AR-17-SF

Transcription

1 Eurofins Sofia GmbH Rudower Chaussee Berlin GERMANY Tel: Fax: Control Union Certifications B.V. attn. Reports Meeuwenlaan BZ Zwolle NIEDERLANDE {E411D42C-BDF5-4A96-BDD3-475D388FB Analytical report Person in charge ASM AR-17-SF Mrs. F. Fuchs Mrs. F. Fuchs Report date Sample Code Reference Walnuts (green, fresh, from tree) Sample sender Control Union Certifications Prescriber Reports Reception date time Transport by DHL Client sample code Start analysis End analysis ÌAR-17-SF-Ç%F/È-01!Î Analysis Testcode Method SFFET / PSFFL 64 LFGB L , mod. SFFED / PSFFL 64 LFGB L , mod. Page 1/11

2 Test results Parameter Measurement Unit Result LOQ SFFED: LC-MS/MS [LC-MS/MS] // LA-LCMS-030 (#) Screened pesticides SFFET: GC-MS [GC-MS] // LA-GCMS-006 (#) Screened pesticides LC-MS/MS [LC-MS/MS] GC-MS [GC-MS] <LOQ <LOQ LOQ = Limit of Quantification <LOQ = below limit of quantification (#) = SOFIA (Berlin) is accredited for this test. MRL = Maximum Residue Level Signature Page 2/11

3 List of analysed substances: SFFED 2,4'-Formoxylidid (Amitraz Metabolite) Hydroxycarbofuran Chlor-3-phenylpyridazin-4-ol 0.01 Abamectin 0.01 Acephate 0.01 Acetamiprid 0.01 Acetochlor 0.02 Alachlor 0.01 Aldicarb 0.01 Aldicarb-sulfone 0.01 Aldicarb-sulfoxide 0.01 Ametoctradin 0.01 Ametryn 0.01 Amidosulfuron 0.01 Aminocarb 0.01 Amitraz 0.01 Ancymidol 0.01 Atrazin, desethyl Atrazine 0.01 Azaconazole 0.01 Azamethiphos 0.01 Aziprotryn 0.01 Azoxystrobin 0.01 Benalaxyl 0.01 Bendiocarb 0.01 Benfuracarb 0.01 Benodanil 0.01 Benomyl 0.01 Bensulfuron methyl 0.01 Benthiavalicarb, isopropyl Bitertanol 0.01 Boscalid 0.01 Bromacil 0.01 Bupirimate 0.01 Buprofezin 0.01 Butocarboxim 0.01 Butocarboxim-sulfoxide 0.01 Butoxycarboxim 0.01 Buturon 0.01 Cadusaphos 0.01 Carbaryl 0.01 Carbendazim 0.01 Carbofuran 0.01 Carbosulfan 0.01 Carboxin 0.01 Chlorantraniliprole 0.01 Chlorbromuron 0.01 Chlorfluazuron 0.01 Chloridazone 0.01 Chlorotoluron 0.01 Chloroxuron 0.01 Chlorpropham 0.05 Chlorsulfuron 0.01 Cinidon-ethyl 0.05 Cinosulfuron 0.01 Clethodim 0.01 Clodinafop-propargyl 0.01 Clofentezine 0.01 Clomazone 0.01 Clothianidin 0.01 Cyanazine 0.01 Cyazofamid 0.01 Cymoxanil 0.02 Cyproconazole 0.01 Cyprodinil 0.01 Cyprofuram 0.01 Page 3/11

