Soil B-11 08/22/2012 Soil 1 The samples were analyzed as specified on the enclosed chain of custody. Analytical non-conformances have been noted on the report. Checked By: Approved By: Cyrus Razmara, Ph.D. Laboratory Director
6 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 2 ANALYTICAL RESULTS Site San Pedro, CA Method: (8260B), Volatile Organic Compounds by GC/MS (SW846) QC Batch No: A1 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/24/ /24/ /24/2012 Preparation Method Date Analyzed 08/24/ /24/ /24/2012 Matrix Soil Soil Soil Units ug/kg ug/kg ug/kg Dilution Factor Analytes MDL PQL Results Results Results Acetone Benzene Bromobenzene (Phenyl bromide) Bromochloromethane Bromodichloromethane Bromoform (Tribromomethane) Bromomethane (Methyl bromide) Butanone (MEK) n-butylbenzene sec-butylbenzene tert-butylbenzene Carbon Disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroethyl vinyl ether Chloroform (Trichloromethane) Chloromethane (Methyl chloride) Chlorotoluene Chlorotoluene ,2-Dibromo-3-chloropropane (DBCP) Dibromochloromethane ,2-Dibromoethane (EDB) Dibromomethane ,2-Dichlorobenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Dichlorodifluoromethane 15 30
7 3 ANALYTICAL RESULTS Method: (8260B), Volatile Organic Compounds by GC/MS (SW846) QC Batch No: A1 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/24/ /24/ /24/2012 Preparation Method Date Analyzed 08/24/ /24/ /24/2012 Matrix Soil Soil Soil Units ug/kg ug/kg ug/kg Dilution Factor Analytes MDL PQL Results Results Results 1,1-Dichloroethane ,2-Dichloroethane (EDC) ,1-Dichloroethene cis-1,2-dichloroethene trans-1,2-dichloroethene ,2-Dichloropropane ,3-Dichloropropane ,2-Dichloropropane ,1-Dichloropropene cis-1,3-dichloropropene trans-1,3-dichloropropene Ethylbenzene Hexachlorobutadiene Hexanone Iodomethane Isopropylbenzene p-isopropyltoluene Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether (MTBE) Methylene chloride (DCM) Naphthalene n-propylbenzene Styrene ,1,1,2-Tetrachloroethane ,1,2,2-Tetrachloroethane Tetrachloroethene Toluene (Methyl benzene) ,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,1,1-Trichloroethane ,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane ,2,3-Trichloropropane
8 4 ANALYTICAL RESULTS Method: (8260B), Volatile Organic Compounds by GC/MS (SW846) QC Batch No: A1 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/24/ /24/ /24/2012 Preparation Method Date Analyzed 08/24/ /24/ /24/2012 Matrix Soil Soil Soil Units ug/kg ug/kg ug/kg Dilution Factor Analytes MDL PQL Results Results Results 1,2,4-Trimethylbenzene ,3,5-Trimethylbenzene Vinyl Acetate Vinyl chloride (Chloroethene) o-xylene m,p-xylenes Our Lab I.D. Method Blank Surrogates %Rec.Limit % Rec. % Rec. % Rec. Bromofluorobenzene Dibromofluoromethane Toluene-d
9 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 5 ANALYTICAL RESULTS Site San Pedro, CA Method: (M8015G), TPH as Gasoline and Light Hydrocarbons Using GC/FID QC Batch No: OB2 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/24/ /24/ /24/2012 Preparation Method Date Analyzed 08/24/ /24/ /24/2012 Matrix Soil Soil Soil Units mg/kg mg/kg mg/kg Dilution Factor Analytes MDL PQL Results Results Results TPH as Gasoline and Light HC. (C4-C12) Our Lab I.D. Method Blank Surrogates %Rec.Limit % Rec. % Rec. % Rec. Bromofluorobenzene
10 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 6 ANALYTICAL RESULTS Site San Pedro, CA Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GC/FID QC Batch No: DB2 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/24/ /24/ /24/2012 Preparation Method 3550B 3550B 3550B Date Analyzed 08/24/ /24/ /24/2012 Matrix Soil Soil Soil Units mg/kg mg/kg mg/kg Dilution Factor Analytes MDL PQL Results Results Results TPH as Diesel (C13-C22) ND 22.1 ND TPH as Heavy Hydrocarbons (C23-C40) ND 89.9 ND TPH Total as Diesel and Heavy HC.C13-C ND 112 ND Our Lab I.D. Method Blank Surrogates %Rec.Limit % Rec. % Rec. % Rec. Chlorobenzene
11 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 7 ANALYTICAL RESULTS Site San Pedro, CA Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846) QC Batch No: C1 Our Lab I.D. Method Blank Client Sample I.D. B-10 B-11 Date Sampled 08/22/ /22/2012 Date Prepared 08/30/ /30/ /30/2012 Preparation Method 3050B 3050B 3050B Date Analyzed 08/30/ /30/ /30/2012 Matrix Soil Soil Soil Units mg/kg mg/kg mg/kg Dilution Factor Analytes MDL PQL Results Results Results Antimony Arsenic Barium ND Beryllium Cadmium Chromium ND J Cobalt ND 2.80J ND Copper ND Lead Mercury (By EPA 7471) Molybdenum ND 4.06J ND Nickel ND Selenium Silver Thallium Vanadium ND Zinc ND
