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7 #=CL# LIMS USE: FR - KATI WEIS LIMS OBJECT ID: January 9, 208 Kati Weis Fox 0 50 Satchel Paige Dr. Mobile, AL RE: Project: Mardi Gras Beads Project Pace Project No.: Dear Kati Weis: Enclosed are the analytical results for sample(s) received by the laboratory on January 2, 208. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Ricky Lopez ricky.lopez@pacelabs.com Project Manager Enclosures Page of 4
8 #=CP# CERTIFICATIONS Project: Pace Project No.: Mardi Gras Beads Project New Orleans Certification IDs California Env. Lab Accreditation Program Branch: 277CA Florida Department of Health (NELAC): E87595 Illinois Environmental Protection Agency: Kansas Department of Health and Environment (NELAC): E-0266 Louisiana Dept. of Environmental Quality (NELAC/LELAP): Pennsylviania Dept. of Env Protection (NELAC): Texas Commission on Env. Quality (NELAC): T TX U.S. Dept. of Agriculture Foreign Soil Import: P Commonwealth of Virginia (TNI): Page 2 of 4
9 #=SS# SAMPLE SUMMARY Project: Pace Project No.: Mardi Gras Beads Project Lab ID Sample ID Matrix Date Collected Date Received Toomey's Small Pink Solid 0//8 08:00 0/2/8 09: Toomey's Small Teal Blue Solid 0//8 08:00 0/2/8 09: Toomey's Large Blue Solid 0//8 08:00 0/2/8 09: Toomey's Small Green Solid 0//8 08:00 0/2/8 09: Toomey's Large Purple&Gold Solid 0//8 08:00 0/2/8 09: Toomey's Patriotic Solid 0//8 08:00 0/2/8 09: Toomey's Alligator Solid 0//8 08:00 0/2/8 09: Toomey's Large Gold Metallic Solid 0//8 08:00 0/2/8 09: Toomey's Large Silver Metallic Solid 0//8 08:00 0/2/8 09: Toomey's Metallic Football Solid 0//8 08:00 0/2/8 09: Gulf Coast Small Silver Solid 0//8 08:00 0/2/8 09: Gulf Coast Large Silver Solid 0//8 08:00 0/2/8 09: Gulf Coast Small Gold Solid 0//8 08:00 0/2/8 09: Gulf Coast Large Purple Solid 0//8 08:00 0/2/8 09: Gulf Coast White Masks Solid 0//8 08:00 0/2/8 09: Gulf Coast Large Green&Purple Solid 0//8 08:00 0/2/8 09: Gulf Coast Large Heart Solid 0//8 08:00 0/2/8 09: Gulf Coast Large R, W, P Solid 0//8 08:00 0/2/8 09: Gulf Coast Small Pink&Green Solid 0//8 08:00 0/2/8 09: Gulf Coast Large Red Ball&Dice Solid 0//8 08:00 0/2/8 09:45 Page 3 of 4
10 #=SA# SAMPLE ANALYTE COUNT Project: Pace Project No.: Mardi Gras Beads Project Lab ID Sample ID Method Analysts Analytes Reported Toomey's Small Pink EPA 600 MHB Toomey's Small Teal Blue EPA 600 MHB Toomey's Large Blue EPA 600 MHB Toomey's Small Green EPA 600 MHB Toomey's Large Purple&Gold EPA 600 MHB Toomey's Patriotic EPA 600 MHB Toomey's Alligator EPA 600 MHB Toomey's Large Gold Metallic EPA 600 MHB Toomey's Large Silver Metallic EPA 600 MHB Toomey's Metallic Football EPA 600 MHB Gulf Coast Small Silver EPA 600 MHB Gulf Coast Large Silver EPA 600 MHB Gulf Coast Small Gold EPA 600 MHB Gulf Coast Large Purple EPA 600 MHB Gulf Coast White Masks EPA 600 MHB Gulf Coast Large Green&Purple EPA 600 MHB Gulf Coast Large Heart EPA 600 MHB Gulf Coast Large R, W, P EPA 600 MHB Gulf Coast Small Pink&Green EPA 600 MHB Gulf Coast Large Red Ball&Dice EPA 600 MHB Page 4 of 4
11 #=AR# ANALYTICAL RESULTS Project: Pace Project No.: Mardi Gras Beads Project Sample: Toomey's Small Pink Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 3.9 mg/kg /5/8 0:2 0/6/8 9: Sample: Toomey's Small Teal Blue Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 5.5 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Large Blue Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 7.9 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Small Green Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 4.3 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Large Purple&Gold Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 0.63 mg/kg /5/8 0:2 0/6/8 20: Date: 0/9/208 0:27 AM Page 5 of 4