4 SFFED Cyromazine 0.01 Demeton 0.01 Demeton-S-methyl 0.01 Demeton-S-methyl-sulfone 0.01 Desmedipham 0.01 Desmetryn 0.01 Diazinon 0.01 Dichlorvos 0.01 Diclobutrazol 0.01 Diethofencarb 0.01 Diethyltoluamide 0.01 Difenoconazole 0.01 Difenoxuron 0.01 Diflubenzuron 0.01 Diflufenican 0.01 Dimefox 0.01 Dimefuron 0.01 Dimethenamid 0.01 Dimethoate 0.01 Dimethomorph 0.01 Dimetilan 0.01 Dimoxystrobin 0.01 Dinotefuran 0.02 Disulfoton 0.01 Disulfoton-sulfon 0.01 Disulfoton-sulfoxide 0.01 Diuron 0.01 Emamectin (Sum) 0.01 Epoxiconazole 0.01 Ethiofencarb 0.01 Ethiofencarb-sulfone 0.01 Ethiofencarb-sulfoxide 0.01 Ethiprole 0.01 Ethofumesat-2-keto 0.05 Ethofumesate 0.01 Ethoprophos 0.01 Etofenprox 0.01 Etoxazole 0.01 Famoxadone 0.01 Fenamidone 0.01 Fenamiphos 0.01 Fenamiphos-sulfone 0.01 Fenamiphos-sulfoxide 0.01 Fenarimol 0.01 Fenazaquin 0.01 Fenbuconazole 0.01 Fenhexamid 0.01 Fenobucarb 0.01 Fenoxaprop-ethyl 0.01 Fenoxycarb 0.01 Fenpiclonil 0.01 Fenpropidin 0.01 Fenpropimorph 0.01 Fenpyroximate 0.01 Fensulfothion 0.01 Fensulfothion-oxon-sulfone 0.01 Fensulfothion-oxon-sulfoxide 0.01 Fensulfothion-sulfone 0.01 Fenthion 0.01 Fenthion-oxon 0.01 Fenthion-oxon-sulfone 0.01 Fenthion-oxon-sulfoxide 0.01 Fenthion-sulfone 0.01 Fenthion-sulfoxide 0.01 Fenuron 0.01 Flazasulfuron 0.01 Flonicamid 0.01 Florasulam 0.01 Fluazifop-P-butyl 0.01 Fluazuron 0.02 Flucycloxuron 0.01 Fludioxonil 0.01 Flufenacet 0.01 Flufenoxuron 0.01 Fluometuron 0.01 Fluopicolid 0.01 Page 4/11

5 SFFED Flurochloridone 0.01 Flurprimidol 0.01 Flusilazole 0.01 Flutriafol 0.01 FM Formetanate 0.01 Fosthiazate 0.01 Fuberidazole 0.01 Furathiocarb 0.01 Halofenozide 0.01 Haloxyfop-2-ethoxyethyl 0.01 Haloxyfop-methyl 0.01 Hexaconazole 0.01 Hexaflumuron 0.05 Hexazinone 0.01 Hexythiazox 0.01 Imazalil 0.01 Imibenconazole 0.01 Imidacloprid 0.01 Indoxacarb 0.01 Iodosulfuron methyl 0.01 Iprovalicarb 0.01 Isoprocarb 0.01 Isoprothiolane 0.01 Isoproturon 0.01 Isoxaben 0.01 Isoxaflutole 0.01 Isoxathion 0.01 Lenacil 0.01 Linuron 0.01 Lufenuron 0.05 Malaoxon 0.01 Malathion 0.01 Mandipropamid 0.01 Mepanipyrim 0.01 Metalaxyl 0.01 Metamitron 0.01 Metazachlor 0.01 Metconazole 0.01 Methabenzthiazuron 0.01 Methacriphos 0.01 Methamidophos 0.01 Methidathion 0.01 Methiocarb 0.01 Methiocarb-sulfone 0.01 Methiocarb-sulfoxide 0.01 Methomyl 0.01 Methoprotryne 0.01 Methoxyfenozide 0.01 Metobromuron 0.01 Metolachlor 0.01 Metolcarb 0.01 Metoxuron 0.01 Metrafenone 0.01 Metribuzin 0.01 Metsulfuron-methyl 0.01 Molinate 0.01 Monocrotophos 0.01 Monolinuron 0.01 Monuron 0.01 N-2,4-dimethylphenyl-N-methylforma 0.05 Napropamide 0.01 midine Neburon 0.01 Nicosulfuron 0.01 Novaluron 0.02 Nuarimol 0.01 Ofurace 0.01 Omethoate 0.01 Orbencarb 0.01 Oxadixyl 0.01 Oxamyl 0.01 Oxamyl-oxime 0.01 Oxydemeton-methyl 0.01 Paclobutrazol 0.01 Page 5/11

