Limited Site Investigation

Transcription

1 Limited Site Investigation Lot 20 Northwest Corner of West Osceola Parkway and Orange Avenue Kissimmee, Osceola County, Florida April 7, 2017 Terracon Project No. H Prepared for: Deerfield Land Corporation Orlando, Florida Prepared by: Terracon Consultants, Inc. Winter Park, Florida

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3 TABLE OF CONTENTS 1.0 SITE DESCRIPTION SCOPE OF SERVICES Standard of Care Additional Scope Limitations Reliance FIELD INVESTIGATION Soil Sampling and Analysis Temporary Monitoring Well Installation, Groundwater Sampling and Analysis Surface Water Sampling and Analysis CONCLSIONS RECOMMENDATIONS... 7 APPENDIX A EXHIBITS Exhibit 1 Topographic Map Exhibit 2 Site Diagram APPENDIX B FIELD NOTES Boring Logs Groundwater Sampling Logs Field Instrument Calibration Records APPENDIX C ANALYTICAL REPORT AND CHAIN OF CSTODY ii

4 LIMITED SITE INVESTIGATION LOT 20 NORTHWEST CORNER of WEST OSCEOLA PARKWAY AND ORANGE AVENE KISSIMMEE, OSCEOLA CONTY, FLORIDA 1.0 SITE DESCRIPTION Terracon Project No. H April 7, 2017 The Lot 20 site is a acre parcel of wooded land (Osceola County Property Appraiser parcel ID # ) located at the northwest of the intersection of Orange Avenue and East Osceola Parkway in Kissimmee, Osceola County, Florida. A Topographic Map showing the site location is included as Exhibit 1 and a Site Diagram is included as Exhibit 2 in Appendix A. Terracon previously completed a Phase I Environmental Site Assessment of the site (Terracon Project No. H , report dated March 8, 2017). At the time of the site reconnaissance, the site was predominantly wooded with manmade ponds on the west and northeast portions of the site. Based on a review of the historical information, the site was sparsely wooded land crossed by two roads from at least 1944 until the early 1980s, when the northeast portion of the site was developed as a portion of a golf course. The roads were removed in the late 1980s. Review of the aerial photograph dated 1984 identified one location of cleared land in the northwest portion of the site that appeared to be used for golf course landscape related disposal activities. Dumping and burial of refuse reported as primarily consisting of paper and construction debris was conducted by Tupperware at three on-site locations at the west portion of the site in the early 1980s. The refuse was reported by the client to have been excavated and removed from the site in the mid-1990s where the pond exists at the west portion of the site. A previous Report of Investigation prepared by ERC Groundwater Services, Inc. dated June 1990 for the site was provided by the client to Terracon for review. The report indicates that the shallow groundwater flow direction was measured toward the northwest during the investigation activities. 2.0 SCOPE OF SERVICES Terracon s LSI was undertaken in response to the results of our Phase I Environmental Site Assessment of the site (Terracon Project No. H , report dated March 8, 2017), which identified the following recognized environmental conditions (RECs). Potential impacts to soil attributed to historical pesticide application associated with previous golf course turf maintenance at the northeast portion of the site. Potential previous golf course related disposal activities in the northwest portion of the site. Responsive Resourceful Reliable

5 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H Potential impacts to groundwater associated with the previous refuse burial at the west portion of the site. The LSI was conducted to visually screen soil in the areas of the historical refuse burials as well as to determine the presence or absence of arsenic, organochlorine pesticides and petroleum constituents in groundwater in the refuse burial areas. The LSI was also conducted to evaluate presence or absence of arsenic and organochlorine pesticide in soil at the previous golf greens. The scope of services was not intended to identify every chemical possibly associated with the site. Similarly, the proposed scope was not intended to determine the extent or magnitude of any existing contamination. 2.1 Standard of Care Terracon s services were performed in a manner consistent with generally accepted practices of the profession undertaken in similar studies in the same geographical area during the same time. Terracon makes no warranties, either express or implied, regarding the findings, conclusions, or recommendations. Please note that Terracon does not warrant the work of laboratories, regulatory agencies, or other third parties supplying information used in the preparation of the report. These LSI services were performed in accordance with the scope of work agreed with you, our client, as reflected in our proposal and were not restricted by ASTM E Additional Scope Limitations Findings, conclusions, and recommendations resulting from these services are based upon information derived from the on-site activities and other services performed under this scope of work; such information is subject to change over time. Certain indicators of the presence of hazardous substances, petroleum products, or other constituents may have been latent, inaccessible, unobservable, nondetectable, or not present during these services. We cannot represent that the site contains no hazardous substances, toxic materials, petroleum products, or other latent conditions beyond those identified during this LSI. Subsurface conditions may vary from those encountered at specific borings or wells or during other surveys, tests, assessments, investigations, or exploratory services. The data, interpretations, findings, and our recommendations are based solely upon data obtained at the time and within the scope of these services. 2.3 Reliance This report has been prepared for the exclusive use of Deerfield Land Corporation, and any authorization for use or reliance by any other party (except a governmental entity having jurisdiction over the site) is prohibited without the express written authorization of Deerfield Land Corporation and Terracon. Any unauthorized distribution or reuse is at Deerfield Land Corporation s sole risk. Notwithstanding the foregoing, reliance by authorized parties will be Responsive Resourceful Reliable 2

6 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H subject to the terms, conditions, and limitations stated in the proposal, LSI report, and Terracon s Agreement for Services. The limitation of liability defined in the terms and conditions is the aggregate limit of Terracon s liability to Deerfield Land Corporation and all relying parties unless otherwise agreed in writing. 3.0 FIELD INVESTIGATION Terracon has a 100% commitment to the safety of all its employees. As such, and in accordance with our Incident and Injury Free safety culture, a site safety pre-task plan was developed to identify potential safety concerns and prepare our personnel to handle conditions during field services. Prior to commencement of daily on-site activities, Terracon held a meeting with assigned staff to review the proposed work sequence and evaluate work practices for safe completion of the project. Fieldwork was conducted by environmental staff with OSHA training. Terracon contacted Sunshine 811 to mark locations of underground utilities in the work area prior to initiating intrusive activities. Soil sampling activities were conducted in general accordance with standard operating procedures established by the Florida Department of Environmental Protection (FDEP), DEP-SOP-001/ Soil Sampling and Analysis On March 9, 2017, Terracon advanced three soil borings B-1, B-2 and B-3 in the areas of the former on-site refuse burial areas along the west portion of the site. Approximate soil boring locations are shown on Exhibit 2 in Appendix A. Soil samples for visual screening were collected at 1-foot depth intervals to a depth of 1 to 2 feet below the groundwater table. The soils were visually screened for physical characteristics and potential refuse. Evidence of refuse was not observed at soil borings B-1 through B-3. Sandy to silty sandy soils were observed at the borings. Saturated soils were evident at an approximate depth of 4 to 5 feet below ground surface (bgs). A copy of the soil boring logs is contained in Appendix B. On March 13, 2017, Terracon collected soil samples for laboratory analysis of COC at select areas, including: soil boring B-15 at the previous golf course hole green area at the northeast portion of the site; and soil boring B-16 at the northwest portion of the site in an area suspected to have previously been used for golf course landscape related disposal activities. Approximate soil boring locations are shown on Exhibit 2 in Appendix A. Soil samples were collected at depths of 0 to 6 inches bgs and 6 to 24 inches bgs at both soil boring locations. The soil samples were placed in laboratory prepared glassware, labelled, and placed on ice in a cooler sealed with custody tape. The sample cooler and completed chain-of-custody record were relinquished to Pace Analytical Services, Inc. for analysis of organochlorine pesticides by EPA Method 8081 and arsenic concentrations by EPA Method The laboratory analytical report and chain-ofcustody record are attached in Appendix C. (Note that the laboratory report also contains analytical results for soil samples B-8-6', B-8-24', B-9-6', B-9-24', B-10-6', B-10-24', B-11-6', B-11-24', B-12-6', B-12-24, B-13-6', B-13-24', B-14-6' and B-14-24'. Those data are associated with soil Responsive Resourceful Reliable 3

7 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H borings B-1 through B-14 that were advanced within adjacent Lots 22 and 23, which are discussed in a separate LSI report). Laboratory analytical results for soil samples collected at boring locations B-15 and B-16 were compared to Florida s Soil Cleanup Target Levels (SCTLs) listed in Chapter , Florida Administrative Code (FAC). Reported organochlorine pesticide concentrations in the soil samples did not exceed laboratory method detection limits (MDLs). Table 1 contains a summary of reported arsenic concentrations in the soil samples. None of the tested analyte concentrations were reported above Florida s SCTLs. Boring ID Sample ID Sample Interval (feet below ground surface) TABLE 1 Arsenic (mg/kg) B to B-15 B to B to I B-16 B to Leachability-based SCTL *** Residential SCTL 2.1 Industrial SCTL 12 SCTL - Soil Cleanup Target Level specified in Table II of Chapter , FAC - Indicates that the compound was analyzed for but not detected. I - The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. mg/kg milligrams per kilogram *** - Leachability values may be derived using the SPLP Test to calculate site-specific SCTLs or may be determined using TCLP in the event oily wastes are present 3.2 Temporary Monitoring Well Installation, Groundwater Sampling and Analysis On March 9, 2017, the soil borings B-1, B-2 and B-3 advanced in the former refuse burial areas at the west portion of the site were converted into temporary shallow groundwater monitoring wells TMW-1, TMW-2 and TMW-3 respectively. Approximate shallow temporary monitoring well locations are shown on Exhibit 2 in Appendix A. The shallow temporary monitoring wells were installed using a direct-push drilling rig. The wells were constructed with 10 feet of 1-inch diameter inch factory-slotted Schedule 40 polyvinyl chloride (PVC) screen coupled to a section solid PVC riser that extended to a level approximately 3 feet above ground surface. The well screens were set at a depth of approximately 2 to 12 feet bgs to bracket the groundwater table and surrounded by a 30/65-graded sand filter pack. Responsive Resourceful Reliable 4

8 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H Terracon collected groundwater samples from temporary monitoring wells TMW-1, TMW-2 and TMW-3 on March 10, Prior to sample collection, each monitoring well was purged in accordance with DEP-SOP-01/001, FS Elevated turbidity at levels exceeding persisted while purging the wells. Temporary monitoring well TMW-1 purged dry and the groundwater was collected after recharge of the well. Field data sheets and equipment calibration logs are provided in Appendix B. Groundwater samples were collected using new polyethylene tubing and a peristaltic pump. Groundwater samples from the wells were placed in laboratory prepared glassware, labelled, and placed on ice in a cooler sealed with custody tape. The sample cooler and completed chain-of-custody record were relinquished to Pace Analytical Services, Inc. for analysis of volatile organic compounds (VOC) by EPA Method 8260, semivolatile organic compounds (SVOCs) by EPA Method 8270, total recoverable petroleum hydrocarbons (TRPH) by the FL-PRO method, organochlorine pesticides by EPA Method 8081 and arsenic concentrations (total and dissolved) by EPA Method The laboratory analytical report and chain-of-custody record are attached in Appendix C. (Note that the laboratory report also contains analytical results for groundwater samples TMW-4 and TMW-5. Those data are associated with adjacent Lots 22 and 23, which are discussed in a separate LSI report). Laboratory analytical results for groundwater samples TMW-1, TMW-2 and TMW-3 were compared to Florida s groundwater cleanup target levels (GCTLs) listed in Chapter , FAC. Table 2 contains a summary of reported arsenic concentrations in the groundwater samples. None of the other tested analyte concentrations were reported above Florida s GCTLs. Laboratory MDLs of 500 micrograms per liter (µg/l) for dissolved arsenic and 1,000 µg/l for total arsenic used for groundwater sample TMW-1, and the MDL of 50 µg/l used for total arsenic in groundwater sample TMW-2 exceed the GCTL for arsenic of 10 µg/l. The elevated MDLs are apparently attributed to matrix interference associated with elevated turbidity levels in these groundwater samples. A total arsenic concentration of 12.4 µg/l, slightly exceeding its GCTL, was reported in groundwater sample TMW-3; however, the dissolved arsenic concentration in sample TMW-3 did not exceed the laboratory MDL of 5.0 µg/l. The total arsenic concentration reported for sample TMW-3 apparently reflects turbidity. None of the other tested analyte concentrations were reported above Florida s GCTLs. Responsive Resourceful Reliable 5

9 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H TABLE 2 Arsenic Sample ID total / dissolved (µg/l) TMW / 1000 TMW / 5.0 TMW / 5.0 GCTL 10 NADC 100 GCTL - Groundwater Cleanup Target Level specified in Table I of Chapter , FAC NADC - Natural Attenuation Default Source Concentration specified in Table V of Chapter , FAC - Indicates that the compound was analyzed for but not detected. I - The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. µg/l - micrograms per liter TRPH - Total Recoverable Petroleum Hydrocarbons DEHP - Bis(2-Ethylhexyl)phthalate DNOP- Di-n-octylphthalate DBP Di-n-butylphthalate Bold - exceeds GCTL 3.3 Surface Water Sampling and Analysis On March 11, 2017, one surface water sample, SW-1, was collected at the central portion of the stormwater pond that was excavated in the area of the former refuse burial along the west portion of the site. The surface water sampling location is indicated on Exhibit 2. Surface water sampling activities were conducted in general accordance with standard operating procedures established by the FDEP-SOP-01/001, FS The surface water sample collected from the pond was placed in laboratory prepared glassware, labelled, and placed on ice in a cooler sealed with custody tape. The sample cooler and completed chain-of-custody record were relinquished to Pace Analytical Services, Inc. for analysis of VOC by EPA Method 8260, SVOCs by EPA Method 8270, TRPH by the FL-PRO method, organochlorine pesticides by EPA Method 8081 and arsenic concentration by EPA Method The laboratory analytical report and chain-of-custody record are attached in Appendix C. Laboratory analytical results for the surface water sample were compared to Florida s Freshwater Surface Water Cleanup Target Levels (SWCTLs) listed in Chapter , FAC. Table 3 contains a summary of reported aldrin and dieldrin in the surface water sample. Aldrin and dieldrin were estimated by the laboratory at concentrations of µg/l, exceeding Florida s SWCTLs for aldrin and dieldrin of µg/l, but below the laboratory Practical Quantitation Limits (PQLs) of µg/l. However, the laboratory reported PQLs of µg/l did not exceed the Target PQL of 0.05 µg/l for aldrin or Target PQL of 0.1 µg/l for dieldrin listed in Table D of the FDEP s Guidance for the Selection of Analytical Methods and for the Evaluation of Practical Quantitation Limits referenced in Chapter , dated October 12, According to the FDEP Division of Waste Management s cleanup rule guidance, if the cleanup target level (CTL) is lower than the Responsive Resourceful Reliable 6

10 Limited Site Investigation Lot 20 Kissimmee, Florida April 7, 2017 Terracon Project No. H PQL, the reported PQL (best achievable detection limit) becomes the alternative CTL. None of the other tested analyte concentrations in the surface water sample were reported above Florida s SWCTLs. TABLE 3 Sample ID Aldrin Dieldrin (µg/l) (µg/l) SW I I SWCTL PQL SWCTL - Surface Water Cleanup Target Levels specified in Table I of Chapter , FAC I - The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. µg/l - micrograms per liter PQL - Practical Quantitation Limits 4.0 CONCLSIONS Based on the scope of services described in this report and subject to the limitations described herein, Terracon concludes the following. Reported concentrations of organochlorine pesticides and arsenic did not exceed Florida s SCTLs in the soil samples collected at the previous golf course hole green area at the northeast portion of the site, or in an area at the northwest portion of the site suspected to have previously been used for golf course landscape related disposal activities. Buried refuse was not observed at the soil borings advanced in the area of the previous refuse burial at the west portion of the site. Detected concentrations of COCs tested in groundwater at the sampling locations did not exceed Florida s GCTLs, except for arsenic concentrations apparently reflecting sample turbidity associated with sampling activities, rather than static subsurface conditions. Detected concentrations of COCs tested at the surface water sampling location did not exceed either Florida s SWCTLs, or alternative SWCTLs based on PQLs. 5.0 RECOMMENDATIONS Based on the results of this LSI, no additional assessment appears warranted regarding the RECs identified in the Phase I ESA. Responsive Resourceful Reliable 7

11 APPENDIX A EXHIBITS

12 SITE Project Mngr: IIK Drawn By: IIK Checked By: ERK Approved By: ERK Project No. H Scale: AS SHOWN File No. H Date: February 2017 Consulting Engineers and Scientists 1675 LEE ROAD WINTER PARK, FLORIDA PH: (407) FAX: (407) TOPOGRAPHIC MAP LIMITED SITE INVESTIGATION LOT 20 WEST OSCEOLA PARKWAY KISSIMMEE, OSCEOLA CONTY, FLORIDA EXHIBIT 1

13 LEGEND - SITE/LOT BONDARY - FORMER REFSE DISPOSAL AREA - AREA OF POTENTIAL GOLF CORSE RELATED DISPOSAL ACTIVITIES - FORMER GOLF CORSE AREA - SOIL SCREENING BORING / TEMPORARY MONITORING WELL LOCATION - SRFACE WATER SAMPLING LOCATION - SOIL SAMPLING LOCATION FOR ARSENIC AND CHLORINATED PESTICIDES Project Mngr: IIK Drawn By: IIK Checked By: ERK Approved By: ERK Project No. H Scale: AS SHOWN File No. H Date: February 2017 Consulting Engineers and Scientists 1675 LEE ROAD WINTER PARK, FLORIDA PH: (407) FAX: (407) SITE DIAGRAM LIMITED SITE INVESTIGATION LOT 20 WEST OSCEOLA PARKWAY KISSIMMEE, OSCEOLA CONTY, FLORIDA EXHIBIT 2

14 APPENDIX B FIELD NOTES

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21 APPENDIX C ANALYTICAL REPORT AND CHAIN OF CSTODY

22 #=CL# LIMS SE: FR - IGOR KARIMOV LIMS OBJECT ID: March 22, 2017 Igor Karimov Terracon Consulting Engineers 1675 Lee Road Winter Park, FL RE: H / LOT 20,22, Dear Igor Karimov: Enclosed are the analytical results for sample(s) received by the laboratory on March 15, The results relate only to the samples included in this report. s reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sakina Mckenzie sakina.mckenzie@pacelabs.com Project Manager Enclosures without the written consent of. Page 1 of 35

23 #=CP# CERTIFICATIONS H / LOT 20,22, Ormond Beach Certification IDs, Alabama Certification #: Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS Nevada Certification: FL NELAC Reciprocity New York Certification #: North Carolina Environmental Certificate #: 667 North Carolina Certification #: Oklahoma Certification #: D9947 Pennsylvania Certification #: Puerto Rico Certification #: FL01264 South Carolina Certification: # Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity S Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: Wyoming (EPA Region 8): FL NELAC Reciprocity without the written consent of. Page 2 of 35

24 #=SS# SAMPLE SMMARY H / LOT 20,22, Lab ID Sample ID Matrix Date Collected Date Received B-16-6' Solid 03/13/17 11:50 03/15/17 03: B-16-24' Solid 03/13/17 11:55 03/15/17 03: B-15-6' Solid 03/13/17 13:15 03/15/17 03: B-15-24' Solid 03/13/17 13:16 03/15/17 03: B-14-6' Solid 03/13/17 13:20 03/15/17 03: B-14-24' Solid 03/13/17 13:22 03/15/17 03: B-13-6' Solid 03/13/17 13:25 03/15/17 03: B-13-24' Solid 03/13/17 13:26 03/15/17 03: B-11-6' Solid 03/13/17 13:45 03/15/17 03: B-11-24' Solid 03/13/17 13:46 03/15/17 03: B-10-6' Solid 03/13/17 13:49 03/15/17 03: B-10-24' Solid 03/13/17 13:50 03/15/17 03: B-12-6' Solid 03/13/17 14:05 03/15/17 03: B Solid 03/13/17 14:07 03/15/17 03: B-8-6 Solid 03/13/17 14:25 03/15/17 03: B-8-24 Solid 03/13/17 14:26 03/15/17 03: B-9-6 Solid 03/13/17 14:30 03/15/17 03: B-9-24 Solid 03/13/17 14:32 03/15/17 03:20 without the written consent of. Page 3 of 35