12 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 8 QUALITY CONTROL RESULTS Site San Pedro, CA Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846) QC Batch No: C1; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/30/2012; QC Analyzed: 08/30/2012; Units: mg/kg Analytes Sample Result MS MS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD Concen Recov % REC Concen Recov % REC % % Limit % Limit Antimony M M <15 Arsenic <15 Barium <15 Beryllium <15 Cadmium <15 Chromium <15 Cobalt <15 Copper <15 Lead <15 Mercury (By EPA 7471) < <15 Molybdenum <15 Nickel <15 Selenium < <15 Silver <15 Thallium M M <15 Vanadium <15 Zinc M <15 QC Batch No: C1; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/30/2012; QC Analyzed: 08/30/2012; Units: mg/kg Analytes LCS Concen LCS LCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD Recov % REC Concen Recov % REC % REC % Limit % Limit Antimony < <15 Arsenic < <15 Barium < <15 Beryllium < <15 Cadmium < <15 Chromium < <15 Cobalt < <15 Copper < <15 Lead < <15
13 9 QUALITY CONTROL RESULTS Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846) QC Batch No: C1; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/30/2012; QC Analyzed: 08/30/2012; Units: mg/kg Analytes LCS Concen LCS LCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD Recov % REC Concen Recov % REC % REC % Limit % Limit Mercury (By EPA 7471) < <15 Molybdenum < <15 Nickel < <15 Selenium < <15 Silver < <15 Thallium < <15 Vanadium < <15 Zinc < <15
14 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 10 QUALITY CONTROL RESULTS Site San Pedro, CA Method: (8260B), Volatile Organic Compounds by GC/MS (SW846) QC Batch No: A1; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012; Units: ug/kg Analytes Sample Result MS MS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD Concen Recov % REC Concen Recov % REC % % Limit % Limit Benzene <20 Chlorobenzene <20 1,1-Dichloroethene <20 Methyl-tert-butyl ether (MTBE) <20 Toluene (Methyl benzene) <20 Trichloroethene <20 Surrogates Bromofluorobenzene <20 Dibromofluoromethane <20 Toluene-d < <20 QC Batch No: A1; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012; Units: ug/kg Analytes LCS Concen LCS LCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD Recov % REC Concen Recov % REC % REC % Limit % Limit Benzene <20 Chlorobenzene <20 1,1-Dichloroethene <20 Methyl-tert-butyl ether (MTBE) <20 Toluene (Methyl benzene) < <20 Trichloroethene < <20 LCS Chloroform (Trichloromethane) <20 Ethylbenzene < <20 1,1,1-Trichloroethane < <20 o-xylene < <20 m,p-xylenes < <20 Surrogates Bromofluorobenzene < <20 Dibromofluoromethane < <20 Toluene-d < <20
15 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 11 QUALITY CONTROL RESULTS Site San Pedro, CA Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GC/FID QC Batch No: DB2; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012; Units: mg/kg Analytes Sample Result MS MS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD Concen Recov % REC Concen Recov % REC % % Limit % Limit TPH as Diesel (C13-C22) <20 Surrogates Chlorobenzene <20 QC Batch No: DB2; Dup or Spiked Sample: ; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/24/2012; Units: mg/kg LCS LCS LCS LCS/LCSD Analytes Concen Recov % REC % Limit TPH as Diesel (C13-C22) Surrogates Chlorobenzene
16 Ordered By Shannon & Wilson 664 W. Broadway Avenue Glendale, CA Telephone: (818) Dean Francuch Attn: 12 QUALITY CONTROL RESULTS Site San Pedro, CA Method: (M8015G), TPH as Gasoline and Light Hydrocarbons Using GC/FID QC Batch No: OB2; Dup or Spiked Sample: A; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/25/2012; Units: mg/kg Analytes TPH as Gasoline and Light HC. (C4-C12) Surrogates Sample MS MS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD Result Concen Recov % REC Concen Recov % REC % % Limit % Limit <20 Bromofluorobenzene <20 QC Batch No: OB2; Dup or Spiked Sample: A; LCS: Clean Sand; QC Prepared: 08/24/2012; QC Analyzed: 08/25/2012; Units: mg/kg Analytes TPH as Gasoline and Light HC. (C4-C12) Surrogates LCS LCS LCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD Concen Recov % REC Concen Recov % REC % REC % Limit % Limit <20 Bromofluorobenzene <20
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