6 SFFED Paraoxon-ethyl 0.01 Paraoxon-methyl 0.01 Penconazole 0.01 Pencycuron 0.01 Pendimethalin 0.01 Pentanochlor 0.01 Phenmedipham 0.01 Phorate 0.05 Phorate-sulfone 0.01 Phorate-sulfoxide 0.01 Phosphamidon 0.01 Phoxim 0.01 Picoxystrobin 0.01 Piperonyl butoxide 0.01 Pirimicarb 0.01 Pirimicarb, desmethyl Pirimicarb, desmethyl-formamido Primisulfuron-methyl 0.02 Prochloraz 0.01 Promecarb 0.01 Prometon 0.01 Prometryn 0.01 Propamocarb 0.01 Propargite 0.01 Propazine 0.01 Propham 0.05 Propiconazole 0.01 Propoxur 0.01 Propoxycarbazone 0.02 Proquinazid 0.01 Prosulfocarb 0.01 Prosulfuron 0.01 Pymetrozine 0.01 Pyraclostrobin 0.01 Pyraflufen-ethyl 0.01 Pyrethrins 0.1 Pyridate 0.05 Pyrimethanil 0.01 Pyrimidifen 0.01 Pyriproxyfen 0.01 Quizalofop ethyl 0.01 Rabenzazole 0.01 Rimsulfuron 0.05 Rotenone 0.01 Sebuthylazine 0.01 Sethoxydim 0.01 Silafluofen 0.02 Simazine 0.01 Simazine, desethyl Simeconazole 0.01 Spinosad 0.02 Spirodiclofen 0.01 Spiromesifen 0.01 Spirotetramat 0.01 Spiroxamine 0.01 Tebuconazole 0.01 Tebufenozide 0.01 Tebufenpyrad 0.01 Teflubenzuron 0.05 TEPP 0.01 Terbacil 0.01 Terbufos 0.01 Terbufos-sulfone 0.01 Terbufos-sulfoxide 0.01 Terbuthylazine 0.01 Terbuthylazine, desethyl Terbutryn 0.01 Tetraconazole 0.01 Thiabendazole 0.01 Thiabendazole, 5-hydroxy Thiacloprid 0.01 Thiamethoxam 0.01 Thiazafluron 0.01 Thifensulfuron methyl 0.01 Thiocarbazil 0.01 Thiodicarb 0.01 Page 6/11

7 SFFED Thiofanox 0.05 Thiofanox-sulfone 0.01 Thiofanox-sulfone 0.01 Thiofanox-sulfoxide 0.01 Thiofanox-sulfoxide 0.01 Thionazin 0.01 Thiophanate (-ethyl) 0.01 Thiophanate-methyl 0.01 Triadimefon 0.01 Triadimenol 0.01 Triamiphos 0.01 Triasulfuron 0.01 Triazamate 0.01 Triazophos 0.01 Tribenuron-methyl 0.01 Trichlorfon 0.02 Tricyclazole 0.01 Tridemorph 0.1 Trietazine 0.01 Trifloxystrobin 0.01 Trifloxysulfuron 0.01 Triflumizole 0.01 Triflumuron 0.01 Triflusulfuron-methyl 0.05 Triforine 0.01 Trimethycarb, 3,4, Triticonazole 0.01 Uniconazole 0.01 Vamidothion 0.01 Vamidothion-sulfone 0.01 Vamidothion-sulfoxide 0.01 Zoxamide 0.01 SFFET 2,4,5-T-Methylester ,4-D-Methylester 0.1 Acetochlor 0.02 Aclonifen 0.02 Acrinathrin 0.01 Alachlor 0.1 Aldrin Allethrin 0.03 Amidithion 0.03 Atrazine 0.1 Azaconazole 0.02 Azinphos-ethyl 0.01 Azinphos-methyl 0.01 Azoxystrobin 0.01 Benfluralin Benoxacor 0.01 Benzoylprop-ethyl 0.01 Bifenox 0.01 Bifenthrin Binapacryl 0.02 Bitertanol 0.1 Boscalid 0.02 Bromfenvinphos 0.01 Bromocyclen 0.01 Bromophos-ethyl Bromophos-methyl Bromopropylate 0.01 Buprofezin 0.05 Butachlor 0.1 Butamifos 0.01 Butralin 0.01 Cadusaphos 0.01 Page 7/11