25 #=SA# SAMPLE ANALYTE CONT H / LOT 20,22, Lab ID Sample ID Method Analysts Analytes Reported Laboratory B-16-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-16-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-15-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-15-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-14-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-14-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-13-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-13-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-11-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-11-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-10-6' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-10-24' EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-12-6' EPA 8081 JLG 22 PASI-O without the written consent of. Page 4 of 35

26 #=SA# SAMPLE ANALYTE CONT H / LOT 20,22, Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-8-6 EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-8-24 EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-9-6 EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O B-9-24 EPA 8081 JLG 22 PASI-O EPA 6010 BTS 1 PASI-O ASTM D MED 1 PASI-O without the written consent of. Page 5 of 35

27 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-16-6' Lab ID: Collected: 03/13/17 11:50 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 16: alpha-bhc mg/kg /16/17 09:15 03/16/17 16: beta-bhc mg/kg /16/17 09:15 03/16/17 16: delta-bhc mg/kg /16/17 09:15 03/16/17 16: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 16: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 16: ,4'-DDD mg/kg /16/17 09:15 03/16/17 16: ,4'-DDE mg/kg /16/17 09:15 03/16/17 16: ,4'-DDT mg/kg /16/17 09:15 03/16/17 16: Dieldrin mg/kg /16/17 09:15 03/16/17 16: Endosulfan I mg/kg /16/17 09:15 03/16/17 16: Endosulfan II mg/kg /16/17 09:15 03/16/17 16: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 16: Endrin mg/kg /16/17 09:15 03/16/17 16: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 16: Endrin ketone mg/kg /16/17 09:15 03/16/17 16: Heptachlor mg/kg /16/17 09:15 03/16/17 16: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 16: Methoxychlor mg/kg /16/17 09:15 03/16/17 16: Toxaphene mg/kg /16/17 09:15 03/16/17 16: Surrogates Tetrachloro-m-xylene (S) 88 % /16/17 09:15 03/16/17 16: Decachlorobiphenyl (S) 76 % /16/17 09:15 03/16/17 16: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.32 I mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.9 % /21/17 14:20 Date: 03/22/ :47 AM without the written consent of. Page 6 of 35

28 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-16-24' Lab ID: Collected: 03/13/17 11:55 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 16: alpha-bhc mg/kg /16/17 09:15 03/16/17 16: beta-bhc mg/kg /16/17 09:15 03/16/17 16: delta-bhc mg/kg /16/17 09:15 03/16/17 16: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 16: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 16: ,4'-DDD mg/kg /16/17 09:15 03/16/17 16: ,4'-DDE mg/kg /16/17 09:15 03/16/17 16: ,4'-DDT mg/kg /16/17 09:15 03/16/17 16: Dieldrin mg/kg /16/17 09:15 03/16/17 16: Endosulfan I mg/kg /16/17 09:15 03/16/17 16: Endosulfan II mg/kg /16/17 09:15 03/16/17 16: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 16: Endrin mg/kg /16/17 09:15 03/16/17 16: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 16: Endrin ketone mg/kg /16/17 09:15 03/16/17 16: Heptachlor mg/kg /16/17 09:15 03/16/17 16: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 16: Methoxychlor mg/kg /16/17 09:15 03/16/17 16: Toxaphene mg/kg /16/17 09:15 03/16/17 16: Surrogates Tetrachloro-m-xylene (S) 85 % /16/17 09:15 03/16/17 16: Decachlorobiphenyl (S) 81 % /16/17 09:15 03/16/17 16: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.30 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.4 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 7 of 35

29 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-15-6' Lab ID: Collected: 03/13/17 13:15 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 18: alpha-bhc mg/kg /16/17 09:15 03/16/17 18: beta-bhc mg/kg /16/17 09:15 03/16/17 18: delta-bhc mg/kg /16/17 09:15 03/16/17 18: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 18: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 18: ,4'-DDD mg/kg /16/17 09:15 03/16/17 18: ,4'-DDE mg/kg /16/17 09:15 03/16/17 18: ,4'-DDT mg/kg /16/17 09:15 03/16/17 18: Dieldrin mg/kg /16/17 09:15 03/16/17 18: Endosulfan I mg/kg /16/17 09:15 03/16/17 18: Endosulfan II mg/kg /16/17 09:15 03/16/17 18: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 18: Endrin mg/kg /16/17 09:15 03/16/17 18: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 18: Endrin ketone mg/kg /16/17 09:15 03/16/17 18: Heptachlor mg/kg /16/17 09:15 03/16/17 18: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 18: Methoxychlor mg/kg /16/17 09:15 03/16/17 18: Toxaphene mg/kg /16/17 09:15 03/16/17 18: Surrogates Tetrachloro-m-xylene (S) 94 % /16/17 09:15 03/16/17 18: Decachlorobiphenyl (S) 87 % /16/17 09:15 03/16/17 18: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.25 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.47 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 8 of 35

30 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-15-24' Lab ID: Collected: 03/13/17 13:16 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 19: alpha-bhc mg/kg /16/17 09:15 03/16/17 19: beta-bhc mg/kg /16/17 09:15 03/16/17 19: delta-bhc mg/kg /16/17 09:15 03/16/17 19: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 19: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 19: ,4'-DDD mg/kg /16/17 09:15 03/16/17 19: ,4'-DDE mg/kg /16/17 09:15 03/16/17 19: ,4'-DDT mg/kg /16/17 09:15 03/16/17 19: Dieldrin mg/kg /16/17 09:15 03/16/17 19: Endosulfan I mg/kg /16/17 09:15 03/16/17 19: Endosulfan II mg/kg /16/17 09:15 03/16/17 19: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 19: Endrin mg/kg /16/17 09:15 03/16/17 19: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 19: Endrin ketone mg/kg /16/17 09:15 03/16/17 19: Heptachlor mg/kg /16/17 09:15 03/16/17 19: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 19: Methoxychlor mg/kg /16/17 09:15 03/16/17 19: Toxaphene mg/kg /16/17 09:15 03/16/17 19: Surrogates Tetrachloro-m-xylene (S) 85 % /16/17 09:15 03/16/17 19: Decachlorobiphenyl (S) 78 % /16/17 09:15 03/16/17 19: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.28 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.0 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 9 of 35

31 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-14-6' Lab ID: Collected: 03/13/17 13:20 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 17: alpha-bhc mg/kg /16/17 09:15 03/16/17 17: beta-bhc mg/kg /16/17 09:15 03/16/17 17: delta-bhc mg/kg /16/17 09:15 03/16/17 17: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 17: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 17: ,4'-DDD mg/kg /16/17 09:15 03/16/17 17: ,4'-DDE mg/kg /16/17 09:15 03/16/17 17: ,4'-DDT mg/kg /16/17 09:15 03/16/17 17: Dieldrin mg/kg /16/17 09:15 03/16/17 17: Endosulfan I mg/kg /16/17 09:15 03/16/17 17: Endosulfan II mg/kg /16/17 09:15 03/16/17 17: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 17: Endrin mg/kg /16/17 09:15 03/16/17 17: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 17: Endrin ketone mg/kg /16/17 09:15 03/16/17 17: Heptachlor mg/kg /16/17 09:15 03/16/17 17: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 17: Methoxychlor mg/kg /16/17 09:15 03/16/17 17: Toxaphene mg/kg /16/17 09:15 03/16/17 17: Surrogates Tetrachloro-m-xylene (S) 99 % /16/17 09:15 03/16/17 17: Decachlorobiphenyl (S) 95 % /16/17 09:15 03/16/17 17: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.96 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.45 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 10 of 35

32 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-14-24' Lab ID: Collected: 03/13/17 13:22 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 19: alpha-bhc mg/kg /16/17 09:15 03/16/17 19: beta-bhc mg/kg /16/17 09:15 03/16/17 19: delta-bhc mg/kg /16/17 09:15 03/16/17 19: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 19: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 19: ,4'-DDD mg/kg /16/17 09:15 03/16/17 19: ,4'-DDE mg/kg /16/17 09:15 03/16/17 19: ,4'-DDT mg/kg /16/17 09:15 03/16/17 19: Dieldrin mg/kg /16/17 09:15 03/16/17 19: Endosulfan I mg/kg /16/17 09:15 03/16/17 19: Endosulfan II mg/kg /16/17 09:15 03/16/17 19: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 19: Endrin mg/kg /16/17 09:15 03/16/17 19: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 19: Endrin ketone mg/kg /16/17 09:15 03/16/17 19: Heptachlor mg/kg /16/17 09:15 03/16/17 19: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 19: Methoxychlor mg/kg /16/17 09:15 03/16/17 19: Toxaphene mg/kg /16/17 09:15 03/16/17 19: Surrogates Tetrachloro-m-xylene (S) 85 % /16/17 09:15 03/16/17 19: Decachlorobiphenyl (S) 73 % /16/17 09:15 03/16/17 19: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 4.9 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 12.6 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 11 of 35

33 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-13-6' Lab ID: Collected: 03/13/17 13:25 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 19: alpha-bhc mg/kg /16/17 09:15 03/16/17 19: beta-bhc mg/kg /16/17 09:15 03/16/17 19: delta-bhc mg/kg /16/17 09:15 03/16/17 19: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 19: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 19: ,4'-DDD mg/kg /16/17 09:15 03/16/17 19: ,4'-DDE mg/kg /16/17 09:15 03/16/17 19: ,4'-DDT mg/kg /16/17 09:15 03/16/17 19: Dieldrin mg/kg /16/17 09:15 03/16/17 19: Endosulfan I mg/kg /16/17 09:15 03/16/17 19: Endosulfan II mg/kg /16/17 09:15 03/16/17 19: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 19: Endrin mg/kg /16/17 09:15 03/16/17 19: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 19: Endrin ketone mg/kg /16/17 09:15 03/16/17 19: Heptachlor mg/kg /16/17 09:15 03/16/17 19: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 19: Methoxychlor mg/kg /16/17 09:15 03/16/17 19: Toxaphene mg/kg /16/17 09:15 03/16/17 19: Surrogates Tetrachloro-m-xylene (S) 82 % /16/17 09:15 03/16/17 19: Decachlorobiphenyl (S) 78 % /16/17 09:15 03/16/17 19: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.7 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.7 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 12 of 35

34 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-13-24' Lab ID: Collected: 03/13/17 13:26 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 15: alpha-bhc mg/kg /16/17 09:15 03/16/17 15: beta-bhc mg/kg /16/17 09:15 03/16/17 15: delta-bhc mg/kg /16/17 09:15 03/16/17 15: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 15: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 15: ,4'-DDD mg/kg /16/17 09:15 03/16/17 15: ,4'-DDE mg/kg /16/17 09:15 03/16/17 15: ,4'-DDT mg/kg /16/17 09:15 03/16/17 15: Dieldrin mg/kg /16/17 09:15 03/16/17 15: Endosulfan I mg/kg /16/17 09:15 03/16/17 15: Endosulfan II mg/kg /16/17 09:15 03/16/17 15: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 15: Endrin mg/kg /16/17 09:15 03/16/17 15: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 15: Endrin ketone mg/kg /16/17 09:15 03/16/17 15: Heptachlor mg/kg /16/17 09:15 03/16/17 15: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 15: Methoxychlor mg/kg /16/17 09:15 03/16/17 15: Toxaphene mg/kg /16/17 09:15 03/16/17 15: Surrogates Tetrachloro-m-xylene (S) 82 % /16/17 09:15 03/16/17 15: Decachlorobiphenyl (S) 79 % /16/17 09:15 03/16/17 15: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 1.7 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.4 % /21/17 14:21 J(D6) Date: 03/22/ :47 AM without the written consent of. Page 13 of 35

35 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-11-6' Lab ID: Collected: 03/13/17 13:45 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 16: alpha-bhc mg/kg /16/17 09:15 03/16/17 16: beta-bhc mg/kg /16/17 09:15 03/16/17 16: delta-bhc mg/kg /16/17 09:15 03/16/17 16: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 16: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 16: ,4'-DDD mg/kg /16/17 09:15 03/16/17 16: ,4'-DDE mg/kg /16/17 09:15 03/16/17 16: ,4'-DDT mg/kg /16/17 09:15 03/16/17 16: Dieldrin mg/kg /16/17 09:15 03/16/17 16: Endosulfan I mg/kg /16/17 09:15 03/16/17 16: Endosulfan II mg/kg /16/17 09:15 03/16/17 16: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 16: Endrin mg/kg /16/17 09:15 03/16/17 16: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 16: Endrin ketone mg/kg /16/17 09:15 03/16/17 16: Heptachlor I mg/kg /16/17 09:15 03/16/17 16: Heptachlor epoxide I mg/kg /16/17 09:15 03/16/17 16: Methoxychlor mg/kg /16/17 09:15 03/16/17 16: Toxaphene mg/kg /16/17 09:15 03/16/17 16: Surrogates Tetrachloro-m-xylene (S) 84 % /16/17 09:15 03/16/17 16: Decachlorobiphenyl (S) 77 % /16/17 09:15 03/16/17 16: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 1.3 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.40 % /21/17 14:21 Date: 03/22/ :47 AM without the written consent of. Page 14 of 35

36 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-11-24' Lab ID: Collected: 03/13/17 13:46 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 20: alpha-bhc mg/kg /16/17 09:15 03/16/17 20: beta-bhc mg/kg /16/17 09:15 03/16/17 20: delta-bhc mg/kg /16/17 09:15 03/16/17 20: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 20: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 20: ,4'-DDD mg/kg /16/17 09:15 03/16/17 20: ,4'-DDE mg/kg /16/17 09:15 03/16/17 20: ,4'-DDT mg/kg /16/17 09:15 03/16/17 20: Dieldrin mg/kg /16/17 09:15 03/16/17 20: Endosulfan I mg/kg /16/17 09:15 03/16/17 20: Endosulfan II mg/kg /16/17 09:15 03/16/17 20: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 20: Endrin mg/kg /16/17 09:15 03/16/17 20: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 20: Endrin ketone mg/kg /16/17 09:15 03/16/17 20: Heptachlor mg/kg /16/17 09:15 03/16/17 20: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 20: Methoxychlor mg/kg /16/17 09:15 03/16/17 20: Toxaphene mg/kg /16/17 09:15 03/16/17 20: Surrogates Tetrachloro-m-xylene (S) 96 % /16/17 09:15 03/16/17 20: Decachlorobiphenyl (S) 85 % /16/17 09:15 03/16/17 20: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 9.0 mg/kg /21/17 05:05 03/21/17 15: Percent Moisture Analytical Method: ASTM D Percent Moisture 18.3 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 15 of 35

37 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-10-6' Lab ID: Collected: 03/13/17 13:49 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 17: alpha-bhc mg/kg /16/17 09:15 03/16/17 17: beta-bhc mg/kg /16/17 09:15 03/16/17 17: delta-bhc mg/kg /16/17 09:15 03/16/17 17: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 17: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 17: ,4'-DDD mg/kg /16/17 09:15 03/16/17 17: ,4'-DDE mg/kg /16/17 09:15 03/16/17 17: ,4'-DDT mg/kg /16/17 09:15 03/16/17 17: Dieldrin mg/kg /16/17 09:15 03/16/17 17: Endosulfan I mg/kg /16/17 09:15 03/16/17 17: Endosulfan II mg/kg /16/17 09:15 03/16/17 17: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 17: Endrin mg/kg /16/17 09:15 03/16/17 17: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 17: Endrin ketone mg/kg /16/17 09:15 03/16/17 17: Heptachlor I mg/kg /16/17 09:15 03/16/17 17: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 17: J(M1), J(R1) Methoxychlor mg/kg /16/17 09:15 03/16/17 17: Toxaphene mg/kg /16/17 09:15 03/16/17 17: Surrogates Tetrachloro-m-xylene (S) 85 % /16/17 09:15 03/16/17 17: Decachlorobiphenyl (S) 101 % /16/17 09:15 03/16/17 17: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.8 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.53 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 16 of 35

38 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-10-24' Lab ID: Collected: 03/13/17 13:50 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 15: alpha-bhc mg/kg /16/17 09:15 03/16/17 15: beta-bhc mg/kg /16/17 09:15 03/16/17 15: delta-bhc mg/kg /16/17 09:15 03/16/17 15: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 15: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 15: ,4'-DDD mg/kg /16/17 09:15 03/16/17 15: ,4'-DDE mg/kg /16/17 09:15 03/16/17 15: ,4'-DDT mg/kg /16/17 09:15 03/16/17 15: Dieldrin mg/kg /16/17 09:15 03/16/17 15: Endosulfan I mg/kg /16/17 09:15 03/16/17 15: Endosulfan II mg/kg /16/17 09:15 03/16/17 15: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 15: Endrin mg/kg /16/17 09:15 03/16/17 15: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 15: Endrin ketone mg/kg /16/17 09:15 03/16/17 15: Heptachlor mg/kg /16/17 09:15 03/16/17 15: Heptachlor epoxide I mg/kg /16/17 09:15 03/16/17 15: Methoxychlor mg/kg /16/17 09:15 03/16/17 15: Toxaphene mg/kg /16/17 09:15 03/16/17 15: Surrogates Tetrachloro-m-xylene (S) 80 % /16/17 09:15 03/16/17 15: Decachlorobiphenyl (S) 79 % /16/17 09:15 03/16/17 15: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.2 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 2.1 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 17 of 35

39 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-12-6' Lab ID: Collected: 03/13/17 14:05 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 20: alpha-bhc mg/kg /16/17 09:15 03/16/17 20: beta-bhc mg/kg /16/17 09:15 03/16/17 20: delta-bhc mg/kg /16/17 09:15 03/16/17 20: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 20: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 20: ,4'-DDD mg/kg /16/17 09:15 03/16/17 20: ,4'-DDE mg/kg /16/17 09:15 03/16/17 20: ,4'-DDT mg/kg /16/17 09:15 03/16/17 20: Dieldrin mg/kg /16/17 09:15 03/16/17 20: Endosulfan I mg/kg /16/17 09:15 03/16/17 20: Endosulfan II mg/kg /16/17 09:15 03/16/17 20: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 20: Endrin mg/kg /16/17 09:15 03/16/17 20: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 20: Endrin ketone mg/kg /16/17 09:15 03/16/17 20: Heptachlor mg/kg /16/17 09:15 03/16/17 20: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 20: Methoxychlor mg/kg /16/17 09:15 03/16/17 20: Toxaphene mg/kg /16/17 09:15 03/16/17 20: Surrogates Tetrachloro-m-xylene (S) 80 % /16/17 09:15 03/16/17 20: Decachlorobiphenyl (S) 69 % /16/17 09:15 03/16/17 20: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.27 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.53 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 18 of 35

40 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B Lab ID: Collected: 03/13/17 14:07 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 20: alpha-bhc mg/kg /16/17 09:15 03/16/17 20: beta-bhc mg/kg /16/17 09:15 03/16/17 20: delta-bhc mg/kg /16/17 09:15 03/16/17 20: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 20: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 20: ,4'-DDD mg/kg /16/17 09:15 03/16/17 20: ,4'-DDE mg/kg /16/17 09:15 03/16/17 20: ,4'-DDT mg/kg /16/17 09:15 03/16/17 20: Dieldrin mg/kg /16/17 09:15 03/16/17 20: Endosulfan I mg/kg /16/17 09:15 03/16/17 20: Endosulfan II mg/kg /16/17 09:15 03/16/17 20: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 20: Endrin mg/kg /16/17 09:15 03/16/17 20: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 20: Endrin ketone mg/kg /16/17 09:15 03/16/17 20: Heptachlor mg/kg /16/17 09:15 03/16/17 20: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 20: Methoxychlor mg/kg /16/17 09:15 03/16/17 20: Toxaphene mg/kg /16/17 09:15 03/16/17 20: Surrogates Tetrachloro-m-xylene (S) 79 % /16/17 09:15 03/16/17 20: Decachlorobiphenyl (S) 75 % /16/17 09:15 03/16/17 20: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 0.31 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 3.9 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 19 of 35

