The pooled samples meet the requirements EN 71-3:2013 (migration of certain elements).
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1 SGS INSTITUT FRESENIUS GmbH Postfach Taunusstein Gummiwerk Czermak & Feger Brennbichl IMST/TIROL Österreich Order No Client: Gabriele Göttsch / st t f gabriele.goettsch@sgs.com Consumer Testing Services Hardlines / E&E Chemical Testing Taunusstein, December 19, 2013 SGS INSTITUT FRESENIUS GmbH Im Maisel 14 D Taunusstein Your order : Testing for Nitrosamines EN and testing for EN 71 part 3 Your reference : Ms. Angela Jenewein Order date : 02/DEC/2013 Test period : 05/DEC/ /DEC/2013 Test Report Testing of balloons Dear Ms. Jenewein, Following your request we have tested the sample received on December 3, 2013 for N-Nitrosamines and N-nitrosatable substances according to EN and migration of certain elements according to EN The tests should be carried out on pooled samples. The sample was marked as followed: Sample no. Sample Designation Balloons, assorted colours Detailed results are given on the following page(s). Assessment: The pooled samples meet the requirements of LFGB and Directive 2009/48/EC in the tested item Nitrosamines and nitrosatable substances. The pooled samples meet the requirements EN 71-3:2013 (migration of certain elements). Yours sincerely, SGS INSTITUT FRESENIUS GmbH i.v. Gabriele Göttsch R:\G\Gummiwerk Czermak & Feger\2013\ \ _Luftballons_EN 71-12_TEA und LC_Metalle_engl..doc i.v. Jasmin Digles page 1 of 6
2 Client : Gummiwerk, IMST/TIROL page 2 of 6 Photo documentation Subsample Subsample no. Sample designation Balloon, black Balloon, grey Balloon, orange Balloon, yellow Balloon, dark red Balloon, berry Balloon, pink Balloon, white Balloon, lime-green Balloon, dark green Balloon, lime-blue Balloon, royal blue Balloon, dark blue
3 Client : Gummiwerk, IMST/TIROL page 3 of 6 Test : 1. N-Nitrosamines and N-nitrosatable substances In accordance with: EN-71-12:2013 Migration 1 hour at 40 C Detection method: GC-TEA / NDELA: LC-MS/MS Sample designation: Balloon Colour: black, grey, orange, yellow, dark red, berry, pink Parameter Abbrev. migratable N-nitrosamines migratable, nitrosatable substances Limits of quantification N-Nitrosodimethylamine NDMA N-Nitrosodiethylamine NDEA n. d. n. d N-Nitrosodiisopropylamine NDiPA n. d. n. d N-Nitrosodipropylamine NDPA n. d. n. d N-Nitrosodiisobutylamine NDiBA n. d. n. d N-Nitrosodibutylamin NDBA n. d. n. d N-Nitrosomorpholine NMOR n. d. n. d N-Nitrosopiperidine NPIP n. d. n. d N-Nitrosomethylphenylamine NMPhA n. d. n. d N-Nitrosoethylphenylamine NEPhA n. d. n. d N-Nitrosodiisononylamin NDiNA n. d. n. d N-Nitrosodibenzylamine NDBzA n. d. n. d N-Nitrosodiethanolamin NDELA < 0.01 < Total: Quantity allowed*: max max. 1.0 n. d. = not detectable < LoQ = trace below the limit of quantification *: Requirement for balloons according to Bedarfsgegenstände-Verordnung (German Consumer Goods Ordinance) For the summation of all Nitrosamines only those with a result above the limit of quantification will be taken into account. The sample material has been examined in the condition as received. The results of analysis refer solely to the examined sample specimen!