8 SFFET Captafol 0.02 Captan 0.02 Carbophenothion Carbophenothion-methyl 0.01 Carfentrazone-ethyl 0.01 Chinomethionate 0.01 Chlorbenside Chlordane, cis Chlordane, oxy Chlordane, trans Chlorethoxyfos 0.01 Chlorfenapyr Chlorfenprop-methyl Chlorfenson Chlorfenvinphos 0.02 Chloridazone 0.1 Chlormephos Chloroneb 0.1 Chloropropylate Chlorothalonil Chlorpyrifos (-ethyl) Chlorpyrifos-methyl Chlorthal-dimethyl Chlorthion 0.01 Chlorthiophos Chlozolinate Cinidon-ethyl 0.05 Clodinafop-propargyl 0.05 Coumaphos Crotoxyphos 0.01 Cyanofenphos Cyanophos 0.01 Cyfluthrin Cyhalothrin Cyhalothrin, lambda Cypermethrin Cyphenothrin 0.01 Cyproconazole 0.05 DDD, o,p DDE, o,p DDT 0.01 Deltamethrin 0.01 (p,p'-ddt+o,p'-ddt+p,p'-dde+p,p'-t DE) Dialifos 0.01 Diallate 0.01 Diazinon 0.01 Dibromobenzophenone, p,p Dicapthon 0.01 Dichlobenil 0.02 Dichlofenthion Dichlofluanid 0.01 Diclofop-methyl 0.01 Dicloran Dicofol, o,p Dicofol, p,p Dicrotophos 0.01 Dieldrin 0.01 Difenoconazole 0.01 Diflufenican 0.01 Dimethachlor 0.1 Dimethipin Dimethoate 0.02 Dimethomorph 0.05 Diniconazole 0.01 Dinitramine 0.01 Disulfoton 0.01 Disulfoton-sulfon 0.02 Disulfoton-sulfoxide 0.05 Ditalimfos Edifenphos 0.02 Endosulfan sulphate Endosulfan, alpha Endosulfan, beta Page 8/11

9 SFFET Endrin 0.01 EPN 0.01 Epoxiconazole Etaconazole 0.01 Ethalfluralin Ethion Ethiprole 0.01 Ethofumesate 0.2 Ethoprophos Etridiazole Etrimfos Famophos 0.02 Famoxadone 0.01 Fenamidone 0.01 Fenamiphos 0.02 Fenarimol 0.02 Fenbuconazole 0.02 Fenchlorazole-ethyl 0.02 Fenchlorphos Fenfluthrin 0.01 Fenhexamid 0.01 Fenitrothion Fenoxaprop-ethyl 0.05 Fenpiclonil 0.05 Fenpropathrin Fenpropimorph 0.1 Fenson Fensulfothion 0.01 Fenvalerate (RR-/SS-Isomers) Fenvalerate (RS-/SR-Isomers) Fipronil Fipronil, desulfinyl Fipronil-sulfide Fipronil-sulfone Flamprop-isopropyl 0.02 Flamprop-methyl 0.02 Flonicamid 0.05 Fluazifop-butyl 0.1 Fluazinam 0.02 Fluchloralin Flucythrinate 0.01 Flufenoxuron 0.01 Flumethrine 0.1 Flumetralin Fluopicolid 0.01 Fluorodifen Fluotrimazole 0.01 Fluquinconazole 0.01 Flurenol-butyl 0.01 Flurochloridone 0.02 Flurtamone 0.01 Flusilazole 0.1 Folpet Fonofos Formothion Genite 0.02 Halfenprox Haloxyfop-2-ethoxyethyl 0.01 Haloxyfop-methyl 0.02 HCH, alpha HCH, beta HCH, delta HCH, epsilon Heptachlor Heptachlor epoxide, cis Heptachlor epoxide, trans Heptenophos Hexachlorobenzene (HCB) Hexaconazole Indanofan 0.02 Indoxacarb 0.01 Iodofenphos Ioxynil-octanoate 0.02 Iprobenfos 0.01 Iprodione 0.02 Isazophos 0.02 Page 9/11