41 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-8-6 Lab ID: Collected: 03/13/17 14:25 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 14: alpha-bhc mg/kg /16/17 09:15 03/16/17 14: beta-bhc mg/kg /16/17 09:15 03/16/17 14: delta-bhc mg/kg /16/17 09:15 03/16/17 14: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 14: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 14: ,4'-DDD mg/kg /16/17 09:15 03/16/17 14: ,4'-DDE mg/kg /16/17 09:15 03/16/17 14: ,4'-DDT mg/kg /16/17 09:15 03/16/17 14: Dieldrin mg/kg /16/17 09:15 03/16/17 14: Endosulfan I mg/kg /16/17 09:15 03/16/17 14: Endosulfan II mg/kg /16/17 09:15 03/16/17 14: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 14: Endrin mg/kg /16/17 09:15 03/16/17 14: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 14: Endrin ketone mg/kg /16/17 09:15 03/16/17 14: Heptachlor mg/kg /16/17 09:15 03/16/17 14: Heptachlor epoxide I mg/kg /16/17 09:15 03/16/17 14: Methoxychlor mg/kg /16/17 09:15 03/16/17 14: Toxaphene mg/kg /16/17 09:15 03/16/17 14: Surrogates Tetrachloro-m-xylene (S) 84 % /16/17 09:15 03/16/17 14: Decachlorobiphenyl (S) 102 % /16/17 09:15 03/16/17 14: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 6.4 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.94 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 20 of 35

42 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-8-24 Lab ID: Collected: 03/13/17 14:26 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 15: alpha-bhc mg/kg /16/17 09:15 03/16/17 15: beta-bhc mg/kg /16/17 09:15 03/16/17 15: delta-bhc mg/kg /16/17 09:15 03/16/17 15: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 15: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 15: ,4'-DDD mg/kg /16/17 09:15 03/16/17 15: ,4'-DDE mg/kg /16/17 09:15 03/16/17 15: ,4'-DDT mg/kg /16/17 09:15 03/16/17 15: Dieldrin mg/kg /16/17 09:15 03/16/17 15: Endosulfan I mg/kg /16/17 09:15 03/16/17 15: Endosulfan II mg/kg /16/17 09:15 03/16/17 15: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 15: Endrin mg/kg /16/17 09:15 03/16/17 15: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 15: Endrin ketone I mg/kg /16/17 09:15 03/16/17 15: Heptachlor mg/kg /16/17 09:15 03/16/17 15: Heptachlor epoxide I mg/kg /16/17 09:15 03/16/17 15: Methoxychlor mg/kg /16/17 09:15 03/16/17 15: Toxaphene mg/kg /16/17 09:15 03/16/17 15: Surrogates Tetrachloro-m-xylene (S) 81 % /16/17 09:15 03/16/17 15: Decachlorobiphenyl (S) 80 % /16/17 09:15 03/16/17 15: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 3.4 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 1.4 % /21/17 14:22 Date: 03/22/ :47 AM without the written consent of. Page 21 of 35

43 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-9-6 Lab ID: Collected: 03/13/17 14:30 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 14: alpha-bhc mg/kg /16/17 09:15 03/16/17 14: beta-bhc mg/kg /16/17 09:15 03/16/17 14: delta-bhc mg/kg /16/17 09:15 03/16/17 14: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 14: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 14: ,4'-DDD mg/kg /16/17 09:15 03/16/17 14: ,4'-DDE mg/kg /16/17 09:15 03/16/17 14: ,4'-DDT mg/kg /16/17 09:15 03/16/17 14: Dieldrin mg/kg /16/17 09:15 03/16/17 14: Endosulfan I mg/kg /16/17 09:15 03/16/17 14: Endosulfan II mg/kg /16/17 09:15 03/16/17 14: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 14: Endrin mg/kg /16/17 09:15 03/16/17 14: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 14: Endrin ketone mg/kg /16/17 09:15 03/16/17 14: Heptachlor I mg/kg /16/17 09:15 03/16/17 14: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 14: Methoxychlor mg/kg /16/17 09:15 03/16/17 14: Toxaphene mg/kg /16/17 09:15 03/16/17 14: Surrogates Tetrachloro-m-xylene (S) 82 % /16/17 09:15 03/16/17 14: Decachlorobiphenyl (S) 107 % /16/17 09:15 03/16/17 14: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 2.0 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.50 % /21/17 14:22 J(D6) Date: 03/22/ :47 AM without the written consent of. Page 22 of 35

44 #=AR# ANALYTICAL RESLTS H / LOT 20,22, Sample: B-9-24 Lab ID: Collected: 03/13/17 14:32 Received: 03/15/17 03:20 Matrix: Solid s reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3546 Aldrin mg/kg /16/17 09:15 03/16/17 17: alpha-bhc mg/kg /16/17 09:15 03/16/17 17: beta-bhc mg/kg /16/17 09:15 03/16/17 17: delta-bhc mg/kg /16/17 09:15 03/16/17 17: gamma-bhc (Lindane) mg/kg /16/17 09:15 03/16/17 17: Chlordane (Technical) mg/kg /16/17 09:15 03/16/17 17: ,4'-DDD mg/kg /16/17 09:15 03/16/17 17: ,4'-DDE mg/kg /16/17 09:15 03/16/17 17: ,4'-DDT mg/kg /16/17 09:15 03/16/17 17: Dieldrin mg/kg /16/17 09:15 03/16/17 17: Endosulfan I mg/kg /16/17 09:15 03/16/17 17: Endosulfan II mg/kg /16/17 09:15 03/16/17 17: Endosulfan sulfate mg/kg /16/17 09:15 03/16/17 17: Endrin mg/kg /16/17 09:15 03/16/17 17: Endrin aldehyde mg/kg /16/17 09:15 03/16/17 17: Endrin ketone mg/kg /16/17 09:15 03/16/17 17: Heptachlor mg/kg /16/17 09:15 03/16/17 17: Heptachlor epoxide mg/kg /16/17 09:15 03/16/17 17: Methoxychlor mg/kg /16/17 09:15 03/16/17 17: Toxaphene mg/kg /16/17 09:15 03/16/17 17: Surrogates Tetrachloro-m-xylene (S) 85 % /16/17 09:15 03/16/17 17: Decachlorobiphenyl (S) 79 % /16/17 09:15 03/16/17 17: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic 1.4 mg/kg /21/17 05:05 03/21/17 16: Percent Moisture Analytical Method: ASTM D Percent Moisture 0.52 % /21/17 14:23 Date: 03/22/ :47 AM without the written consent of. Page 23 of 35

45 #=QC# QALITY CONTROL DATA H / LOT 20,22, QC Batch: QC Batch Method: EPA 3050 Analysis Method: Analysis Description: EPA MET Solid Associated Lab Samples: , , , , , , , , , , , , , , , , , METHOD BLANK: Matrix: Solid Associated Lab Samples: , , , , , , , , , , , , , , , , , nits Blank Reporting Limit MDL Analyzed Qualifiers Arsenic mg/kg /21/17 14:36 LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Arsenic mg/kg Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Arsenic mg/kg 2.8 I Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 24 of 35

46 #=QC# QALITY CONTROL DATA H / LOT 20,22, QC Batch: QC Batch Method: EPA 3546 Analysis Method: Analysis Description: EPA GCS Pesticides Associated Lab Samples: , , , , , , , , , , , , , , , , , METHOD BLANK: Matrix: Solid Associated Lab Samples: , , , , , , , , , , , , , , , , , nits Blank Reporting Limit MDL Analyzed Qualifiers 4,4'-DDD mg/kg /16/17 18:15 4,4'-DDE mg/kg /16/17 18:15 4,4'-DDT mg/kg /16/17 18:15 Aldrin mg/kg /16/17 18:15 alpha-bhc mg/kg /16/17 18:15 beta-bhc mg/kg /16/17 18:15 Chlordane (Technical) mg/kg /16/17 18:15 delta-bhc mg/kg /16/17 18:15 Dieldrin mg/kg /16/17 18:15 Endosulfan I mg/kg /16/17 18:15 Endosulfan II mg/kg /16/17 18:15 Endosulfan sulfate mg/kg /16/17 18:15 Endrin mg/kg /16/17 18:15 Endrin aldehyde mg/kg /16/17 18:15 Endrin ketone mg/kg /16/17 18:15 gamma-bhc (Lindane) mg/kg /16/17 18:15 Heptachlor mg/kg /16/17 18:15 Heptachlor epoxide mg/kg /16/17 18:15 Methoxychlor mg/kg /16/17 18:15 Toxaphene mg/kg /16/17 18:15 Decachlorobiphenyl (S) % /16/17 18:15 Tetrachloro-m-xylene (S) % /16/17 18:15 LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits 4,4'-DDD mg/kg ,4'-DDE mg/kg ,4'-DDT mg/kg Aldrin mg/kg alpha-bhc mg/kg beta-bhc mg/kg delta-bhc mg/kg Dieldrin mg/kg Endosulfan I mg/kg Endosulfan II mg/kg Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 25 of 35

47 #=QC# QALITY CONTROL DATA H / LOT 20,22, LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Endosulfan sulfate mg/kg Endrin mg/kg Endrin aldehyde mg/kg Endrin ketone mg/kg gamma-bhc (Lindane) mg/kg Heptachlor mg/kg Heptachlor epoxide mg/kg Methoxychlor mg/kg Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD 4,4'-DDD mg/kg ,4'-DDE mg/kg ,4'-DDT mg/kg Aldrin mg/kg alpha-bhc mg/kg beta-bhc mg/kg delta-bhc mg/kg Dieldrin mg/kg Endosulfan I mg/kg Endosulfan II mg/kg Endosulfan sulfate mg/kg Endrin mg/kg Endrin aldehyde mg/kg Endrin ketone mg/kg gamma-bhc (Lindane) mg/kg Heptachlor mg/kg I Heptachlor epoxide mg/kg J(M1), J(R1) Methoxychlor mg/kg Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 26 of 35

48 #=QC# QALITY CONTROL DATA H / LOT 20,22, MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 27 of 35

49 #=QC# QALITY CONTROL DATA H / LOT 20,22, QC Batch: QC Batch Method: ASTM D Analysis Method: Analysis Description: ASTM D Dry Weight/Percent Moisture Associated Lab Samples: , , , , , , , , , , , , , , , , , SAMPLE DPLICATE: nits Dup Percent Moisture % RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % J(D6) RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % J(D6) RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % J(D6) RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % RPD Max RPD Qualifiers SAMPLE DPLICATE: nits Dup Percent Moisture % RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 28 of 35

50 #=QC# QALITY CONTROL DATA H / LOT 20,22, SAMPLE DPLICATE: nits Dup Percent Moisture % RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :47 AM without the written consent of. Page 29 of 35

51 #=QL# QALIFIERS H / LOT 20,22, DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-p - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-O Pace Analytical Services - Ormond Beach ANALYTE QALIFIERS I J(D6) J(M1) J(R1) The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Compound was analyzed for but not detected. Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Estimated Value. RPD value was outside control limits. Date: 03/22/ :47 AM without the written consent of. Page 30 of 35

52 #=CR# QALITY CONTROL DATA CROSS REFERENCE TABLE H / LOT 20,22, Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch B-16-6' EPA EPA B-16-24' EPA EPA B-15-6' EPA EPA B-15-24' EPA EPA B-14-6' EPA EPA B-14-24' EPA EPA B-13-6' EPA EPA B-13-24' EPA EPA B-11-6' EPA EPA B-11-24' EPA EPA B-10-6' EPA EPA B-10-24' EPA EPA B-12-6' EPA EPA B EPA EPA B-8-6 EPA EPA B-8-24 EPA EPA B-9-6 EPA EPA B-9-24 EPA EPA B-16-6' EPA EPA B-16-24' EPA EPA B-15-6' EPA EPA B-15-24' EPA EPA B-14-6' EPA EPA B-14-24' EPA EPA B-13-6' EPA EPA B-13-24' EPA EPA B-11-6' EPA EPA B-11-24' EPA EPA B-10-6' EPA EPA B-10-24' EPA EPA B-12-6' EPA EPA B EPA EPA B-8-6 EPA EPA B-8-24 EPA EPA B-9-6 EPA EPA B-9-24 EPA EPA B-16-6' ASTM D B-16-24' ASTM D B-15-6' ASTM D B-15-24' ASTM D B-14-6' ASTM D B-14-24' ASTM D B-13-6' ASTM D B-13-24' ASTM D B-11-6' ASTM D B-11-24' ASTM D B-10-6' ASTM D B-10-24' ASTM D Date: 03/22/ :47 AM without the written consent of. Page 31 of 35

53 #=CR# QALITY CONTROL DATA CROSS REFERENCE TABLE H / LOT 20,22, Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch B-12-6' ASTM D B ASTM D B-8-6 ASTM D B-8-24 ASTM D B-9-6 ASTM D B-9-24 ASTM D Date: 03/22/ :47 AM without the written consent of. Page 32 of 35

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57 #=CL# LIMS SE: FR - IGOR KARIMOV LIMS OBJECT ID: March 22, 2017 Igor Karimov Terracon Consulting Engineers 1675 Lee Road Winter Park, FL RE: Dear Igor Karimov: Enclosed are the analytical results for sample(s) received by the laboratory on March 14, The results relate only to the samples included in this report. s reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Sakina Mckenzie sakina.mckenzie@pacelabs.com Project Manager Enclosures without the written consent of. Page 1 of 69

58 #=CP# CERTIFICATIONS Ormond Beach Certification IDs, Alabama Certification #: Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: Maryland Certification: #346 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS Nevada Certification: FL NELAC Reciprocity New York Certification #: North Carolina Environmental Certificate #: 667 North Carolina Certification #: Oklahoma Certification #: D9947 Pennsylvania Certification #: Puerto Rico Certification #: FL01264 South Carolina Certification: # Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity S Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: Wyoming Certification: FL NELAC Reciprocity West Virginia Certification #: 9962C Wisconsin Certification #: Wyoming (EPA Region 8): FL NELAC Reciprocity without the written consent of. Page 2 of 69

59 #=SS# SAMPLE SMMARY Lab ID Sample ID Matrix Date Collected Date Received TMW-1 Water 03/10/17 17:10 03/14/17 03: TMW-2 Water 03/10/17 15:21 03/14/17 03: TMW-3 Water 03/10/17 13:59 03/14/17 03: TMW-4 Water 03/10/17 12:36 03/14/17 03: TMW-5 Water 03/10/17 11:37 03/14/17 03: SW-1 Water 03/10/17 16:10 03/14/17 03:20 without the written consent of. Page 3 of 69

60 #=SA# SAMPLE ANALYTE CONT Lab ID Sample ID Method Analysts Analytes Reported Laboratory TMW-1 EPA 8081 JLG 22 PASI-O FL-PRO BP1 3 PASI-O EPA 6010 RVK 1 PASI-O EPA 6010 BTS 1 PASI-O EPA 8270 by SIM JDT 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O TMW-2 EPA 8081 JLG 22 PASI-O FL-PRO JGW 3 PASI-O EPA 6010 RVK 1 PASI-O EPA 6010 RVK 1 PASI-O EPA 8270 by SIM TWB 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O TMW-3 EPA 8081 JLG 22 PASI-O FL-PRO BP1 3 PASI-O EPA 6010 RVK 1 PASI-O EPA 6010 RVK 1 PASI-O EPA 8270 by SIM TWB 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O TMW-4 EPA 8081 JLG 22 PASI-O FL-PRO JGW 3 PASI-O EPA 6010 RVK 1 PASI-O EPA 6010 RVK 1 PASI-O EPA 8270 by SIM TWB 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O TMW-5 EPA 8081 JLG 22 PASI-O FL-PRO JGW 3 PASI-O EPA 6010 BTS 1 PASI-O EPA 6010 RVK 1 PASI-O EPA 8270 by SIM TWB 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O SW-1 EPA 8081 JLG 22 PASI-O FL-PRO JGW 3 PASI-O without the written consent of. Page 4 of 69

61 #=SA# SAMPLE ANALYTE CONT Lab ID Sample ID Method Analysts Analytes Reported Laboratory EPA 6010 RVK 1 PASI-O EPA 6010 RVK 1 PASI-O EPA 8270 by SIM TWB 20 PASI-O EPA 8270 TWB 82 PASI-O EPA 8260 SK1 57 PASI-O without the written consent of. Page 5 of 69

62 #=AR# ANALYTICAL RESLTS Sample: TMW-1 Lab ID: Collected: 03/10/17 17:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ug/l /16/17 12:00 03/17/17 08: alpha-bhc ug/l /16/17 12:00 03/17/17 08: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 08: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 08: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 08: J(L2) Chlordane (Technical) 0.18 ug/l /16/17 12:00 03/17/17 08: ,4'-DDD ug/l /16/17 12:00 03/17/17 08: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 08: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 08: J(L2) Dieldrin ug/l /16/17 12:00 03/17/17 08: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 08: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 08: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 08: J(L2) Endrin ug/l /16/17 12:00 03/17/17 08: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 08: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 08: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 08: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 08: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 08: Toxaphene 0.25 ug/l /16/17 12:00 03/17/17 08: Surrogates Tetrachloro-m-xylene (S) 7 % /16/17 12:00 03/17/17 08: S7 Decachlorobiphenyl (S) 9 % /16/17 12:00 03/17/17 08: S7 FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 1.4 mg/l /16/17 08:00 03/16/17 17:33 Surrogates o-terphenyl (S) 81 % /16/17 08:00 03/16/17 17: J(S5) N-Pentatriacontane (S) 75 % /16/17 08:00 03/16/17 17: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 500 ug/l /16/17 18:37 03/17/17 21: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 1000 ug/l /16/17 19:54 03/20/17 14: M MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene 0.30 I ug/l /17/17 23:55 03/19/17 20: p Acenaphthylene ug/l /17/17 23:55 03/19/17 20: p Anthracene 0.11 I ug/l /17/17 23:55 03/19/17 20: p Benzo(a)anthracene ug/l /17/17 23:55 03/19/17 20: p Benzo(a)pyrene ug/l /17/17 23:55 03/19/17 20: p Benzo(b)fluoranthene ug/l /17/17 23:55 03/19/17 20: p Benzo(g,h,i)perylene ug/l /17/17 23:55 03/19/17 20: p Benzo(k)fluoranthene ug/l /17/17 23:55 03/19/17 20: p Chrysene ug/l /17/17 23:55 03/19/17 20: p Date: 03/22/ :42 PM without the written consent of. Page 6 of 69

63 #=AR# ANALYTICAL RESLTS Sample: TMW-1 Lab ID: Collected: 03/10/17 17:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /17/17 23:55 03/19/17 20: p Fluoranthene 0.23 I ug/l /17/17 23:55 03/19/17 20: p Fluorene 0.24 I ug/l /17/17 23:55 03/19/17 20: p Indeno(1,2,3-cd)pyrene ug/l /17/17 23:55 03/19/17 20: p 1-Methylnaphthalene 1.0 ug/l /17/17 23:55 03/19/17 20: p 2-Methylnaphthalene 1.0 ug/l /17/17 23:55 03/19/17 20: p Naphthalene 1.0 ug/l /17/17 23:55 03/19/17 20: p Phenanthrene 1.0 ug/l /17/17 23:55 03/19/17 20: p Pyrene 0.10 I ug/l /17/17 23:55 03/19/17 20: p Surrogates 2-Fluorobiphenyl (S) 43 % /17/17 23:55 03/19/17 20: Terphenyl-d14 (S) 109 % /17/17 23:55 03/19/17 20: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.82 ug/l /15/17 16:32 03/18/17 09: Acenaphthylene 0.90 ug/l /15/17 16:32 03/18/17 09: Aniline 1.9 ug/l /15/17 16:32 03/18/17 09: Anthracene 0.57 ug/l /15/17 16:32 03/18/17 09: Benzidine 0.73 ug/l /15/17 16:32 03/18/17 09: Benzo(a)anthracene 0.60 ug/l /15/17 16:32 03/18/17 09: Benzo(a)pyrene 0.55 ug/l /15/17 16:32 03/18/17 09: Benzo(b)fluoranthene 0.59 ug/l /15/17 16:32 03/18/17 09: Benzo(g,h,i)perylene 0.65 ug/l /15/17 16:32 03/18/17 09: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 09: J(L1) Benzyl alcohol 0.60 ug/l /15/17 16:32 03/18/17 09: Bromophenylphenyl ether 0.64 ug/l /15/17 16:32 03/18/17 09: Butylbenzylphthalate 0.68 ug/l /15/17 16:32 03/18/17 09: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 09: J(L1), N2 Carbazole 0.45 ug/l /15/17 16:32 03/18/17 09: Chloro-3-methylphenol 0.59 ug/l /15/17 16:32 03/18/17 09: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethyl) ether 0.71 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroisopropyl) ether 0.69 ug/l /15/17 16:32 03/18/17 09: Chloronaphthalene 0.76 ug/l /15/17 16:32 03/18/17 09: Chlorophenol 0.65 ug/l /15/17 16:32 03/18/17 09: Chlorophenylphenyl ether 0.60 ug/l /15/17 16:32 03/18/17 09: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 09: Dibenz(a,h)anthracene 0.62 ug/l /15/17 16:32 03/18/17 09: Dibenzofuran 0.64 ug/l /15/17 16:32 03/18/17 09: ,2-Dichlorobenzene 0.65 ug/l /15/17 16:32 03/18/17 09: ,3-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorobenzene 0.73 ug/l /15/17 16:32 03/18/17 09: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorophenol 0.53 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 7 of 69