4 Client : Gummiwerk, IMST/TIROL page 4 of 6 Balloon Colour:white, lime-green, dark green, lime-blue, royal blue and dark blue Parameter Abbrev. migratable N-nitrosamines migratable, nitrosatable substances Limits of quantification N-Nitrosodimethylamine NDMA 0,004 0, N-Nitrosodiethylamine NDEA n. d. n. d N-Nitrosodiisopropylamine NDiPA n. d. n. d N-Nitrosodipropylamine NDPA n. d. n. d N-Nitrosodiisobutylamine NDiBA n. d. n. d N-Nitrosodibutylamin NDBA n. d. n. d N-Nitrosomorpholine NMOR n. d. n. d N-Nitrosopiperidine NPIP n. d. n. d N-Nitrosomethylphenylamine NMPhA n. d. n. d N-Nitrosoethylphenylamine NEPhA n. d. n. d N-Nitrosodiisononylamin NDiNA n. d. n. d N-Nitrosodibenzylamine NDBzA n. d. n. d N-Nitrosodiethanolamin NDELA < 0.01 < Total: Quantity allowed*: max max. 1.0 n. d. = not detectable < LoQ = trace below the limit of quantification *: Requirement for balloons according to Bedarfsgegenstände-Verordnung (German Consumer Goods Ordinance) For the summation of all Nitrosamines only those with a result above the limit of quantification will be taken into account. The sample material has been examined in the condition as received. The results of analysis refer solely to the examined sample specimen!
5 Client : Gummiwerk, IMST/TIROL page 5 of 6 2. Migration of certain elements The soluble elements were determined according to EN 71-3: EN 71-3:2013 category III Aluminium (Al) < 10 < 10 max Arsenic (As) < 1 < 1 max. 47 Boron (B) < 10 < 10 max Barium (Ba) < 10 < 10 max Cadmium (Cd) < 1 < 1 max. 23 Cobalt (Co) < 10 < 10 max. 130 Chrom ges. (Cr) < 0.2 < 0.2 max. 460 Copper (Cu) < 10 < 10 max Manganese (Mn) < 10 < 10 max Nickel (Ni) < 10 < 10 max. 930 Lead (Pb) < 10 < 10 max. 160 Antimony (Sb) < 10 < 10 max. 560 Selenium (Se) < 10 < 10 max. 460 Tin (Sn) < 1 < 1 max Strontium (Sr) < 10 < 10 max Zinc (Zn) max Mercury (Hg) < 1 < 1 max EN 71-3:2013 category III Aluminium (Al) < 10 < 10 max Arsenic (As) < 1 < 1 max. 47 Boron (B) < 10 < 10 max Barium (Ba) < 10 < 10 max Cadmium (Cd) < 1 < 1 max. 23 Cobalt (Co) < 10 < 10 max. 130 Chrom ges. (Cr) < 0.2 < 0.2 max. 460 Copper (Cu) < 10 < 10 max Manganese (Mn) < 10 < 10 max Nickel (Ni) < 10 < 10 max. 930 Lead (Pb) < 10 < 10 max. 160 Antimony (Sb) < 10 < 10 max. 560 Selenium (Se) < 10 < 10 max. 460 Tin (Sn) < 1 < 1 max Strontium (Sr) < 10 < 10 max Zinc (Zn) max Mercury (Hg) < 1 < 1 max. 94
6 Client : Gummiwerk, IMST/TIROL page 6 of EN 71-3:2013 category III Aluminium (Al) < 10 max Arsenic (As) < 1 max. 47 Boron (B) < 10 max Barium (Ba) < 10 max Cadmium (Cd) < 1 max. 23 Cobalt (Co) < 10 max. 130 Chrom ges. (Cr) < 0.2 max. 460 Copper (Cu) < 10 max Manganese (Mn) < 10 max Nickel (Ni) < 10 max. 930 Lead (Pb) < 10 max. 160 Antimony (Sb) < 10 max. 560 Selenium (Se) < 10 max. 460 Tin (Sn) < 1 max Strontium (Sr) < 10 max Zinc (Zn) 290 max Mercury (Hg) < 1 max. 94 SGS INSTITUT FRESENIUS GmbH i.v. Gabriele Göttsch i.v. Jasmin Digles
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