10 SFFET Isobenzan Isocarbofos Isodrin Isofenphos Isofenphos-methyl Isomethiozin Isopropalin Isoxadifen-ethyl 0.01 Kresoxim-methyl 0.01 Lactofen 0.01 Leptophos 0.01 Lindane (gamma-hch) Lufenuron 0.02 Malaoxon 0.02 Malathion Mecarbam 0.01 Mephosfolan 0.01 Merphos 0.01 Metazachlor 0.1 Methacriphos Methidathion 0.02 Methoxychlor 0.05 Metolachlor 0.1 Metrafenone 0.01 Metribuzin 0.01 Mirex 0.01 Molinate 0.1 Myclobutanil 0.01 Nitralin 0.01 Nitrapyrin 0.02 Nitrofen 0.01 Nitrothal-isopropyl 0.02 Norflurazon Nuarimol 0.01 Omethoate 0.1 Oxadiazon 0.01 Oxydemeton-methyl 0.02 Oxyfluorfen Paclobutrazol 0.01 Paraoxon-ethyl 0.02 Paraoxon-methyl 0.02 Parathion 0.01 Parathion-methyl 0.01 PCB PCB PCB PCB PCB PCB Penconazole 0.01 Pendimethalin 0.01 Pentachloranisole Pentachloroaniline 0.01 Pentachlorobenzene Permethrin 0.02 Perthane 0.1 Phenkapton 0.01 Phenothrin 0.05 Phenthoate 0.01 Phosalone 0.01 Phosfolan 0.01 Phosmet 0.01 Picolinafen 0.01 Picoxystrobin 0.01 Piperophos 0.05 Pirimiphos-ethyl 0.01 Pirimiphos-methyl 0.01 Plifenate 0.01 Prallethrin 0.02 Procymidone 0.04 Profenofos Profluralin Propachlor 0.1 Propanil 0.01 Propazine 0.05 Propetamphos Page 10/11

11 SFFET Propiconazole 0.01 Propyzamide 0.02 Prothiofos Prothoate 0.01 Pyraflufen-ethyl 0.02 Pyrazophos 0.01 Pyrethrins 0.02 Pyridaben 0.01 Pyridaphenthion 0.01 Pyrifenox 0.02 Pyrimitate 0.05 Quinalphos Quinoxyfen 0.02 Quintozene Quizalofop ethyl 0.02 Resmethrin 0.1 S Spiromesifen 0.02 Sulfotep Sulprofos 0.01 Swep 0.1 tau-fluvalinate Tebupirimfos 0.01 Tecnazene Tefluthrin Temephos 0.01 Terbufos Tetrachlorvinphos Tetraconazole 0.01 Tetradifon Tetramethrin 0.01 Tetrasul 0.01 Tolclofos-methyl Tolylfluanid 0.01 Toxaphene Parlar Toxaphene Parlar Toxaphene Parlar Transfluthrin 0.01 Triadimefon 0.01 Triadimenol 0.1 Triallate 0.01 Triamiphos Triazophos 0.02 Tribufos Trichloronat Tridiphane 0.05 Trifloxystrobin 0.01 Trifluralin Vamidothion Vinclozolin Page 11/11