64 #=AR# ANALYTICAL RESLTS Sample: TMW-1 Lab ID: Collected: 03/10/17 17:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 09: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 09: Dimethylphthalate 0.61 ug/l /15/17 16:32 03/18/17 09: Di-n-butylphthalate 0.43 I ug/l /15/17 16:32 03/18/17 09: ,6-Dinitro-2-methylphenol 1.3 ug/l /15/17 16:32 03/18/17 09: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 09: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 09: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 09: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 09: ,6-Dinitrotoluene 1.2 ug/l /15/17 16:32 03/18/17 09: Di-n-octylphthalate 2.2 I ug/l /15/17 16:32 03/18/17 09: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 09: bis(2-ethylhexyl)phthalate 2.2 I ug/l /15/17 16:32 03/18/17 09: Fluoranthene 0.55 I ug/l /15/17 16:32 03/18/17 09: Fluorene 0.53 ug/l /15/17 16:32 03/18/17 09: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 09: Hexachlorobenzene 0.76 ug/l /15/17 16:32 03/18/17 09: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 09: C Hexachloroethane 0.67 ug/l /15/17 16:32 03/18/17 09: Indeno(1,2,3-cd)pyrene 0.69 ug/l /15/17 16:32 03/18/17 09: Isophorone 0.69 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.95 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 09: Methylphenol(o-Cresol) 0.69 ug/l /15/17 16:32 03/18/17 09: &4-Methylphenol(m&p Cresol) 0.63 ug/l /15/17 16:32 03/18/17 09:07 Naphthalene 0.74 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.57 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.94 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 09: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 0.77 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodimethylamine 0.92 ug/l /15/17 16:32 03/18/17 09: N-Nitroso-di-n-propylamine 0.89 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 09: Pentachlorophenol 0.63 ug/l /15/17 16:32 03/18/17 09: C Phenanthrene 1.9 I ug/l /15/17 16:32 03/18/17 09: Phenol 0.51 ug/l /15/17 16:32 03/18/17 09: Pyrene 0.65 ug/l /15/17 16:32 03/18/17 09: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 09: ,3,4,6-Tetrachlorophenol 3.7 ug/l /15/17 16:32 03/18/17 09: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: N2 1,2,4-Trichlorobenzene 0.79 ug/l /15/17 16:32 03/18/17 09: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 8 of 69

65 #=AR# ANALYTICAL RESLTS Sample: TMW-1 Lab ID: Collected: 03/10/17 17:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 23 % /15/17 16:32 03/18/17 09: Fluorobiphenyl (S) 25 % /15/17 16:32 03/18/17 09: Terphenyl-d14 (S) 33 % /15/17 16:32 03/18/17 09: Phenol-d6 (S) 10 % /15/17 16:32 03/18/17 09: Fluorophenol (S) 11 % /15/17 16:32 03/18/17 09: ,4,6-Tribromophenol (S) 31 % /15/17 16:32 03/18/17 09: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 07: Acetonitrile 5.0 ug/l /15/17 07: Benzene 0.10 ug/l /15/17 07: Bromochloromethane 0.50 ug/l /15/17 07: Bromodichloromethane 0.27 ug/l /15/17 07: Bromoform 0.50 ug/l /15/17 07: Bromomethane 0.50 ug/l /15/17 07: Butanone (MEK) 5.0 ug/l /15/17 07: Carbon disulfide 5.0 ug/l /15/17 07: Carbon tetrachloride 0.50 ug/l /15/17 07: Chlorobenzene 0.50 ug/l /15/17 07: Chloroethane 0.50 ug/l /15/17 07: Chloroform 0.50 ug/l /15/17 07: Chloromethane 0.62 ug/l /15/17 07: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 07: Dibromochloromethane 0.26 ug/l /15/17 07: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 07: Dibromomethane 0.50 ug/l /15/17 07: ,2-Dichlorobenzene 0.50 ug/l /15/17 07: ,4-Dichlorobenzene 0.50 ug/l /15/17 07: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 07: ,1-Dichloroethane 0.50 ug/l /15/17 07: ,2-Dichloroethane 0.50 ug/l /15/17 07: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 07: N2 1,1-Dichloroethene 0.50 ug/l /15/17 07: cis-1,2-dichloroethene 0.50 ug/l /15/17 07: trans-1,2-dichloroethene 0.50 ug/l /15/17 07: ,2-Dichloropropane 0.50 ug/l /15/17 07: cis-1,3-dichloropropene 0.25 ug/l /15/17 07: trans-1,3-dichloropropene 0.25 ug/l /15/17 07: Ethylbenzene 0.50 ug/l /15/17 07: Hexanone 5.0 ug/l /15/17 07: Iodomethane 0.50 ug/l /15/17 07: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 07: Methylene Chloride 2.5 ug/l /15/17 07: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 07: Methyl-tert-butyl ether 0.50 ug/l /15/17 07: Date: 03/22/ :42 PM without the written consent of. Page 9 of 69

66 #=AR# ANALYTICAL RESLTS Sample: TMW-1 Lab ID: Collected: 03/10/17 17:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 07: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 07: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 07: Tetrachloroethene 0.50 ug/l /15/17 07: Toluene 0.50 ug/l /15/17 07: ,1,1-Trichloroethane 0.50 ug/l /15/17 07: ,1,2-Trichloroethane 0.50 ug/l /15/17 07: Trichloroethene 0.50 ug/l /15/17 07: Trichlorofluoromethane 0.50 ug/l /15/17 07: ,2,3-Trichloropropane 0.59 ug/l /15/17 07: ,2,4-Trimethylbenzene 0.53 I ug/l /15/17 07: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 07: Vinyl acetate 1.0 ug/l /15/17 07: Vinyl chloride 0.50 ug/l /15/17 07: Xylene (Total) 1.5 ug/l /15/17 07: m&p-xylene 1.0 ug/l /15/17 07: o-xylene 0.50 ug/l /15/17 07: Surrogates 4-Bromofluorobenzene (S) 97 % /15/17 07: ,2-Dichloroethane-d4 (S) 99 % /15/17 07: Toluene-d8 (S) 94 % /15/17 07: Date: 03/22/ :42 PM without the written consent of. Page 10 of 69

67 #=AR# ANALYTICAL RESLTS Sample: TMW-2 Lab ID: Collected: 03/10/17 15:21 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ug/l /16/17 12:00 03/17/17 09: alpha-bhc ug/l /16/17 12:00 03/17/17 09: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 09: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 09: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 09: J(L2) Chlordane (Technical) 0.17 ug/l /16/17 12:00 03/17/17 09: ,4'-DDD ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 09: J(L2) Dieldrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 09: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 09: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 09: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 09: Toxaphene 0.24 ug/l /16/17 12:00 03/17/17 09: Surrogates Tetrachloro-m-xylene (S) 10 % /16/17 12:00 03/17/17 09: S7 Decachlorobiphenyl (S) 9 % /16/17 12:00 03/17/17 09: S7 FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 0.80 mg/l /16/17 08:00 03/17/17 00:36 Surrogates o-terphenyl (S) 97 % /16/17 08:00 03/17/17 00: N-Pentatriacontane (S) 77 % /16/17 08:00 03/17/17 00: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 50.0 ug/l /16/17 18:37 03/17/17 21: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 5.0 ug/l /16/17 19:54 03/20/17 15: MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ug/l /16/17 15:32 03/17/17 08: Acenaphthylene ug/l /16/17 15:32 03/17/17 08: Anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)pyrene ug/l /16/17 15:32 03/17/17 08: Benzo(b)fluoranthene ug/l /16/17 15:32 03/17/17 08: C Benzo(g,h,i)perylene ug/l /16/17 15:32 03/17/17 08: Benzo(k)fluoranthene ug/l /16/17 15:32 03/17/17 08: Chrysene ug/l /16/17 15:32 03/17/17 08: Date: 03/22/ :42 PM without the written consent of. Page 11 of 69

68 #=AR# ANALYTICAL RESLTS Sample: TMW-2 Lab ID: Collected: 03/10/17 15:21 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /16/17 15:32 03/17/17 08: Fluoranthene ug/l /16/17 15:32 03/17/17 08: Fluorene ug/l /16/17 15:32 03/17/17 08: Indeno(1,2,3-cd)pyrene ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Naphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Phenanthrene ug/l /16/17 15:32 03/17/17 08: Pyrene ug/l /16/17 15:32 03/17/17 08: Surrogates 2-Fluorobiphenyl (S) 50 % /16/17 15:32 03/17/17 08: Terphenyl-d14 (S) 48 % /16/17 15:32 03/17/17 08: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.80 ug/l /15/17 16:32 03/18/17 09: Acenaphthylene 0.89 ug/l /15/17 16:32 03/18/17 09: Aniline 1.9 ug/l /15/17 16:32 03/18/17 09: Anthracene 0.56 ug/l /15/17 16:32 03/18/17 09: Benzidine 0.72 ug/l /15/17 16:32 03/18/17 09: Benzo(a)anthracene 0.59 ug/l /15/17 16:32 03/18/17 09: Benzo(a)pyrene 0.54 ug/l /15/17 16:32 03/18/17 09: Benzo(b)fluoranthene 0.58 ug/l /15/17 16:32 03/18/17 09: Benzo(g,h,i)perylene 0.64 ug/l /15/17 16:32 03/18/17 09: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 09: J(L1) Benzyl alcohol 0.59 ug/l /15/17 16:32 03/18/17 09: Bromophenylphenyl ether 0.63 ug/l /15/17 16:32 03/18/17 09: Butylbenzylphthalate 0.67 ug/l /15/17 16:32 03/18/17 09: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 09: J(L1), N2 Carbazole 0.44 ug/l /15/17 16:32 03/18/17 09: Chloro-3-methylphenol 0.58 ug/l /15/17 16:32 03/18/17 09: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethyl) ether 0.70 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroisopropyl) ether 0.68 ug/l /15/17 16:32 03/18/17 09: Chloronaphthalene 0.75 ug/l /15/17 16:32 03/18/17 09: Chlorophenol 0.64 ug/l /15/17 16:32 03/18/17 09: Chlorophenylphenyl ether 0.59 ug/l /15/17 16:32 03/18/17 09: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 09: Dibenz(a,h)anthracene 0.61 ug/l /15/17 16:32 03/18/17 09: Dibenzofuran 0.63 ug/l /15/17 16:32 03/18/17 09: ,2-Dichlorobenzene 0.64 ug/l /15/17 16:32 03/18/17 09: ,3-Dichlorobenzene 0.71 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 09: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorophenol 0.52 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 12 of 69

69 #=AR# ANALYTICAL RESLTS Sample: TMW-2 Lab ID: Collected: 03/10/17 15:21 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 09: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 09: Dimethylphthalate 0.60 ug/l /15/17 16:32 03/18/17 09: Di-n-butylphthalate 0.38 ug/l /15/17 16:32 03/18/17 09: ,6-Dinitro-2-methylphenol 1.2 ug/l /15/17 16:32 03/18/17 09: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 09: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 09: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 09: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 09: ,6-Dinitrotoluene 1.1 ug/l /15/17 16:32 03/18/17 09: Di-n-octylphthalate 0.84 ug/l /15/17 16:32 03/18/17 09: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 09: bis(2-ethylhexyl)phthalate 1.7 I ug/l /15/17 16:32 03/18/17 09: Fluoranthene 0.51 ug/l /15/17 16:32 03/18/17 09: Fluorene 0.52 ug/l /15/17 16:32 03/18/17 09: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 09: Hexachlorobenzene 0.75 ug/l /15/17 16:32 03/18/17 09: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 09: C Hexachloroethane 0.66 ug/l /15/17 16:32 03/18/17 09: Indeno(1,2,3-cd)pyrene 0.68 ug/l /15/17 16:32 03/18/17 09: Isophorone 0.68 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.93 ug/l /15/17 16:32 03/18/17 09: Methylphenol(o-Cresol) 0.68 ug/l /15/17 16:32 03/18/17 09: &4-Methylphenol(m&p Cresol) 0.62 ug/l /15/17 16:32 03/18/17 09:29 Naphthalene 0.73 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.56 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.93 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 09: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 0.76 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodimethylamine 0.91 ug/l /15/17 16:32 03/18/17 09: N-Nitroso-di-n-propylamine 0.88 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 09: Pentachlorophenol 0.62 ug/l /15/17 16:32 03/18/17 09: C Phenanthrene 0.49 ug/l /15/17 16:32 03/18/17 09: Phenol 0.51 ug/l /15/17 16:32 03/18/17 09: Pyrene 0.64 ug/l /15/17 16:32 03/18/17 09: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 09: ,3,4,6-Tetrachlorophenol 3.6 ug/l /15/17 16:32 03/18/17 09: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: N2 1,2,4-Trichlorobenzene 0.78 ug/l /15/17 16:32 03/18/17 09: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 13 of 69

70 #=AR# ANALYTICAL RESLTS Sample: TMW-2 Lab ID: Collected: 03/10/17 15:21 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 49 % /15/17 16:32 03/18/17 09: Fluorobiphenyl (S) 54 % /15/17 16:32 03/18/17 09: Terphenyl-d14 (S) 74 % /15/17 16:32 03/18/17 09: Phenol-d6 (S) 17 % /15/17 16:32 03/18/17 09: Fluorophenol (S) 22 % /15/17 16:32 03/18/17 09: ,4,6-Tribromophenol (S) 87 % /15/17 16:32 03/18/17 09: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 07: Acetonitrile 5.0 ug/l /15/17 07: Benzene 0.10 ug/l /15/17 07: Bromochloromethane 0.50 ug/l /15/17 07: Bromodichloromethane 0.27 ug/l /15/17 07: Bromoform 0.50 ug/l /15/17 07: Bromomethane 0.50 ug/l /15/17 07: Butanone (MEK) 5.0 ug/l /15/17 07: Carbon disulfide 5.0 ug/l /15/17 07: Carbon tetrachloride 0.50 ug/l /15/17 07: Chlorobenzene 0.50 ug/l /15/17 07: Chloroethane 0.50 ug/l /15/17 07: Chloroform 0.50 ug/l /15/17 07: Chloromethane 0.62 ug/l /15/17 07: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 07: Dibromochloromethane 0.26 ug/l /15/17 07: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 07: Dibromomethane 0.50 ug/l /15/17 07: ,2-Dichlorobenzene 0.50 ug/l /15/17 07: ,4-Dichlorobenzene 0.50 ug/l /15/17 07: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 07: ,1-Dichloroethane 0.50 ug/l /15/17 07: ,2-Dichloroethane 0.50 ug/l /15/17 07: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 07: N2 1,1-Dichloroethene 0.50 ug/l /15/17 07: cis-1,2-dichloroethene 0.50 ug/l /15/17 07: trans-1,2-dichloroethene 0.50 ug/l /15/17 07: ,2-Dichloropropane 0.50 ug/l /15/17 07: cis-1,3-dichloropropene 0.25 ug/l /15/17 07: trans-1,3-dichloropropene 0.25 ug/l /15/17 07: Ethylbenzene 0.50 ug/l /15/17 07: Hexanone 5.0 ug/l /15/17 07: Iodomethane 0.50 ug/l /15/17 07: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 07: Methylene Chloride 2.5 ug/l /15/17 07: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 07: Methyl-tert-butyl ether 0.50 ug/l /15/17 07: Date: 03/22/ :42 PM without the written consent of. Page 14 of 69

71 #=AR# ANALYTICAL RESLTS Sample: TMW-2 Lab ID: Collected: 03/10/17 15:21 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 07: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 07: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 07: Tetrachloroethene 0.50 ug/l /15/17 07: Toluene 0.50 ug/l /15/17 07: ,1,1-Trichloroethane 0.50 ug/l /15/17 07: ,1,2-Trichloroethane 0.50 ug/l /15/17 07: Trichloroethene 0.50 ug/l /15/17 07: Trichlorofluoromethane 0.50 ug/l /15/17 07: ,2,3-Trichloropropane 0.59 ug/l /15/17 07: ,2,4-Trimethylbenzene 0.50 ug/l /15/17 07: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 07: Vinyl acetate 1.0 ug/l /15/17 07: Vinyl chloride 0.50 ug/l /15/17 07: Xylene (Total) 1.5 ug/l /15/17 07: m&p-xylene 1.0 ug/l /15/17 07: o-xylene 0.50 ug/l /15/17 07: Surrogates 4-Bromofluorobenzene (S) 96 % /15/17 07: ,2-Dichloroethane-d4 (S) 102 % /15/17 07: Toluene-d8 (S) 96 % /15/17 07: Date: 03/22/ :42 PM without the written consent of. Page 15 of 69

72 #=AR# ANALYTICAL RESLTS Sample: TMW-3 Lab ID: Collected: 03/10/17 13:59 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ug/l /16/17 12:00 03/17/17 09: alpha-bhc ug/l /16/17 12:00 03/17/17 09: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 09: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 09: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 09: J(L2) Chlordane (Technical) 0.17 ug/l /16/17 12:00 03/17/17 09: ,4'-DDD ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 09: J(L2) Dieldrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 09: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 09: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 09: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 09: Toxaphene 0.24 ug/l /16/17 12:00 03/17/17 09: Surrogates Tetrachloro-m-xylene (S) 47 % /16/17 12:00 03/17/17 09: Decachlorobiphenyl (S) 23 % /16/17 12:00 03/17/17 09: FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 0.80 mg/l /16/17 08:00 03/16/17 18:04 Surrogates o-terphenyl (S) 87 % /16/17 08:00 03/16/17 18: N-Pentatriacontane (S) 93 % /16/17 08:00 03/16/17 18: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 12.4 ug/l /16/17 18:37 03/17/17 22: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 5.0 ug/l /16/17 19:54 03/20/17 15: MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ug/l /16/17 15:32 03/17/17 08: Acenaphthylene ug/l /16/17 15:32 03/17/17 08: Anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)pyrene ug/l /16/17 15:32 03/17/17 08: Benzo(b)fluoranthene ug/l /16/17 15:32 03/17/17 08: C Benzo(g,h,i)perylene ug/l /16/17 15:32 03/17/17 08: Benzo(k)fluoranthene ug/l /16/17 15:32 03/17/17 08: Chrysene ug/l /16/17 15:32 03/17/17 08: Date: 03/22/ :42 PM without the written consent of. Page 16 of 69

