Electronics and Signal Processing in Four Parts Stoll, Che380. Part I Basic Electronics

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1 Electronics and Signal Processing in Four Parts Stoll, Che380 Part I Basic Electronics

2 Skoog, Holler, Crouch, 7 th Ed.

3 Skoog, Holler, Crouch, 7 th Ed.

4 Skoog, Holler, Crouch, 7 th Ed.

5 Skoog, Holler, Crouch, 7 th Ed.

6 Some objectives for our study of electronics and signal processing 1. Be able to define the four laws and apply them to explain the behavior of an electrical circuit (Power Law, Ohm s Law, and Kirchoff s Current and Voltage Laws) 2. Be able to explain, in quantitative terms, the problems that arise in measuring small currents and voltages in instrumentation 3. Be able to explain the valuable characteristics of operational amplifiers for use in instrumentation, and describe the specific circuits used for current and voltage measurements 4. Be able to describe circuits used for signal processing in the analog domain, and predict their behavior in quantitative terms 5. Be able to describe approaches used for signal processing in the digital domain, and prescribe a particular approach when presented with a real instrument signal 6. Be able to describe the characteristics of an analog-to-digital converter, in quantitative terms 7. Be able to describe the concept of Fourier analysis, by showing the relationships between a raw analog signal, a power spectrum, and a reconstructed signal produced using an inverse Fourier transform

7 Complete the following table (including units):

8 For each of the following, write down both an equation and a statement that describes the meaning of the law. 1. Power Law 2. Ohm s Law 3. Kirchoff s First Law 4. Kirchoff s Second Law

9 What is the equivalent property of each of the following? 1. Two voltage sources connected in series; in other words what is the equivalent voltage if these two elements were replaced by a single voltage source? 2. Two resistors connected in series. 3. Two resistors connected in parallel. 4. Two voltage sources connected in parallel.

10 The H 2 O vs. e - analogy e - in a wire Current (1 amp= 1 coulomb/s = 6.2*10 18 electrons/s). Voltage ( 1 volt = 1 joule/coulomb) Resistance (1 ohm = 1 volt/amp) resistance increases with decrease in wire diameter and increase in wire length H 2 O in a pipe Flow rate (e.g. gal/sec) Pressure (e.g. lbs/sq. inch, atm.) Flow resistance (pressure/unit flow) resistance increases with decrease in pipe diameter and increase in pipe length Mod. PWC 4101

11 Rubinson, K.A. and J.F. Rubinson, Contemporary Instrumental Analysis. 2000, Upper Saddle River: Prentice Hall.

12 Electronics and Signal Processing in Four Parts Stoll, Che380 Part II Measurment Errors and Operational Amplifiers

13 Skoog, Holler, and Crouch, 7 th Ed.

14 Schematic of a Glass ph Electrode with Ag/AgCl Reference Electrodes Outer Reference Electrode Salt Bridge, or, Liquid Junction (Porous Plug) Glass Membrane Inner Reference Electrode Ag (s) AgCl (s) Ag + K + Cl- Analyte Solution Unknown [H + ] H + H H + H + H + H + Ag + H + Cl- [H + ], [Cl - ] ~ 1 M Ag (s) AgCl (s) E 1 E 2 E 3 E 4 E 5 Ag ( s ) + Cl( aq) AgCl( s) + e Voltmeter (+) or (-) Ag ( s ) + Cl( aq) AgCl( s) + e Stoll, SOC, 2005

15 +15 volt power Wiring of Simple 741 Op-Amp Positive signal input (v + ) Negative signal input (v - ) Output v out -15 volt power Horowitz and Hill, Figure 3-3

16 What are three performance characteristics of operational amplifiers that make them particularly useful in analytical instrumentation? What does the word operational in operational amplifier imply about the ways op-amps can be used?

17 What is the most important performance characteristic of a voltage follower circuit? In what type of instrument might such a circuit be useful? What is the most important performance characteristic of a current follower circuit? In what type of instrument might such a circuit be useful?

18 Skoog, Holler, Crouch, 7 th Ed., Fig. 3-10

19 Simple Single Transistor Amplifier Ordinarily, α = 0.95 to and β = 20 to 200. Fundamentally transistors are current amplifiers thus small changes in I B give big changes in I C Skoog, Holler, Crouch, 7 th Ed., Fig. 2-18

20 Electronics and Signal Processing in Four Parts Stoll, Che380 Part III Analog Filtering and A/D Conversion

21 Key Concepts for RC Circuits and Analog Filtering 1. Time Constant, Cutoff Frequency calculation and significance 2. How do we use a RC circuit where do we measure V out? 3. Gain and Bode plots for RC filters calculation and significance 4. Passive vs. Active analog filters what is the difference, both in terms of construction and performance? 5. Negative impact of RC filtering

22 Signal vs. Noise-Welcome to the Real World! PWC What we want to see What we do see

23 What you want an IDEAL noise reducer to do. Before filtering After filtering PWC

24 Draw the schematic of a simple circuit (no amplifiers) that can be used as a lowpass analog filter. Draw the schematic of a simple circuit (no amplifiers) that can be used as a highpass analog filter.

25 Calculate the time constant and cutoff frequency for a circuit composted of a 1 kω resistor and a 20 µf capacitor connected in series. Construct a plot that shows the output voltage from a low-pass RC filter as a function of time in response to a step change in the input voltage from 1 to 0 V. Assume the circuit has a time constant of 1 sec.

26 PWC Gaussian Peak + Random Short-Term Noise + Low-Pass RC Filter with RC TOO SMALL

27 PWC Gaussian Peak + Random Short-Term Noise + Simple RC Filter

28 Signal vs. Noise-Welcome to the Real World! PWC What we want to see What we do see

29 What you want an IDEAL noise reducer to do. Before filtering After filtering PWC

30 PWC Gaussian Peak + Random Short-Term Noise + Low-Pass RC Filter with RC TOO SMALL

31 PWC Gaussian Peak + Random Short-Term Noise + Simple RC Filter

32 Horowitz and Hill, Art of Electronics

33 Rubinson and Rubinson Contemporary Instrumental Analysis

34 What is the decimal equivalent of the following binary number? Suppose the full output range of your UV detector is 1 V. What is the smallest signal that be detected following digitization of the analog signal using a 8-bit A/D converter? How does change if you using a 24-bit converter?

35 Electronics and Signal Processing in Four Parts Stoll, Che380 Part IV Digital Filtering and Fourier Analysis

36

37

38 Skoog, Holler, Crouch, 7 th Ed., Fig. 5-10

39

40

41 Noisey Input INPUT to Moving Average Smooth Signal Index PWC

42 5 Point Moving Average Smooth Output Signal Index PWC

43 11 Point Moving Average Smooth Output Signal Index PWC

44 Representation of a Square Wave by a Series of Sine Waves Fig Rubinson and Rubinson Contemporary Instrumental Analysis

45 Original Signal (Analog) Reconstructed Signal (Digital)

46 Skoog; Holler; Crouch Principles of Instrumental Analysis, 6th ed.; Thomson Brooks/Cole, 2007.

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