12 #=AR# ANALYTICAL RESULTS Project: Pace Project No.: Mardi Gras Beads Project Sample: Toomey's Patriotic Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead.5 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Alligator Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead.4 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Large Gold Metallic Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 0.3 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Large Silver Metallic Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 23.4 mg/kg /5/8 0:2 0/6/8 20: Sample: Toomey's Metallic Football Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 4. mg/kg /5/8 0:2 0/6/8 20: Date: 0/9/208 0:27 AM Page 6 of 4
13 #=AR# ANALYTICAL RESULTS Project: Pace Project No.: Mardi Gras Beads Project Sample: Gulf Coast Small Silver Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 2.4 mg/kg /5/8 0:2 0/6/8 20: Sample: Gulf Coast Large Silver Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 2.3 mg/kg /5/8 0:2 0/6/8 20: Sample: Gulf Coast Small Gold Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 8.2 mg/kg /5/8 0:2 0/6/8 20: Sample: Gulf Coast Large Purple Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead.8 mg/kg /5/8 0:2 0/6/8 2: Sample: Gulf Coast White Masks Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead.3 mg/kg /5/8 0:2 0/6/8 2: Date: 0/9/208 0:27 AM Page 7 of 4
14 #=AR# ANALYTICAL RESULTS Project: Pace Project No.: Mardi Gras Beads Project Sample: Gulf Coast Large Green&Purple Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 2. mg/kg /5/8 0:2 0/6/8 2: Sample: Gulf Coast Large Heart Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead.4 mg/kg /5/8 0:2 0/6/8 2: Sample: Gulf Coast Large R, W, P Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 2.5 mg/kg /5/8 0:2 0/6/8 2: Sample: Gulf Coast Small Pink&Green Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 0.60 mg/kg /5/8 0:2 0/6/8 2: Sample: Gulf Coast Large Red Ball&Dice Lab ID: Collected: 0//8 08:00 Received: 0/2/8 09:45 Matrix: Solid 600 Metals, Total Lead 0.39 mg/kg /5/8 0:2 0/6/8 2: Date: 0/9/208 0:27 AM Page 8 of 4
15 #=QC# QUALITY CONTROL DATA Project: Pace Project No.: Mardi Gras Beads Project QC Batch: QC Batch Method: EPA 3050 Analysis Method: Analysis Description: EPA MET Associated Lab Samples: , , , , , , , , , , , , , , , , , , , METHOD BLANK: Associated Lab Samples: , , , , , , , , , , , , , , , , Parameter Matrix: Solid , , , Blank Units Result Reporting Limit Analyzed Lead mg/kg ND /6/8 9:36 Qualifiers LABORATORY CONTROL SAMPLE: Parameter Units Spike Conc. LCS Result LCS % Rec % Rec Limits Lead mg/kg Qualifiers MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MS Spike Parameter Units Result Conc. MSD Spike Conc MS Result MSD Result MS % Rec MSD % Rec Max % Rec Limits RPD RPD Lead mg/kg Qual Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Date: 0/9/208 0:27 AM Page 9 of 4
16 #=QL# QUALIFIERS Project: Pace Project No.: Mardi Gras Beads Project DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The Nelac Institute Date: 0/9/208 0:27 AM Page 0 of 4
17 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Mardi Gras Beads Project Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch Toomey's Small Pink EPA EPA Toomey's Small Teal Blue EPA EPA Toomey's Large Blue EPA EPA Toomey's Small Green EPA EPA Toomey's Large Purple&Gold EPA EPA Toomey's Patriotic EPA EPA Toomey's Alligator EPA EPA Toomey's Large Gold Metallic EPA EPA Toomey's Large Silver Metallic EPA EPA Toomey's Metallic Football EPA EPA Gulf Coast Small Silver EPA EPA Gulf Coast Large Silver EPA EPA Gulf Coast Small Gold EPA EPA Gulf Coast Large Purple EPA EPA Gulf Coast White Masks EPA EPA Gulf Coast Large Green&Purple EPA EPA Gulf Coast Large Heart EPA EPA Gulf Coast Large R, W, P EPA EPA Gulf Coast Small Pink&Green EPA EPA Gulf Coast Large Red Ball&Dice EPA EPA Date: 0/9/208 0:27 AM Page of 4
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