73 #=AR# ANALYTICAL RESLTS Sample: TMW-3 Lab ID: Collected: 03/10/17 13:59 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /16/17 15:32 03/17/17 08: Fluoranthene ug/l /16/17 15:32 03/17/17 08: Fluorene ug/l /16/17 15:32 03/17/17 08: Indeno(1,2,3-cd)pyrene ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Naphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Phenanthrene ug/l /16/17 15:32 03/17/17 08: Pyrene ug/l /16/17 15:32 03/17/17 08: Surrogates 2-Fluorobiphenyl (S) 58 % /16/17 15:32 03/17/17 08: Terphenyl-d14 (S) 54 % /16/17 15:32 03/17/17 08: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.81 ug/l /15/17 16:32 03/18/17 09: Acenaphthylene 0.90 ug/l /15/17 16:32 03/18/17 09: Aniline 1.9 ug/l /15/17 16:32 03/18/17 09: Anthracene 0.57 ug/l /15/17 16:32 03/18/17 09: Benzidine 0.73 ug/l /15/17 16:32 03/18/17 09: Benzo(a)anthracene 0.60 ug/l /15/17 16:32 03/18/17 09: Benzo(a)pyrene 0.55 ug/l /15/17 16:32 03/18/17 09: Benzo(b)fluoranthene 0.59 ug/l /15/17 16:32 03/18/17 09: Benzo(g,h,i)perylene 0.64 ug/l /15/17 16:32 03/18/17 09: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 09: J(L1) Benzyl alcohol 0.60 ug/l /15/17 16:32 03/18/17 09: Bromophenylphenyl ether 0.63 ug/l /15/17 16:32 03/18/17 09: Butylbenzylphthalate 0.68 ug/l /15/17 16:32 03/18/17 09: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 09: J(L1), N2 Carbazole 0.44 ug/l /15/17 16:32 03/18/17 09: Chloro-3-methylphenol 0.59 ug/l /15/17 16:32 03/18/17 09: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroethyl) ether 0.71 ug/l /15/17 16:32 03/18/17 09: bis(2-chloroisopropyl) ether 0.69 ug/l /15/17 16:32 03/18/17 09: Chloronaphthalene 0.76 ug/l /15/17 16:32 03/18/17 09: Chlorophenol 0.64 ug/l /15/17 16:32 03/18/17 09: Chlorophenylphenyl ether 0.60 ug/l /15/17 16:32 03/18/17 09: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 09: Dibenz(a,h)anthracene 0.61 ug/l /15/17 16:32 03/18/17 09: Dibenzofuran 0.63 ug/l /15/17 16:32 03/18/17 09: ,2-Dichlorobenzene 0.64 ug/l /15/17 16:32 03/18/17 09: ,3-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorobenzene 0.73 ug/l /15/17 16:32 03/18/17 09: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 09: ,4-Dichlorophenol 0.53 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 17 of 69

74 #=AR# ANALYTICAL RESLTS Sample: TMW-3 Lab ID: Collected: 03/10/17 13:59 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 09: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 09: Dimethylphthalate 0.60 ug/l /15/17 16:32 03/18/17 09: Di-n-butylphthalate 0.39 ug/l /15/17 16:32 03/18/17 09: ,6-Dinitro-2-methylphenol 1.2 ug/l /15/17 16:32 03/18/17 09: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 09: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 09: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 09: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 09: ,6-Dinitrotoluene 1.2 ug/l /15/17 16:32 03/18/17 09: Di-n-octylphthalate 0.85 ug/l /15/17 16:32 03/18/17 09: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 09: bis(2-ethylhexyl)phthalate 1.8 I ug/l /15/17 16:32 03/18/17 09: Fluoranthene 0.51 ug/l /15/17 16:32 03/18/17 09: Fluorene 0.53 ug/l /15/17 16:32 03/18/17 09: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 09: Hexachlorobenzene 0.76 ug/l /15/17 16:32 03/18/17 09: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 09: C Hexachloroethane 0.67 ug/l /15/17 16:32 03/18/17 09: Indeno(1,2,3-cd)pyrene 0.69 ug/l /15/17 16:32 03/18/17 09: Isophorone 0.69 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 09: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 09: Methylphenol(o-Cresol) 0.69 ug/l /15/17 16:32 03/18/17 09: &4-Methylphenol(m&p Cresol) 0.62 ug/l /15/17 16:32 03/18/17 09:51 Naphthalene 0.74 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.57 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.94 ug/l /15/17 16:32 03/18/17 09: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 09: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 0.77 ug/l /15/17 16:32 03/18/17 09: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodimethylamine 0.92 ug/l /15/17 16:32 03/18/17 09: N-Nitroso-di-n-propylamine 0.89 ug/l /15/17 16:32 03/18/17 09: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 09: Pentachlorophenol 0.62 ug/l /15/17 16:32 03/18/17 09: C Phenanthrene 0.49 ug/l /15/17 16:32 03/18/17 09: Phenol 0.51 ug/l /15/17 16:32 03/18/17 09: Pyrene 0.64 ug/l /15/17 16:32 03/18/17 09: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 09: ,3,4,6-Tetrachlorophenol 3.6 ug/l /15/17 16:32 03/18/17 09: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: N2 1,2,4-Trichlorobenzene 0.78 ug/l /15/17 16:32 03/18/17 09: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 09: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 09: Date: 03/22/ :42 PM without the written consent of. Page 18 of 69

75 #=AR# ANALYTICAL RESLTS Sample: TMW-3 Lab ID: Collected: 03/10/17 13:59 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 44 % /15/17 16:32 03/18/17 09: Fluorobiphenyl (S) 47 % /15/17 16:32 03/18/17 09: Terphenyl-d14 (S) 53 % /15/17 16:32 03/18/17 09: Phenol-d6 (S) 20 % /15/17 16:32 03/18/17 09: Fluorophenol (S) 27 % /15/17 16:32 03/18/17 09: ,4,6-Tribromophenol (S) 72 % /15/17 16:32 03/18/17 09: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 12: Acetonitrile 5.0 ug/l /15/17 12: Benzene 0.10 ug/l /15/17 12: Bromochloromethane 0.50 ug/l /15/17 12: Bromodichloromethane 0.27 ug/l /15/17 12: Bromoform 0.50 ug/l /15/17 12: Bromomethane 0.50 ug/l /15/17 12: Butanone (MEK) 5.0 ug/l /15/17 12: Carbon disulfide 5.0 ug/l /15/17 12: Carbon tetrachloride 0.50 ug/l /15/17 12: Chlorobenzene 0.50 ug/l /15/17 12: Chloroethane 0.50 ug/l /15/17 12: Chloroform 0.50 ug/l /15/17 12: Chloromethane 0.62 ug/l /15/17 12: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 12: Dibromochloromethane 0.26 ug/l /15/17 12: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 12: Dibromomethane 0.50 ug/l /15/17 12: ,2-Dichlorobenzene 0.50 ug/l /15/17 12: ,4-Dichlorobenzene 0.50 ug/l /15/17 12: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 12: ,1-Dichloroethane 0.50 ug/l /15/17 12: ,2-Dichloroethane 0.50 ug/l /15/17 12: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 12: N2 1,1-Dichloroethene 0.50 ug/l /15/17 12: cis-1,2-dichloroethene 0.50 ug/l /15/17 12: trans-1,2-dichloroethene 0.50 ug/l /15/17 12: ,2-Dichloropropane 0.50 ug/l /15/17 12: cis-1,3-dichloropropene 0.25 ug/l /15/17 12: trans-1,3-dichloropropene 0.25 ug/l /15/17 12: Ethylbenzene 0.50 ug/l /15/17 12: Hexanone 5.0 ug/l /15/17 12: Iodomethane 0.50 ug/l /15/17 12: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 12: Methylene Chloride 2.5 ug/l /15/17 12: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 12: Methyl-tert-butyl ether 0.50 ug/l /15/17 12: Date: 03/22/ :42 PM without the written consent of. Page 19 of 69

76 #=AR# ANALYTICAL RESLTS Sample: TMW-3 Lab ID: Collected: 03/10/17 13:59 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 12: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 12: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 12: Tetrachloroethene 0.50 ug/l /15/17 12: Toluene 0.50 ug/l /15/17 12: ,1,1-Trichloroethane 0.50 ug/l /15/17 12: ,1,2-Trichloroethane 0.50 ug/l /15/17 12: Trichloroethene 0.50 ug/l /15/17 12: Trichlorofluoromethane 0.50 ug/l /15/17 12: ,2,3-Trichloropropane 0.59 ug/l /15/17 12: ,2,4-Trimethylbenzene 0.50 ug/l /15/17 12: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 12: Vinyl acetate 1.0 ug/l /15/17 12: Vinyl chloride 0.50 ug/l /15/17 12: Xylene (Total) 1.5 ug/l /15/17 12: m&p-xylene 1.0 ug/l /15/17 12: o-xylene 0.50 ug/l /15/17 12: Surrogates 4-Bromofluorobenzene (S) 97 % /15/17 12: ,2-Dichloroethane-d4 (S) 104 % /15/17 12: Toluene-d8 (S) 97 % /15/17 12: Date: 03/22/ :42 PM without the written consent of. Page 20 of 69

77 #=AR# ANALYTICAL RESLTS Sample: TMW-4 Lab ID: Collected: 03/10/17 12:36 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ug/l /16/17 12:00 03/17/17 09: alpha-bhc ug/l /16/17 12:00 03/17/17 09: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 09: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 09: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 09: J(L2) Chlordane (Technical) 0.17 ug/l /16/17 12:00 03/17/17 09: ,4'-DDD ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 09: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 09: J(L2) Dieldrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 09: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 09: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 09: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 09: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 09: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 09: Toxaphene 0.24 ug/l /16/17 12:00 03/17/17 09: Surrogates Tetrachloro-m-xylene (S) 50 % /16/17 12:00 03/17/17 09: Decachlorobiphenyl (S) 24 % /16/17 12:00 03/17/17 09: FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 0.80 mg/l /16/17 08:00 03/16/17 23:03 Surrogates o-terphenyl (S) 123 % /16/17 08:00 03/16/17 23: N-Pentatriacontane (S) 84 % /16/17 08:00 03/16/17 23: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 5.0 ug/l /16/17 18:37 03/17/17 22: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 5.0 ug/l /16/17 19:54 03/20/17 15: MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ug/l /16/17 15:32 03/17/17 08: Acenaphthylene ug/l /16/17 15:32 03/17/17 08: Anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)anthracene ug/l /16/17 15:32 03/17/17 08: Benzo(a)pyrene ug/l /16/17 15:32 03/17/17 08: Benzo(b)fluoranthene ug/l /16/17 15:32 03/17/17 08: C Benzo(g,h,i)perylene ug/l /16/17 15:32 03/17/17 08: Benzo(k)fluoranthene ug/l /16/17 15:32 03/17/17 08: Chrysene ug/l /16/17 15:32 03/17/17 08: Date: 03/22/ :42 PM without the written consent of. Page 21 of 69

78 #=AR# ANALYTICAL RESLTS Sample: TMW-4 Lab ID: Collected: 03/10/17 12:36 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /16/17 15:32 03/17/17 08: Fluoranthene ug/l /16/17 15:32 03/17/17 08: Fluorene ug/l /16/17 15:32 03/17/17 08: Indeno(1,2,3-cd)pyrene ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Naphthalene 1.0 ug/l /16/17 15:32 03/17/17 08: Phenanthrene ug/l /16/17 15:32 03/17/17 08: Pyrene ug/l /16/17 15:32 03/17/17 08: Surrogates 2-Fluorobiphenyl (S) 57 % /16/17 15:32 03/17/17 08: Terphenyl-d14 (S) 51 % /16/17 15:32 03/17/17 08: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.81 ug/l /15/17 16:32 03/18/17 10: Acenaphthylene 0.89 ug/l /15/17 16:32 03/18/17 10: Aniline 1.9 ug/l /15/17 16:32 03/18/17 10: Anthracene 0.56 ug/l /15/17 16:32 03/18/17 10: Benzidine 0.72 ug/l /15/17 16:32 03/18/17 10: Benzo(a)anthracene 0.59 ug/l /15/17 16:32 03/18/17 10: Benzo(a)pyrene 0.54 ug/l /15/17 16:32 03/18/17 10: Benzo(b)fluoranthene 0.58 ug/l /15/17 16:32 03/18/17 10: Benzo(g,h,i)perylene 0.64 ug/l /15/17 16:32 03/18/17 10: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 10: J(L1) Benzyl alcohol 0.59 ug/l /15/17 16:32 03/18/17 10: Bromophenylphenyl ether 0.63 ug/l /15/17 16:32 03/18/17 10: Butylbenzylphthalate 0.67 ug/l /15/17 16:32 03/18/17 10: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 10: J(L1), N2 Carbazole 0.44 ug/l /15/17 16:32 03/18/17 10: Chloro-3-methylphenol 0.58 ug/l /15/17 16:32 03/18/17 10: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethyl) ether 0.70 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroisopropyl) ether 0.68 ug/l /15/17 16:32 03/18/17 10: Chloronaphthalene 0.75 ug/l /15/17 16:32 03/18/17 10: Chlorophenol 0.64 ug/l /15/17 16:32 03/18/17 10: Chlorophenylphenyl ether 0.59 ug/l /15/17 16:32 03/18/17 10: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 10: Dibenz(a,h)anthracene 0.61 ug/l /15/17 16:32 03/18/17 10: Dibenzofuran 0.63 ug/l /15/17 16:32 03/18/17 10: ,2-Dichlorobenzene 0.64 ug/l /15/17 16:32 03/18/17 10: ,3-Dichlorobenzene 0.71 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 10: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorophenol 0.52 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 22 of 69

79 #=AR# ANALYTICAL RESLTS Sample: TMW-4 Lab ID: Collected: 03/10/17 12:36 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 10: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 10: Dimethylphthalate 0.60 ug/l /15/17 16:32 03/18/17 10: Di-n-butylphthalate 0.38 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitro-2-methylphenol 1.2 ug/l /15/17 16:32 03/18/17 10: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 10: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 10: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 10: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitrotoluene 1.1 ug/l /15/17 16:32 03/18/17 10: Di-n-octylphthalate 0.84 ug/l /15/17 16:32 03/18/17 10: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 10: bis(2-ethylhexyl)phthalate 1.8 I ug/l /15/17 16:32 03/18/17 10: Fluoranthene 0.51 ug/l /15/17 16:32 03/18/17 10: Fluorene 0.52 ug/l /15/17 16:32 03/18/17 10: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 10: Hexachlorobenzene 0.75 ug/l /15/17 16:32 03/18/17 10: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 10: C Hexachloroethane 0.66 ug/l /15/17 16:32 03/18/17 10: Indeno(1,2,3-cd)pyrene 0.68 ug/l /15/17 16:32 03/18/17 10: Isophorone 0.68 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.93 ug/l /15/17 16:32 03/18/17 10: Methylphenol(o-Cresol) 0.68 ug/l /15/17 16:32 03/18/17 10: &4-Methylphenol(m&p Cresol) 0.62 ug/l /15/17 16:32 03/18/17 10:14 Naphthalene 0.73 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.56 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.93 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 10: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 0.76 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodimethylamine 0.91 ug/l /15/17 16:32 03/18/17 10: N-Nitroso-di-n-propylamine 0.88 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 10: Pentachlorophenol 0.62 ug/l /15/17 16:32 03/18/17 10: C Phenanthrene 0.49 ug/l /15/17 16:32 03/18/17 10: Phenol 0.51 ug/l /15/17 16:32 03/18/17 10: Pyrene 0.64 ug/l /15/17 16:32 03/18/17 10: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 10: ,3,4,6-Tetrachlorophenol 3.6 ug/l /15/17 16:32 03/18/17 10: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: N2 1,2,4-Trichlorobenzene 0.78 ug/l /15/17 16:32 03/18/17 10: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 23 of 69

80 #=AR# ANALYTICAL RESLTS Sample: TMW-4 Lab ID: Collected: 03/10/17 12:36 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 54 % /15/17 16:32 03/18/17 10: Fluorobiphenyl (S) 67 % /15/17 16:32 03/18/17 10: Terphenyl-d14 (S) 96 % /15/17 16:32 03/18/17 10: Phenol-d6 (S) 17 % /15/17 16:32 03/18/17 10: Fluorophenol (S) 26 % /15/17 16:32 03/18/17 10: ,4,6-Tribromophenol (S) 87 % /15/17 16:32 03/18/17 10: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 12: J(M1) Acetonitrile 5.0 ug/l /15/17 12: J(M1) Benzene 0.10 ug/l /15/17 12: Bromochloromethane 0.50 ug/l /15/17 12: Bromodichloromethane 0.27 ug/l /15/17 12: Bromoform 0.50 ug/l /15/17 12: Bromomethane 0.50 ug/l /15/17 12: Butanone (MEK) 5.0 ug/l /15/17 12: J(M1) Carbon disulfide 5.0 ug/l /15/17 12: Carbon tetrachloride 0.50 ug/l /15/17 12: Chlorobenzene 0.50 ug/l /15/17 12: Chloroethane 0.50 ug/l /15/17 12: Chloroform 0.50 ug/l /15/17 12: Chloromethane 0.62 ug/l /15/17 12: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 12: J(M1) Dibromochloromethane 0.26 ug/l /15/17 12: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 12: Dibromomethane 0.50 ug/l /15/17 12: ,2-Dichlorobenzene 0.50 ug/l /15/17 12: ,4-Dichlorobenzene 0.50 ug/l /15/17 12: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 12: ,1-Dichloroethane 0.50 ug/l /15/17 12: ,2-Dichloroethane 0.50 ug/l /15/17 12: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 12: N2 1,1-Dichloroethene 0.50 ug/l /15/17 12: cis-1,2-dichloroethene 0.50 ug/l /15/17 12: trans-1,2-dichloroethene 0.50 ug/l /15/17 12: ,2-Dichloropropane 0.50 ug/l /15/17 12: cis-1,3-dichloropropene 0.25 ug/l /15/17 12: trans-1,3-dichloropropene 0.25 ug/l /15/17 12: Ethylbenzene 0.50 ug/l /15/17 12: Hexanone 5.0 ug/l /15/17 12: J(M1) Iodomethane 0.50 ug/l /15/17 12: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 12: Methylene Chloride 2.5 ug/l /15/17 12: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 12: J(M1) Methyl-tert-butyl ether 0.50 ug/l /15/17 12: Date: 03/22/ :42 PM without the written consent of. Page 24 of 69

81 #=AR# ANALYTICAL RESLTS Sample: TMW-4 Lab ID: Collected: 03/10/17 12:36 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 12: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 12: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 12: Tetrachloroethene 0.50 ug/l /15/17 12: Toluene 0.50 ug/l /15/17 12: ,1,1-Trichloroethane 0.50 ug/l /15/17 12: ,1,2-Trichloroethane 0.50 ug/l /15/17 12: Trichloroethene 0.50 ug/l /15/17 12: Trichlorofluoromethane 0.50 ug/l /15/17 12: ,2,3-Trichloropropane 0.59 ug/l /15/17 12: ,2,4-Trimethylbenzene 0.50 ug/l /15/17 12: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 12: Vinyl acetate 1.0 ug/l /15/17 12: Vinyl chloride 0.50 ug/l /15/17 12: Xylene (Total) 1.5 ug/l /15/17 12: m&p-xylene 1.0 ug/l /15/17 12: o-xylene 0.50 ug/l /15/17 12: Surrogates 4-Bromofluorobenzene (S) 96 % /15/17 12: ,2-Dichloroethane-d4 (S) 102 % /15/17 12: Toluene-d8 (S) 96 % /15/17 12: Date: 03/22/ :42 PM without the written consent of. Page 25 of 69

82 #=AR# ANALYTICAL RESLTS Sample: TMW-5 Lab ID: Collected: 03/10/17 11:37 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin ug/l /16/17 12:00 03/17/17 10: alpha-bhc ug/l /16/17 12:00 03/17/17 10: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 10: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 10: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 10: J(L2) Chlordane (Technical) 0.17 ug/l /16/17 12:00 03/17/17 10: ,4'-DDD ug/l /16/17 12:00 03/17/17 10: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 10: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 10: J(L2) Dieldrin ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 10: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 10: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 10: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 10: Toxaphene 0.24 ug/l /16/17 12:00 03/17/17 10: Surrogates Tetrachloro-m-xylene (S) 36 % /16/17 12:00 03/17/17 10: Decachlorobiphenyl (S) 21 % /16/17 12:00 03/17/17 10: FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 1.3 mg/l /16/17 08:00 03/16/17 20:46 Surrogates o-terphenyl (S) 90 % /16/17 08:00 03/16/17 20: N-Pentatriacontane (S) 106 % /16/17 08:00 03/16/17 20: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 5.0 ug/l /18/17 10:43 03/20/17 17: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 5.0 ug/l /16/17 19:54 03/20/17 15: MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene 0.22 I ug/l /16/17 15:32 03/17/17 09: Acenaphthylene ug/l /16/17 15:32 03/17/17 09: Anthracene ug/l /16/17 15:32 03/17/17 09: Benzo(a)anthracene ug/l /16/17 15:32 03/17/17 09: Benzo(a)pyrene ug/l /16/17 15:32 03/17/17 09: Benzo(b)fluoranthene ug/l /16/17 15:32 03/17/17 09: C Benzo(g,h,i)perylene ug/l /16/17 15:32 03/17/17 09: Benzo(k)fluoranthene ug/l /16/17 15:32 03/17/17 09: Chrysene ug/l /16/17 15:32 03/17/17 09: Date: 03/22/ :42 PM without the written consent of. Page 26 of 69

83 #=AR# ANALYTICAL RESLTS Sample: TMW-5 Lab ID: Collected: 03/10/17 11:37 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /16/17 15:32 03/17/17 09: Fluoranthene ug/l /16/17 15:32 03/17/17 09: Fluorene ug/l /16/17 15:32 03/17/17 09: Indeno(1,2,3-cd)pyrene ug/l /16/17 15:32 03/17/17 09: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Naphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Phenanthrene ug/l /16/17 15:32 03/17/17 09: Pyrene ug/l /16/17 15:32 03/17/17 09: Surrogates 2-Fluorobiphenyl (S) 60 % /16/17 15:32 03/17/17 09: Terphenyl-d14 (S) 53 % /16/17 15:32 03/17/17 09: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.81 ug/l /15/17 16:32 03/18/17 10: Acenaphthylene 0.90 ug/l /15/17 16:32 03/18/17 10: Aniline 1.9 ug/l /15/17 16:32 03/18/17 10: Anthracene 0.57 ug/l /15/17 16:32 03/18/17 10: Benzidine 0.73 ug/l /15/17 16:32 03/18/17 10: Benzo(a)anthracene 0.59 ug/l /15/17 16:32 03/18/17 10: Benzo(a)pyrene 0.55 ug/l /15/17 16:32 03/18/17 10: Benzo(b)fluoranthene 0.58 ug/l /15/17 16:32 03/18/17 10: Benzo(g,h,i)perylene 0.64 ug/l /15/17 16:32 03/18/17 10: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 10: J(L1) Benzyl alcohol 0.59 ug/l /15/17 16:32 03/18/17 10: Bromophenylphenyl ether 0.63 ug/l /15/17 16:32 03/18/17 10: Butylbenzylphthalate 0.68 ug/l /15/17 16:32 03/18/17 10: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 10: J(L1), N2 Carbazole 0.44 ug/l /15/17 16:32 03/18/17 10: Chloro-3-methylphenol 0.58 ug/l /15/17 16:32 03/18/17 10: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethyl) ether 0.71 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroisopropyl) ether 0.69 ug/l /15/17 16:32 03/18/17 10: Chloronaphthalene 0.75 ug/l /15/17 16:32 03/18/17 10: Chlorophenol 0.64 ug/l /15/17 16:32 03/18/17 10: Chlorophenylphenyl ether 0.59 ug/l /15/17 16:32 03/18/17 10: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 10: Dibenz(a,h)anthracene 0.61 ug/l /15/17 16:32 03/18/17 10: Dibenzofuran 0.63 ug/l /15/17 16:32 03/18/17 10: ,2-Dichlorobenzene 0.64 ug/l /15/17 16:32 03/18/17 10: ,3-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorobenzene 0.73 ug/l /15/17 16:32 03/18/17 10: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorophenol 0.53 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 27 of 69

84 #=AR# ANALYTICAL RESLTS Sample: TMW-5 Lab ID: Collected: 03/10/17 11:37 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 10: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 10: Dimethylphthalate 0.60 ug/l /15/17 16:32 03/18/17 10: Di-n-butylphthalate 0.39 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitro-2-methylphenol 1.2 ug/l /15/17 16:32 03/18/17 10: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 10: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 10: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 10: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitrotoluene 1.1 ug/l /15/17 16:32 03/18/17 10: Di-n-octylphthalate 0.85 ug/l /15/17 16:32 03/18/17 10: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 10: bis(2-ethylhexyl)phthalate 1.7 I ug/l /15/17 16:32 03/18/17 10: Fluoranthene 0.51 ug/l /15/17 16:32 03/18/17 10: Fluorene 0.53 ug/l /15/17 16:32 03/18/17 10: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 10: Hexachlorobenzene 0.75 ug/l /15/17 16:32 03/18/17 10: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 10: C Hexachloroethane 0.67 ug/l /15/17 16:32 03/18/17 10: Indeno(1,2,3-cd)pyrene 0.69 ug/l /15/17 16:32 03/18/17 10: Isophorone 0.69 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.93 ug/l /15/17 16:32 03/18/17 10: Methylphenol(o-Cresol) 0.69 ug/l /15/17 16:32 03/18/17 10: &4-Methylphenol(m&p Cresol) 0.62 ug/l /15/17 16:32 03/18/17 10:36 Naphthalene 0.74 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.57 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.93 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 10: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 0.76 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodimethylamine 0.91 ug/l /15/17 16:32 03/18/17 10: N-Nitroso-di-n-propylamine 0.89 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 10: Pentachlorophenol 0.62 ug/l /15/17 16:32 03/18/17 10: C Phenanthrene 0.49 ug/l /15/17 16:32 03/18/17 10: Phenol 0.51 ug/l /15/17 16:32 03/18/17 10: Pyrene 0.64 ug/l /15/17 16:32 03/18/17 10: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 10: ,3,4,6-Tetrachlorophenol 3.6 ug/l /15/17 16:32 03/18/17 10: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: N2 1,2,4-Trichlorobenzene 0.78 ug/l /15/17 16:32 03/18/17 10: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 28 of 69

85 #=AR# ANALYTICAL RESLTS Sample: TMW-5 Lab ID: Collected: 03/10/17 11:37 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 48 % /15/17 16:32 03/18/17 10: Fluorobiphenyl (S) 55 % /15/17 16:32 03/18/17 10: Terphenyl-d14 (S) 40 % /15/17 16:32 03/18/17 10: Phenol-d6 (S) 16 % /15/17 16:32 03/18/17 10: Fluorophenol (S) 19 % /15/17 16:32 03/18/17 10: ,4,6-Tribromophenol (S) 80 % /15/17 16:32 03/18/17 10: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 13: Acetonitrile 5.0 ug/l /15/17 13: Benzene 0.10 ug/l /15/17 13: Bromochloromethane 0.50 ug/l /15/17 13: Bromodichloromethane 0.27 ug/l /15/17 13: Bromoform 0.50 ug/l /15/17 13: Bromomethane 0.50 ug/l /15/17 13: Butanone (MEK) 5.0 ug/l /15/17 13: Carbon disulfide 5.0 ug/l /15/17 13: Carbon tetrachloride 0.50 ug/l /15/17 13: Chlorobenzene 0.50 ug/l /15/17 13: Chloroethane 0.50 ug/l /15/17 13: Chloroform 0.50 ug/l /15/17 13: Chloromethane 0.62 ug/l /15/17 13: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 13: Dibromochloromethane 0.26 ug/l /15/17 13: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 13: Dibromomethane 0.50 ug/l /15/17 13: ,2-Dichlorobenzene 0.50 ug/l /15/17 13: ,4-Dichlorobenzene 0.50 ug/l /15/17 13: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 13: ,1-Dichloroethane 0.50 ug/l /15/17 13: ,2-Dichloroethane 0.50 ug/l /15/17 13: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 13: N2 1,1-Dichloroethene 0.50 ug/l /15/17 13: cis-1,2-dichloroethene 0.50 ug/l /15/17 13: trans-1,2-dichloroethene 0.50 ug/l /15/17 13: ,2-Dichloropropane 0.50 ug/l /15/17 13: cis-1,3-dichloropropene 0.25 ug/l /15/17 13: trans-1,3-dichloropropene 0.25 ug/l /15/17 13: Ethylbenzene 0.50 ug/l /15/17 13: Hexanone 5.0 ug/l /15/17 13: Iodomethane 0.50 ug/l /15/17 13: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 13: Methylene Chloride 2.5 ug/l /15/17 13: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 13: Methyl-tert-butyl ether 0.50 ug/l /15/17 13: Date: 03/22/ :42 PM without the written consent of. Page 29 of 69

86 #=AR# ANALYTICAL RESLTS Sample: TMW-5 Lab ID: Collected: 03/10/17 11:37 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 13: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 13: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 13: Tetrachloroethene 0.50 ug/l /15/17 13: Toluene 0.50 ug/l /15/17 13: ,1,1-Trichloroethane 0.50 ug/l /15/17 13: ,1,2-Trichloroethane 0.50 ug/l /15/17 13: Trichloroethene 0.50 ug/l /15/17 13: Trichlorofluoromethane 0.50 ug/l /15/17 13: ,2,3-Trichloropropane 0.59 ug/l /15/17 13: ,2,4-Trimethylbenzene 0.50 ug/l /15/17 13: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 13: Vinyl acetate 1.0 ug/l /15/17 13: Vinyl chloride 0.50 ug/l /15/17 13: Xylene (Total) 1.5 ug/l /15/17 13: m&p-xylene 1.0 ug/l /15/17 13: o-xylene 0.50 ug/l /15/17 13: Surrogates 4-Bromofluorobenzene (S) 96 % /15/17 13: ,2-Dichloroethane-d4 (S) 102 % /15/17 13: Toluene-d8 (S) 96 % /15/17 13: Date: 03/22/ :42 PM without the written consent of. Page 30 of 69

87 #=AR# ANALYTICAL RESLTS Sample: SW-1 Lab ID: Collected: 03/10/17 16:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides Analytical Method: EPA 8081 Preparation Method: EPA 3510 Aldrin I ug/l /16/17 12:00 03/17/17 10: alpha-bhc ug/l /16/17 12:00 03/17/17 10: p,J(L2) beta-bhc ug/l /16/17 12:00 03/17/17 10: J(L2) delta-bhc ug/l /16/17 12:00 03/17/17 10: gamma-bhc (Lindane) ug/l /16/17 12:00 03/17/17 10: J(L2) Chlordane (Technical) 0.17 ug/l /16/17 12:00 03/17/17 10: ,4'-DDD ug/l /16/17 12:00 03/17/17 10: J(L2) 4,4'-DDE ug/l /16/17 12:00 03/17/17 10: J(L2) 4,4'-DDT ug/l /16/17 12:00 03/17/17 10: J(L2) Dieldrin I ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan I ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan II ug/l /16/17 12:00 03/17/17 10: J(L2) Endosulfan sulfate ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin aldehyde ug/l /16/17 12:00 03/17/17 10: J(L2) Endrin ketone ug/l /16/17 12:00 03/17/17 10: J(L2) Heptachlor ug/l /16/17 12:00 03/17/17 10: Heptachlor epoxide ug/l /16/17 12:00 03/17/17 10: J(L2) Methoxychlor ug/l /16/17 12:00 03/17/17 10: Toxaphene 0.24 ug/l /16/17 12:00 03/17/17 10: Surrogates Tetrachloro-m-xylene (S) 28 % /16/17 12:00 03/17/17 10: Decachlorobiphenyl (S) 16 % /16/17 12:00 03/17/17 10: FL-PRO Water, Low Volume Analytical Method: FL-PRO Preparation Method: EPA 3510 Petroleum Range Organics 0.80 mg/l /16/17 08:00 03/17/17 01:10 Surrogates o-terphenyl (S) 108 % /16/17 08:00 03/17/17 01: N-Pentatriacontane (S) 90 % /16/17 08:00 03/17/17 01: MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic 5.0 ug/l /18/17 10:43 03/20/17 17: MET ICP, Dissolved Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic, Dissolved 5.0 ug/l /16/17 19:54 03/20/17 15: MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Acenaphthene ug/l /16/17 15:32 03/17/17 09: Acenaphthylene ug/l /16/17 15:32 03/17/17 09: Anthracene ug/l /16/17 15:32 03/17/17 09: Benzo(a)anthracene ug/l /16/17 15:32 03/17/17 09: Benzo(a)pyrene ug/l /16/17 15:32 03/17/17 09: Benzo(b)fluoranthene ug/l /16/17 15:32 03/17/17 09: C Benzo(g,h,i)perylene ug/l /16/17 15:32 03/17/17 09: Benzo(k)fluoranthene ug/l /16/17 15:32 03/17/17 09: Chrysene ug/l /16/17 15:32 03/17/17 09: Date: 03/22/ :42 PM without the written consent of. Page 31 of 69

88 #=AR# ANALYTICAL RESLTS Sample: SW-1 Lab ID: Collected: 03/10/17 16:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV PAHLV by SIM Analytical Method: EPA 8270 by SIM Preparation Method: EPA 3510 Dibenz(a,h)anthracene ug/l /16/17 15:32 03/17/17 09: Fluoranthene ug/l /16/17 15:32 03/17/17 09: Fluorene ug/l /16/17 15:32 03/17/17 09: Indeno(1,2,3-cd)pyrene ug/l /16/17 15:32 03/17/17 09: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Methylnaphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Naphthalene 1.0 ug/l /16/17 15:32 03/17/17 09: Phenanthrene ug/l /16/17 15:32 03/17/17 09: Pyrene ug/l /16/17 15:32 03/17/17 09: Surrogates 2-Fluorobiphenyl (S) 55 % /16/17 15:32 03/17/17 09: Terphenyl-d14 (S) 51 % /16/17 15:32 03/17/17 09: MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene 0.81 ug/l /15/17 16:32 03/18/17 10: Acenaphthylene 0.90 ug/l /15/17 16:32 03/18/17 10: Aniline 1.9 ug/l /15/17 16:32 03/18/17 10: Anthracene 0.57 ug/l /15/17 16:32 03/18/17 10: Benzidine 0.73 ug/l /15/17 16:32 03/18/17 10: Benzo(a)anthracene 0.60 ug/l /15/17 16:32 03/18/17 10: Benzo(a)pyrene 0.55 ug/l /15/17 16:32 03/18/17 10: Benzo(b)fluoranthene 0.59 ug/l /15/17 16:32 03/18/17 10: Benzo(g,h,i)perylene 0.64 ug/l /15/17 16:32 03/18/17 10: Benzo(k)fluoranthene 0.48 ug/l /15/17 16:32 03/18/17 10: J(L1) Benzyl alcohol 0.60 ug/l /15/17 16:32 03/18/17 10: Bromophenylphenyl ether 0.63 ug/l /15/17 16:32 03/18/17 10: Butylbenzylphthalate 0.68 ug/l /15/17 16:32 03/18/17 10: Caprolactam 1.2 ug/l /15/17 16:32 03/18/17 10: J(L1), N2 Carbazole 0.45 ug/l /15/17 16:32 03/18/17 10: Chloro-3-methylphenol 0.59 ug/l /15/17 16:32 03/18/17 10: Chloroaniline 1.1 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethoxy)methane 2.8 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroethyl) ether 0.71 ug/l /15/17 16:32 03/18/17 10: bis(2-chloroisopropyl) ether 0.69 ug/l /15/17 16:32 03/18/17 10: Chloronaphthalene 0.76 ug/l /15/17 16:32 03/18/17 10: Chlorophenol 0.64 ug/l /15/17 16:32 03/18/17 10: Chlorophenylphenyl ether 0.60 ug/l /15/17 16:32 03/18/17 10: Chrysene 0.35 ug/l /15/17 16:32 03/18/17 10: Dibenz(a,h)anthracene 0.62 ug/l /15/17 16:32 03/18/17 10: Dibenzofuran 0.63 ug/l /15/17 16:32 03/18/17 10: ,2-Dichlorobenzene 0.64 ug/l /15/17 16:32 03/18/17 10: ,3-Dichlorobenzene 0.72 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorobenzene 0.73 ug/l /15/17 16:32 03/18/17 10: ,3'-Dichlorobenzidine 0.65 ug/l /15/17 16:32 03/18/17 10: ,4-Dichlorophenol 0.53 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 32 of 69

89 #=AR# ANALYTICAL RESLTS Sample: SW-1 Lab ID: Collected: 03/10/17 16:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Diethylphthalate 0.48 ug/l /15/17 16:32 03/18/17 10: ,4-Dimethylphenol 1.5 ug/l /15/17 16:32 03/18/17 10: Dimethylphthalate 0.61 ug/l /15/17 16:32 03/18/17 10: Di-n-butylphthalate 0.39 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitro-2-methylphenol 1.2 ug/l /15/17 16:32 03/18/17 10: C 1,2-Dinitrobenzene 0.31 ug/l /15/17 16:32 03/18/17 10: ,3-Dinitrobenzene 0.28 ug/l /15/17 16:32 03/18/17 10: ,4-Dinitrophenol 1.5 ug/l /15/17 16:32 03/18/17 10: C 2,4-Dinitrotoluene 0.50 ug/l /15/17 16:32 03/18/17 10: ,6-Dinitrotoluene 1.2 ug/l /15/17 16:32 03/18/17 10: Di-n-octylphthalate 0.85 ug/l /15/17 16:32 03/18/17 10: ,2-Diphenylhydrazine 0.31 ug/l /15/17 16:32 03/18/17 10: bis(2-ethylhexyl)phthalate 1.7 I ug/l /15/17 16:32 03/18/17 10: Fluoranthene 0.51 ug/l /15/17 16:32 03/18/17 10: Fluorene 0.53 ug/l /15/17 16:32 03/18/17 10: Hexachloro-1,3-butadiene 1.0 ug/l /15/17 16:32 03/18/17 10: Hexachlorobenzene 0.76 ug/l /15/17 16:32 03/18/17 10: Hexachlorocyclopentadiene 1.2 ug/l /15/17 16:32 03/18/17 10: C Hexachloroethane 0.67 ug/l /15/17 16:32 03/18/17 10: Indeno(1,2,3-cd)pyrene 0.69 ug/l /15/17 16:32 03/18/17 10: Isophorone 0.69 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.95 ug/l /15/17 16:32 03/18/17 10: Methylnaphthalene 0.94 ug/l /15/17 16:32 03/18/17 10: Methylphenol(o-Cresol) 0.69 ug/l /15/17 16:32 03/18/17 10: &4-Methylphenol(m&p Cresol) 0.62 ug/l /15/17 16:32 03/18/17 10:59 Naphthalene 0.74 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.57 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.94 ug/l /15/17 16:32 03/18/17 10: Nitroaniline 0.65 ug/l /15/17 16:32 03/18/17 10: Nitrobenzene 1.0 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 0.77 ug/l /15/17 16:32 03/18/17 10: Nitrophenol 1.0 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodimethylamine 0.92 ug/l /15/17 16:32 03/18/17 10: N-Nitroso-di-n-propylamine 0.89 ug/l /15/17 16:32 03/18/17 10: N-Nitrosodiphenylamine 0.47 ug/l /15/17 16:32 03/18/17 10: Pentachlorophenol 0.62 ug/l /15/17 16:32 03/18/17 10: C Phenanthrene 0.49 ug/l /15/17 16:32 03/18/17 10: Phenol 0.51 ug/l /15/17 16:32 03/18/17 10: Pyrene 0.64 ug/l /15/17 16:32 03/18/17 10: Pyridine 1.4 ug/l /15/17 16:32 03/18/17 10: ,3,4,6-Tetrachlorophenol 3.6 ug/l /15/17 16:32 03/18/17 10: ,3,5,6-Tetrachlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: N2 1,2,4-Trichlorobenzene 0.79 ug/l /15/17 16:32 03/18/17 10: ,4,5-Trichlorophenol 0.49 ug/l /15/17 16:32 03/18/17 10: ,4,6-Trichlorophenol 0.65 ug/l /15/17 16:32 03/18/17 10: Date: 03/22/ :42 PM without the written consent of. Page 33 of 69

90 #=AR# ANALYTICAL RESLTS Sample: SW-1 Lab ID: Collected: 03/10/17 16:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510 Surrogates Nitrobenzene-d5 (S) 42 % /15/17 16:32 03/18/17 10: Fluorobiphenyl (S) 57 % /15/17 16:32 03/18/17 10: Terphenyl-d14 (S) 100 % /15/17 16:32 03/18/17 10: Phenol-d6 (S) 14 % /15/17 16:32 03/18/17 10: Fluorophenol (S) 19 % /15/17 16:32 03/18/17 10: ,4,6-Tribromophenol (S) 90 % /15/17 16:32 03/18/17 10: MSV Analytical Method: EPA 8260 Acetone 10.0 ug/l /15/17 13: Acetonitrile 5.0 ug/l /15/17 13: Benzene 0.10 ug/l /15/17 13: Bromochloromethane 0.50 ug/l /15/17 13: Bromodichloromethane 0.27 ug/l /15/17 13: Bromoform 0.50 ug/l /15/17 13: Bromomethane 0.50 ug/l /15/17 13: Butanone (MEK) 5.0 ug/l /15/17 13: Carbon disulfide 5.0 ug/l /15/17 13: Carbon tetrachloride 0.50 ug/l /15/17 13: Chlorobenzene 0.50 ug/l /15/17 13: Chloroethane 0.50 ug/l /15/17 13: Chloroform 0.50 ug/l /15/17 13: Chloromethane 0.62 ug/l /15/17 13: ,2-Dibromo-3-chloropropane 1.0 ug/l /15/17 13: Dibromochloromethane 0.26 ug/l /15/17 13: ,2-Dibromoethane (EDB) 0.50 ug/l /15/17 13: Dibromomethane 0.50 ug/l /15/17 13: ,2-Dichlorobenzene 0.50 ug/l /15/17 13: ,4-Dichlorobenzene 0.50 ug/l /15/17 13: trans-1,4-dichloro-2-butene 5.0 ug/l /15/17 13: ,1-Dichloroethane 0.50 ug/l /15/17 13: ,2-Dichloroethane 0.50 ug/l /15/17 13: ,2-Dichloroethene (Total) 0.50 ug/l /15/17 13: N2 1,1-Dichloroethene 0.50 ug/l /15/17 13: cis-1,2-dichloroethene 0.50 ug/l /15/17 13: trans-1,2-dichloroethene 0.50 ug/l /15/17 13: ,2-Dichloropropane 0.50 ug/l /15/17 13: cis-1,3-dichloropropene 0.25 ug/l /15/17 13: trans-1,3-dichloropropene 0.25 ug/l /15/17 13: Ethylbenzene 0.50 ug/l /15/17 13: Hexanone 5.0 ug/l /15/17 13: Iodomethane 0.50 ug/l /15/17 13: Isopropylbenzene (Cumene) 0.50 ug/l /15/17 13: Methylene Chloride 2.5 ug/l /15/17 13: Methyl-2-pentanone (MIBK) 5.0 ug/l /15/17 13: Methyl-tert-butyl ether 0.50 ug/l /15/17 13: Date: 03/22/ :42 PM without the written consent of. Page 34 of 69

91 #=AR# ANALYTICAL RESLTS Sample: SW-1 Lab ID: Collected: 03/10/17 16:10 Received: 03/14/17 03:20 Matrix: Water s s nits PQL MDL DF Prepared Analyzed CAS No. Qual 8260 MSV Analytical Method: EPA 8260 Styrene 0.50 ug/l /15/17 13: ,1,1,2-Tetrachloroethane 0.50 ug/l /15/17 13: ,1,2,2-Tetrachloroethane 0.12 ug/l /15/17 13: Tetrachloroethene 0.50 ug/l /15/17 13: Toluene 0.50 ug/l /15/17 13: ,1,1-Trichloroethane 0.50 ug/l /15/17 13: ,1,2-Trichloroethane 0.50 ug/l /15/17 13: Trichloroethene 0.50 ug/l /15/17 13: Trichlorofluoromethane 0.50 ug/l /15/17 13: ,2,3-Trichloropropane 0.59 ug/l /15/17 13: ,2,4-Trimethylbenzene 0.50 ug/l /15/17 13: ,3,5-Trimethylbenzene 0.50 ug/l /15/17 13: Vinyl acetate 1.0 ug/l /15/17 13: Vinyl chloride 0.50 ug/l /15/17 13: Xylene (Total) 1.5 ug/l /15/17 13: m&p-xylene 1.0 ug/l /15/17 13: o-xylene 0.50 ug/l /15/17 13: Surrogates 4-Bromofluorobenzene (S) 96 % /15/17 13: ,2-Dichloroethane-d4 (S) 104 % /15/17 13: Toluene-d8 (S) 96 % /15/17 13: Date: 03/22/ :42 PM without the written consent of. Page 35 of 69

92 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3010 Analysis Method: Analysis Description: EPA MET Associated Lab Samples: , , , METHOD BLANK: Associated Lab Samples: , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed Arsenic ug/l /17/17 20:15 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Arsenic ug/l Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Arsenic ug/l Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 36 of 69

93 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3010 Associated Lab Samples: , Analysis Method: Analysis Description: EPA MET METHOD BLANK: Associated Lab Samples: , nits Blank Matrix: Water Reporting Limit MDL Analyzed Arsenic ug/l /20/17 16:21 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Arsenic ug/l Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Arsenic ug/l Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 37 of 69

94 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3010 Analysis Method: Analysis Description: EPA MET Filtered Associated Lab Samples: , , , , , METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed Arsenic, Dissolved ug/l /20/17 14:34 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Arsenic, Dissolved ug/l Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Arsenic, Dissolved ug/l I M6 Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 38 of 69

95 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 8260 Associated Lab Samples: , Analysis Method: Analysis Description: EPA MSV METHOD BLANK: Associated Lab Samples: , nits Blank Matrix: Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/l /14/17 23:59 1,1,1-Trichloroethane ug/l /14/17 23:59 1,1,2,2-Tetrachloroethane ug/l /14/17 23:59 1,1,2-Trichloroethane ug/l /14/17 23:59 1,1-Dichloroethane ug/l /14/17 23:59 1,1-Dichloroethene ug/l /14/17 23:59 1,2,3-Trichloropropane ug/l /14/17 23:59 1,2,4-Trimethylbenzene ug/l /14/17 23:59 1,2-Dibromo-3-chloropropane ug/l /14/17 23:59 1,2-Dibromoethane (EDB) ug/l /14/17 23:59 1,2-Dichlorobenzene ug/l /14/17 23:59 1,2-Dichloroethane ug/l /14/17 23:59 1,2-Dichloroethene (Total) ug/l /14/17 23:59 N2 1,2-Dichloropropane ug/l /14/17 23:59 1,3,5-Trimethylbenzene ug/l /14/17 23:59 1,4-Dichlorobenzene ug/l /14/17 23:59 2-Butanone (MEK) ug/l /14/17 23:59 2-Hexanone ug/l /14/17 23:59 4-Methyl-2-pentanone (MIBK) ug/l /14/17 23:59 Acetone ug/l /14/17 23:59 Acetonitrile ug/l /14/17 23:59 Benzene ug/l /14/17 23:59 Bromochloromethane ug/l /14/17 23:59 Bromodichloromethane ug/l /14/17 23:59 Bromoform ug/l /14/17 23:59 Bromomethane ug/l /14/17 23:59 Carbon disulfide ug/l /14/17 23:59 Carbon tetrachloride ug/l /14/17 23:59 Chlorobenzene ug/l /14/17 23:59 Chloroethane ug/l /14/17 23:59 Chloroform ug/l /14/17 23:59 Chloromethane ug/l /14/17 23:59 cis-1,2-dichloroethene ug/l /14/17 23:59 cis-1,3-dichloropropene ug/l /14/17 23:59 Dibromochloromethane ug/l /14/17 23:59 Dibromomethane ug/l /14/17 23:59 Ethylbenzene ug/l /14/17 23:59 Iodomethane ug/l /14/17 23:59 Isopropylbenzene (Cumene) ug/l /14/17 23:59 m&p-xylene ug/l /14/17 23:59 Methyl-tert-butyl ether ug/l /14/17 23:59 Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 39 of 69

96 #=QC# QALITY CONTROL DATA METHOD BLANK: Associated Lab Samples: , nits Blank Matrix: Water Reporting Limit MDL Analyzed Methylene Chloride ug/l /14/17 23:59 o-xylene ug/l /14/17 23:59 Styrene ug/l /14/17 23:59 Tetrachloroethene ug/l /14/17 23:59 Toluene ug/l /14/17 23:59 trans-1,2-dichloroethene ug/l /14/17 23:59 trans-1,3-dichloropropene ug/l /14/17 23:59 trans-1,4-dichloro-2-butene ug/l /14/17 23:59 Trichloroethene ug/l /14/17 23:59 Trichlorofluoromethane ug/l /14/17 23:59 Vinyl acetate ug/l /14/17 23:59 Vinyl chloride ug/l /14/17 23:59 Xylene (Total) ug/l /14/17 23:59 1,2-Dichloroethane-d4 (S) % /14/17 23:59 4-Bromofluorobenzene (S) % /14/17 23:59 Toluene-d8 (S) % /14/17 23:59 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l ,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l Butanone (MEK) ug/l Hexanone ug/l Methyl-2-pentanone (MIBK) ug/l Acetone ug/l Acetonitrile ug/l Benzene ug/l Bromochloromethane ug/l Bromodichloromethane ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 40 of 69

97 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 41 of 69

98 #=QC# QALITY CONTROL DATA MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec 1,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l Butanone (MEK) ug/l Hexanone ug/l Methyl-2-pentanone (MIBK) ug/l Acetone ug/l Acetonitrile ug/l Benzene ug/l Bromochloromethane ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % % Rec Limits s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Qualifiers Date: 03/22/ :42 PM without the written consent of. Page 42 of 69

99 #=QC# QALITY CONTROL DATA MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec % Rec Limits 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers SAMPLE DPLICATE: nits Dup 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l ,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l 0.91 I 0.84 I 40 N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l 0.54 I 0.50 I 40 2-Butanone (MEK) ug/l Hexanone ug/l Methyl-2-pentanone (MIBK) ug/l Acetone ug/l Acetonitrile ug/l Benzene ug/l 0.35 I 0.36 I 40 Bromochloromethane ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l 0.70 I 0.69 I 40 Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l 0.91 I 0.84 I 40 cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 43 of 69

100 #=QC# QALITY CONTROL DATA SAMPLE DPLICATE: nits Dup m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 44 of 69

101 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 8260 Analysis Method: Analysis Description: Associated Lab Samples: , , , METHOD BLANK: Associated Lab Samples: , , , nits Blank Matrix: Water Reporting Limit EPA MSV MDL Analyzed 1,1,1,2-Tetrachloroethane ug/l /15/17 11:38 1,1,1-Trichloroethane ug/l /15/17 11:38 1,1,2,2-Tetrachloroethane ug/l /15/17 11:38 1,1,2-Trichloroethane ug/l /15/17 11:38 1,1-Dichloroethane ug/l /15/17 11:38 1,1-Dichloroethene ug/l /15/17 11:38 1,2,3-Trichloropropane ug/l /15/17 11:38 1,2,4-Trimethylbenzene ug/l /15/17 11:38 1,2-Dibromo-3-chloropropane ug/l /15/17 11:38 1,2-Dibromoethane (EDB) ug/l /15/17 11:38 1,2-Dichlorobenzene ug/l /15/17 11:38 1,2-Dichloroethane ug/l /15/17 11:38 1,2-Dichloroethene (Total) ug/l /15/17 11:38 N2 1,2-Dichloropropane ug/l /15/17 11:38 1,3,5-Trimethylbenzene ug/l /15/17 11:38 1,4-Dichlorobenzene ug/l /15/17 11:38 2-Butanone (MEK) ug/l /15/17 11:38 2-Hexanone ug/l /15/17 11:38 4-Methyl-2-pentanone (MIBK) ug/l /15/17 11:38 Acetone ug/l /15/17 11:38 Acetonitrile ug/l /15/17 11:38 Benzene ug/l /15/17 11:38 Bromochloromethane ug/l /15/17 11:38 Bromodichloromethane ug/l /15/17 11:38 Bromoform ug/l /15/17 11:38 Bromomethane ug/l /15/17 11:38 Carbon disulfide ug/l /15/17 11:38 Carbon tetrachloride ug/l /15/17 11:38 Chlorobenzene ug/l /15/17 11:38 Chloroethane ug/l /15/17 11:38 Chloroform ug/l /15/17 11:38 Chloromethane ug/l /15/17 11:38 cis-1,2-dichloroethene ug/l /15/17 11:38 cis-1,3-dichloropropene ug/l /15/17 11:38 Dibromochloromethane ug/l /15/17 11:38 Dibromomethane ug/l /15/17 11:38 Ethylbenzene ug/l /15/17 11:38 Iodomethane ug/l /15/17 11:38 Isopropylbenzene (Cumene) ug/l /15/17 11:38 m&p-xylene ug/l /15/17 11:38 Methyl-tert-butyl ether ug/l /15/17 11:38 Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 45 of 69

102 #=QC# QALITY CONTROL DATA METHOD BLANK: Associated Lab Samples: , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed Methylene Chloride ug/l /15/17 11:38 o-xylene ug/l /15/17 11:38 Styrene ug/l /15/17 11:38 Tetrachloroethene ug/l /15/17 11:38 Toluene ug/l /15/17 11:38 trans-1,2-dichloroethene ug/l /15/17 11:38 trans-1,3-dichloropropene ug/l /15/17 11:38 trans-1,4-dichloro-2-butene ug/l /15/17 11:38 Trichloroethene ug/l /15/17 11:38 Trichlorofluoromethane ug/l /15/17 11:38 Vinyl acetate ug/l /15/17 11:38 Vinyl chloride ug/l /15/17 11:38 Xylene (Total) ug/l /15/17 11:38 1,2-Dichloroethane-d4 (S) % /15/17 11:38 4-Bromofluorobenzene (S) % /15/17 11:38 Toluene-d8 (S) % /15/17 11:38 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l ,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l Butanone (MEK) ug/l Hexanone ug/l Methyl-2-pentanone (MIBK) ug/l Acetone ug/l Acetonitrile ug/l Benzene ug/l Bromochloromethane ug/l Bromodichloromethane ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 46 of 69

103 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 47 of 69

104 #=QC# QALITY CONTROL DATA MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec 1,2-Dibromo-3-chloropropane ug/l J(M1) 1,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l Butanone (MEK) ug/l J(M1) 2-Hexanone ug/l J(M1) 4-Methyl-2-pentanone (MIBK) ug/l J(M1) Acetone ug/l I J(M1) Acetonitrile ug/l J(M1) Benzene ug/l Bromochloromethane ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % % Rec Limits s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Qualifiers Date: 03/22/ :42 PM without the written consent of. Page 48 of 69

105 #=QC# QALITY CONTROL DATA MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec % Rec Limits 4-Bromofluorobenzene (S) % Toluene-d8 (S) % Qualifiers SAMPLE DPLICATE: nits Dup 1,1,1,2-Tetrachloroethane ug/l ,1,1-Trichloroethane ug/l ,1,2,2-Tetrachloroethane ug/l ,1,2-Trichloroethane ug/l ,1-Dichloroethane ug/l ,1-Dichloroethene ug/l ,2,3-Trichloropropane ug/l ,2,4-Trimethylbenzene ug/l ,2-Dibromo-3-chloropropane ug/l ,2-Dibromoethane (EDB) ug/l ,2-Dichlorobenzene ug/l ,2-Dichloroethane ug/l ,2-Dichloroethene (Total) ug/l N2 1,2-Dichloropropane ug/l ,3,5-Trimethylbenzene ug/l ,4-Dichlorobenzene ug/l Butanone (MEK) ug/l Hexanone ug/l Methyl-2-pentanone (MIBK) ug/l Acetone ug/l Acetonitrile ug/l Benzene ug/l Bromochloromethane ug/l Bromodichloromethane ug/l Bromoform ug/l Bromomethane ug/l Carbon disulfide ug/l Carbon tetrachloride ug/l Chlorobenzene ug/l Chloroethane ug/l Chloroform ug/l Chloromethane ug/l cis-1,2-dichloroethene ug/l cis-1,3-dichloropropene ug/l Dibromochloromethane ug/l Dibromomethane ug/l Ethylbenzene ug/l Iodomethane ug/l Isopropylbenzene (Cumene) ug/l RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 49 of 69

106 #=QC# QALITY CONTROL DATA SAMPLE DPLICATE: nits Dup m&p-xylene ug/l Methyl-tert-butyl ether ug/l Methylene Chloride ug/l o-xylene ug/l Styrene ug/l Tetrachloroethene ug/l Toluene ug/l trans-1,2-dichloroethene ug/l trans-1,3-dichloropropene ug/l trans-1,4-dichloro-2-butene ug/l Trichloroethene ug/l Trichlorofluoromethane ug/l Vinyl acetate ug/l Vinyl chloride ug/l Xylene (Total) ug/l ,2-Dichloroethane-d4 (S) % Bromofluorobenzene (S) % Toluene-d8 (S) % RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 50 of 69

107 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3510 Analysis Method: Analysis Description: EPA GCS Pesticides Associated Lab Samples: , , , , , METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed 4,4'-DDD ug/l /16/17 19:53 4,4'-DDE ug/l /16/17 19:53 4,4'-DDT ug/l /16/17 19:53 Aldrin ug/l /16/17 19:53 alpha-bhc ug/l /16/17 19:53 beta-bhc ug/l /16/17 19:53 Chlordane (Technical) ug/l /16/17 19:53 delta-bhc ug/l /16/17 19:53 Dieldrin ug/l /16/17 19:53 Endosulfan I ug/l /16/17 19:53 Endosulfan II ug/l /16/17 19:53 Endosulfan sulfate ug/l /16/17 19:53 Endrin ug/l /16/17 19:53 Endrin aldehyde ug/l /16/17 19:53 Endrin ketone ug/l /16/17 19:53 gamma-bhc (Lindane) ug/l /16/17 19:53 Heptachlor ug/l /16/17 19:53 Heptachlor epoxide ug/l /16/17 19:53 Methoxychlor ug/l /16/17 19:53 Toxaphene ug/l /16/17 19:53 Decachlorobiphenyl (S) % /16/17 19:53 Tetrachloro-m-xylene (S) % /16/17 19:53 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: nits Spike Conc LCS LCSD LCS LCSD % Rec % Rec % Rec Limits RPD s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Max RPD Qualifiers 4,4'-DDD ug/l J(L2) 4,4'-DDE ug/l J(L2) 4,4'-DDT ug/l J(L2) Aldrin ug/l alpha-bhc ug/l J(L2),J(R1) beta-bhc ug/l J(L2),J(R1) delta-bhc ug/l J(R1) Dieldrin ug/l J(L2) Endosulfan I ug/l J(L2) Endosulfan II ug/l J(L2) Endosulfan sulfate ug/l J(L2) Endrin ug/l J(L2) Endrin aldehyde ug/l J(L2) Endrin ketone ug/l J(L2) Date: 03/22/ :42 PM without the written consent of. Page 51 of 69

108 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: nits Spike Conc LCS LCSD LCS LCSD % Rec % Rec % Rec Limits RPD Max RPD Qualifiers gamma-bhc (Lindane) ug/l J(L2),J(R1) Heptachlor ug/l Heptachlor epoxide ug/l J(L2) Methoxychlor ug/l Decachlorobiphenyl (S) % Tetrachloro-m-xylene (S) % s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 52 of 69

109 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3510 Analysis Method: Analysis Description: EPA 8270 by SIM 8270 Water PAHLV by SIM MSSV Associated Lab Samples: , , , , , METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed 1-Methylnaphthalene ug/l /17/17 03:38 2-Methylnaphthalene ug/l /17/17 03:38 Acenaphthene ug/l /17/17 03:38 Acenaphthylene ug/l /17/17 03:38 Anthracene ug/l /17/17 03:38 Benzo(a)anthracene ug/l /17/17 03:38 Benzo(a)pyrene ug/l /17/17 03:38 Benzo(b)fluoranthene ug/l /17/17 03:38 Benzo(g,h,i)perylene ug/l /17/17 03:38 Benzo(k)fluoranthene ug/l /17/17 03:38 Chrysene ug/l /17/17 03:38 Dibenz(a,h)anthracene ug/l /17/17 03:38 Fluoranthene ug/l /17/17 03:38 Fluorene ug/l /17/17 03:38 Indeno(1,2,3-cd)pyrene ug/l /17/17 03:38 Naphthalene ug/l /17/17 03:38 Phenanthrene ug/l /17/17 03:38 Pyrene ug/l /17/17 03:38 2-Fluorobiphenyl (S) % /17/17 03:38 Terphenyl-d14 (S) % /17/17 03:38 Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits 1-Methylnaphthalene ug/l Methylnaphthalene ug/l Acenaphthene ug/l Acenaphthylene ug/l Anthracene ug/l Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l Chrysene ug/l Dibenz(a,h)anthracene ug/l Fluoranthene ug/l Fluorene ug/l Indeno(1,2,3-cd)pyrene ug/l Naphthalene ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 53 of 69

110 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Phenanthrene ug/l Pyrene ug/l Fluorobiphenyl (S) % Terphenyl-d14 (S) % Qualifiers MATRIX SPIKE SAMPLE: nits Spike Conc. MS MS % Rec % Rec Limits 1-Methylnaphthalene ug/l Methylnaphthalene ug/l Acenaphthene ug/l Acenaphthylene ug/l Anthracene ug/l Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l Chrysene ug/l Dibenz(a,h)anthracene ug/l Fluoranthene ug/l Fluorene ug/l Indeno(1,2,3-cd)pyrene ug/l Naphthalene ug/l Phenanthrene ug/l Pyrene ug/l Fluorobiphenyl (S) % Terphenyl-d14 (S) % Qualifiers SAMPLE DPLICATE: nits Dup 1-Methylnaphthalene ug/l Methylnaphthalene ug/l Acenaphthene ug/l Acenaphthylene ug/l Anthracene ug/l Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l Chrysene ug/l Dibenz(a,h)anthracene ug/l RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 54 of 69

111 #=QC# QALITY CONTROL DATA SAMPLE DPLICATE: nits Dup Fluoranthene ug/l Fluorene ug/l Indeno(1,2,3-cd)pyrene ug/l Naphthalene ug/l Phenanthrene ug/l Pyrene ug/l Fluorobiphenyl (S) % Terphenyl-d14 (S) % RPD Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 55 of 69

112 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3510 Associated Lab Samples: Analysis Method: Analysis Description: EPA 8270 by SIM 8270 Water PAHLV by SIM MSSV METHOD BLANK: Associated Lab Samples: nits Blank Matrix: Water Reporting Limit MDL Analyzed 1-Methylnaphthalene ug/l /19/17 13:01 2-Methylnaphthalene ug/l /19/17 13:01 Acenaphthene ug/l /19/17 13:01 Acenaphthylene ug/l /19/17 13:01 Anthracene ug/l /19/17 13:01 Benzo(a)anthracene ug/l /19/17 13:01 Benzo(a)pyrene ug/l /19/17 13:01 Benzo(b)fluoranthene ug/l /19/17 13:01 Benzo(g,h,i)perylene ug/l /19/17 13:01 Benzo(k)fluoranthene ug/l /19/17 13:01 Chrysene ug/l /19/17 13:01 Dibenz(a,h)anthracene ug/l /19/17 13:01 Fluoranthene ug/l /19/17 13:01 Fluorene ug/l /19/17 13:01 Indeno(1,2,3-cd)pyrene ug/l /19/17 13:01 Naphthalene ug/l /19/17 13:01 Phenanthrene ug/l /19/17 13:01 Pyrene ug/l /19/17 13:01 2-Fluorobiphenyl (S) % /19/17 13:01 Terphenyl-d14 (S) % /19/17 13:01 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: nits Spike Conc LCS LCSD LCS LCSD % Rec % Rec % Rec Limits RPD 1-Methylnaphthalene ug/l Methylnaphthalene ug/l Acenaphthene ug/l Acenaphthylene ug/l Anthracene ug/l Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l Chrysene ug/l Dibenz(a,h)anthracene ug/l Fluoranthene ug/l Fluorene ug/l Indeno(1,2,3-cd)pyrene ug/l Naphthalene ug/l Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 56 of 69

113 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE & LCSD: nits Spike Conc LCS LCSD LCS LCSD % Rec % Rec % Rec Limits RPD Phenanthrene ug/l Pyrene ug/l Fluorobiphenyl (S) % Terphenyl-d14 (S) % Max RPD Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 57 of 69

114 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3510 Analysis Method: Analysis Description: EPA Water MSSV Associated Lab Samples: , , , , , METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed 1,2,4-Trichlorobenzene ug/l /17/17 13:37 1,2-Dichlorobenzene ug/l /17/17 13:37 1,2-Dinitrobenzene ug/l /17/17 13:37 1,2-Diphenylhydrazine ug/l /17/17 13:37 1,3-Dichlorobenzene ug/l /17/17 13:37 1,3-Dinitrobenzene ug/l /17/17 13:37 1,4-Dichlorobenzene ug/l /17/17 13:37 1-Methylnaphthalene ug/l /17/17 13:37 2,3,4,6-Tetrachlorophenol ug/l /17/17 13:37 2,3,5,6-Tetrachlorophenol ug/l /17/17 13:37 N2 2,4,5-Trichlorophenol ug/l /17/17 13:37 2,4,6-Trichlorophenol ug/l /17/17 13:37 2,4-Dichlorophenol ug/l /17/17 13:37 2,4-Dimethylphenol ug/l /17/17 13:37 2,4-Dinitrophenol ug/l /17/17 13:37 2,4-Dinitrotoluene ug/l /17/17 13:37 2,6-Dinitrotoluene ug/l /17/17 13:37 2-Chloronaphthalene ug/l /17/17 13:37 2-Chlorophenol ug/l /17/17 13:37 2-Methylnaphthalene ug/l /17/17 13:37 2-Methylphenol(o-Cresol) ug/l /17/17 13:37 2-Nitroaniline ug/l /17/17 13:37 2-Nitrophenol ug/l /17/17 13:37 3&4-Methylphenol(m&p Cresol) ug/l /17/17 13:37 3,3'-Dichlorobenzidine ug/l /17/17 13:37 3-Nitroaniline ug/l /17/17 13:37 4,6-Dinitro-2-methylphenol ug/l /17/17 13:37 4-Bromophenylphenyl ether ug/l /17/17 13:37 4-Chloro-3-methylphenol ug/l /17/17 13:37 4-Chloroaniline ug/l /17/17 13:37 4-Chlorophenylphenyl ether ug/l /17/17 13:37 4-Nitroaniline ug/l /17/17 13:37 4-Nitrophenol ug/l /17/17 13:37 Acenaphthene ug/l /17/17 13:37 Acenaphthylene ug/l /17/17 13:37 Aniline ug/l /17/17 13:37 Anthracene ug/l /17/17 13:37 Benzidine ug/l /17/17 13:37 Benzo(a)anthracene ug/l /17/17 13:37 Benzo(a)pyrene ug/l /17/17 13:37 Benzo(b)fluoranthene ug/l /17/17 13:37 Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 58 of 69

115 #=QC# QALITY CONTROL DATA METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed Benzo(g,h,i)perylene ug/l /17/17 13:37 Benzo(k)fluoranthene ug/l /17/17 13:37 Benzyl alcohol ug/l /17/17 13:37 bis(2-chloroethoxy)methane ug/l /17/17 13:37 bis(2-chloroethyl) ether ug/l /17/17 13:37 bis(2-chloroisopropyl) ether ug/l /17/17 13:37 bis(2-ethylhexyl)phthalate ug/l /17/17 13:37 Butylbenzylphthalate ug/l /17/17 13:37 Caprolactam ug/l /17/17 13:37 N2 Carbazole ug/l /17/17 13:37 Chrysene ug/l /17/17 13:37 Di-n-butylphthalate ug/l /17/17 13:37 Di-n-octylphthalate ug/l /17/17 13:37 Dibenz(a,h)anthracene ug/l /17/17 13:37 Dibenzofuran ug/l /17/17 13:37 Diethylphthalate ug/l /17/17 13:37 Dimethylphthalate ug/l /17/17 13:37 Fluoranthene ug/l /17/17 13:37 Fluorene ug/l /17/17 13:37 Hexachloro-1,3-butadiene ug/l /17/17 13:37 Hexachlorobenzene ug/l /17/17 13:37 Hexachlorocyclopentadiene ug/l /17/17 13:37 Hexachloroethane ug/l /17/17 13:37 Indeno(1,2,3-cd)pyrene ug/l /17/17 13:37 Isophorone ug/l /17/17 13:37 N-Nitroso-di-n-propylamine ug/l /17/17 13:37 N-Nitrosodimethylamine ug/l /17/17 13:37 N-Nitrosodiphenylamine ug/l /17/17 13:37 Naphthalene ug/l /17/17 13:37 Nitrobenzene ug/l /17/17 13:37 Pentachlorophenol ug/l /17/17 13:37 Phenanthrene ug/l /17/17 13:37 Phenol ug/l /17/17 13:37 Pyrene ug/l /17/17 13:37 Pyridine ug/l /17/17 13:37 2,4,6-Tribromophenol (S) % /17/17 13:37 2-Fluorobiphenyl (S) % /17/17 13:37 2-Fluorophenol (S) % /17/17 13:37 Nitrobenzene-d5 (S) % /17/17 13:37 Phenol-d6 (S) % /17/17 13:37 Terphenyl-d14 (S) % /17/17 13:37 Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 59 of 69

116 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits 1,2,4-Trichlorobenzene ug/l ,2-Dichlorobenzene ug/l ,2-Dinitrobenzene ug/l ,2-Diphenylhydrazine ug/l ,3-Dichlorobenzene ug/l ,3-Dinitrobenzene ug/l ,4-Dichlorobenzene ug/l Methylnaphthalene ug/l ,3,4,6-Tetrachlorophenol ug/l ,3,5,6-Tetrachlorophenol ug/l N2 2,4,5-Trichlorophenol ug/l ,4,6-Trichlorophenol ug/l ,4-Dichlorophenol ug/l ,4-Dimethylphenol ug/l ,4-Dinitrophenol ug/l ,4-Dinitrotoluene ug/l ,6-Dinitrotoluene ug/l Chloronaphthalene ug/l Chlorophenol ug/l Methylnaphthalene ug/l Methylphenol(o-Cresol) ug/l Nitroaniline ug/l Nitrophenol ug/l &4-Methylphenol(m&p Cresol) ug/l ,3'-Dichlorobenzidine ug/l Nitroaniline ug/l ,6-Dinitro-2-methylphenol ug/l Bromophenylphenyl ether ug/l Chloro-3-methylphenol ug/l Chloroaniline ug/l Chlorophenylphenyl ether ug/l Nitroaniline ug/l Nitrophenol ug/l Acenaphthene ug/l Acenaphthylene ug/l Aniline ug/l Anthracene ug/l Benzidine ug/l I Benzo(a)anthracene ug/l Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l Benzo(k)fluoranthene ug/l J(L1) Benzyl alcohol ug/l bis(2-chloroethoxy)methane ug/l bis(2-chloroethyl) ether ug/l bis(2-chloroisopropyl) ether ug/l Qualifiers s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 60 of 69

117 #=QC# QALITY CONTROL DATA LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Qualifiers bis(2-ethylhexyl)phthalate ug/l Butylbenzylphthalate ug/l Caprolactam ug/l J(L1),N2 Carbazole ug/l Chrysene ug/l Di-n-butylphthalate ug/l Di-n-octylphthalate ug/l Dibenz(a,h)anthracene ug/l Dibenzofuran ug/l Diethylphthalate ug/l Dimethylphthalate ug/l Fluoranthene ug/l Fluorene ug/l Hexachloro-1,3-butadiene ug/l Hexachlorobenzene ug/l Hexachlorocyclopentadiene ug/l Hexachloroethane ug/l Indeno(1,2,3-cd)pyrene ug/l Isophorone ug/l N-Nitroso-di-n-propylamine ug/l N-Nitrosodimethylamine ug/l N-Nitrosodiphenylamine ug/l Naphthalene ug/l Nitrobenzene ug/l Pentachlorophenol ug/l Phenanthrene ug/l Phenol ug/l Pyrene ug/l Pyridine ug/l ,4,6-Tribromophenol (S) % Fluorobiphenyl (S) % Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terphenyl-d14 (S) % MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,2,4-Trichlorobenzene ug/l ,2-Dichlorobenzene ug/l ,2-Dinitrobenzene ug/l ,2-Diphenylhydrazine ug/l ,3-Dichlorobenzene ug/l Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 61 of 69

118 #=QC# QALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD 1,3-Dinitrobenzene ug/l ,4-Dichlorobenzene ug/l Methylnaphthalene ug/l ,3,4,6-Tetrachlorophenol ug/l ,3,5,6-Tetrachlorophenol ug/l N2 2,4,5-Trichlorophenol ug/l ,4,6-Trichlorophenol ug/l ,4-Dichlorophenol ug/l ,4-Dimethylphenol ug/l ,4-Dinitrophenol ug/l J(R1) 2,4-Dinitrotoluene ug/l ,6-Dinitrotoluene ug/l Chloronaphthalene ug/l Chlorophenol ug/l Methylnaphthalene ug/l Methylphenol(o-Cresol) ug/l Nitroaniline ug/l Nitrophenol ug/l &4-Methylphenol(m&p ug/l Cresol) 3,3'-Dichlorobenzidine ug/l Nitroaniline ug/l ,6-Dinitro-2-methylphenol ug/l Bromophenylphenyl ether ug/l Chloro-3-methylphenol ug/l Chloroaniline ug/l Chlorophenylphenyl ether ug/l Nitroaniline ug/l Nitrophenol ug/l Acenaphthene ug/l Acenaphthylene ug/l Aniline ug/l Anthracene ug/l Benzidine ug/l I J(M1) Benzo(a)anthracene ug/l J(M1) Benzo(a)pyrene ug/l Benzo(b)fluoranthene ug/l Benzo(g,h,i)perylene ug/l J(M1) Benzo(k)fluoranthene ug/l J(M0) Benzyl alcohol ug/l bis(2-chloroethoxy)methane ug/l bis(2-chloroethyl) ether ug/l bis(2-chloroisopropyl) ether ug/l bis(2-ethylhexyl)phthalate ug/l 12.4 I Butylbenzylphthalate ug/l Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 62 of 69

119 #=QC# QALITY CONTROL DATA MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Caprolactam ug/l J(M0), N2 Carbazole ug/l J(M1) Chrysene ug/l Di-n-butylphthalate ug/l Di-n-octylphthalate ug/l Dibenz(a,h)anthracene ug/l Dibenzofuran ug/l Diethylphthalate ug/l Dimethylphthalate ug/l Fluoranthene ug/l J(M1) Fluorene ug/l Hexachloro-1,3-butadiene ug/l Hexachlorobenzene ug/l Hexachlorocyclopentadiene ug/l Hexachloroethane ug/l Indeno(1,2,3-cd)pyrene ug/l Isophorone ug/l N-Nitroso-di-n-propylamine ug/l N-Nitrosodimethylamine ug/l N-Nitrosodiphenylamine ug/l Naphthalene ug/l Nitrobenzene ug/l Pentachlorophenol ug/l Phenanthrene ug/l Phenol ug/l Pyrene ug/l Pyridine ug/l ,4,6-Tribromophenol (S) % Fluorobiphenyl (S) % Fluorophenol (S) % Nitrobenzene-d5 (S) % Phenol-d6 (S) % Terphenyl-d14 (S) % Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 63 of 69

120 #=QC# QALITY CONTROL DATA QC Batch: QC Batch Method: EPA 3510 Analysis Method: Analysis Description: FL-PRO FL-PRO Water Low Volume Associated Lab Samples: , , , , , METHOD BLANK: Associated Lab Samples: , , , , , nits Blank Matrix: Water Reporting Limit MDL Analyzed Petroleum Range Organics mg/l /16/17 14:06 N-Pentatriacontane (S) % /16/17 14:06 o-terphenyl (S) % /16/17 14:06 J(S0) Qualifiers LABORATORY CONTROL SAMPLE: nits Spike Conc. LCS LCS % Rec % Rec Limits Petroleum Range Organics mg/l N-Pentatriacontane (S) % o-terphenyl (S) % Qualifiers MATRIX SPIKE & MATRIX SPIKE DPLICATE: MS Spike nits Conc. MSD Spike Conc MS MSD MS % Rec MSD % Rec Max % Rec Limits RPD RPD Petroleum Range Organics mg/l N-Pentatriacontane (S) % o-terphenyl (S) % J(S0) Qual s presented on this page are in the units indicated by the "nits" column except where an alternate unit is presented to the right of the result. Date: 03/22/ :42 PM without the written consent of. Page 64 of 69

121 #=QL# QALIFIERS DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-p - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-O Pace Analytical Services - Ormond Beach BATCH QALIFIERS Batch: [M5] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. Batch: [M5] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. Batch: [M5] A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. ANALYTE QALIFIERS I 1p 2p C J(L1) J(L2) J(M0) J(M1) The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. Compound was analyzed for but not detected. A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume. Re-extraction or re-analysis could not be performed within method holding time. The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below reporting limits in associated samples. Estimated Value. Analyte recovery in the laboratory control sample (LCS) was above QC limits. s for this analyte in associated samples may be biased high. Estimated Value. Analyte recovery in the laboratory control sample (LCS) was below QC limits. s for this analyte in associated samples may be biased low. Estimated Value. Matrix spike recovery was outside laboratory control limits. Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date: 03/22/ :42 PM without the written consent of. Page 65 of 69

122 #=QL# QALIFIERS ANALYTE QALIFIERS J(R1) J(S0) J(S5) M6 N2 S7 Estimated Value. RPD value was outside control limits. Estimated Value. Surrogate recovery outside laboratory control limits. Estimated Value. Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis). Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. The lab does not hold NELAC/TNI accreditation for this parameter. Surrogate recovery outside control limits (not confirmed by re-analysis). Date: 03/22/ :42 PM without the written consent of. Page 66 of 69

123 #=CR# QALITY CONTROL DATA CROSS REFERENCE TABLE Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch TMW-1 EPA EPA TMW-2 EPA EPA TMW-3 EPA EPA TMW-4 EPA EPA TMW-5 EPA EPA SW-1 EPA EPA TMW-1 EPA FL-PRO TMW-2 EPA FL-PRO TMW-3 EPA FL-PRO TMW-4 EPA FL-PRO TMW-5 EPA FL-PRO SW-1 EPA FL-PRO TMW-1 EPA EPA TMW-2 EPA EPA TMW-3 EPA EPA TMW-4 EPA EPA TMW-5 EPA EPA SW-1 EPA EPA TMW-1 EPA EPA TMW-2 EPA EPA TMW-3 EPA EPA TMW-4 EPA EPA TMW-5 EPA EPA SW-1 EPA EPA TMW-1 EPA EPA 8270 by SIM TMW-1 EPA EPA 8270 by SIM TMW-2 EPA EPA 8270 by SIM TMW-3 EPA EPA 8270 by SIM TMW-4 EPA EPA 8270 by SIM TMW-5 EPA EPA 8270 by SIM SW-1 EPA EPA 8270 by SIM TMW-1 EPA EPA TMW-2 EPA EPA TMW-3 EPA EPA TMW-4 EPA EPA TMW-5 EPA EPA SW-1 EPA EPA TMW-1 EPA TMW-2 EPA TMW-3 EPA TMW-4 EPA TMW-5 EPA SW-1 EPA Date: 03/22/ :42 PM without the written consent of. Page 67 of 69

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