N-Methyl-1-(6-methylpyridin-2-yl)propan-2-amine
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1 H C N CH HN CH. GENERAL INFORMATION IUPAC Name: CAS#: Not Available Synonyms: Source: Appearance: Not Available DEA Reference Material Collection Pale yellow powder UV max (nm): Not Determined. CHEMICAL AND PHYSICAL DATA. CHEMICAL DATA Form Chemical Formula Molecular Weight Melting Point ( o C) Base C 0 H 6 N 64 Not Determined HCl C 0 H 6 N HCl 00 Not Determined Page of 5
2 . QUALITATIVE DATA. NUCLEAR MAGNETIC RESONANCE Sample Preparation: Dilute analyte to ~4 mg/ml in CD OD containing TMS for 0 ppm reference and dimethylfumarate as quantitative internal standard. Instrument: Parameters: 0 0 MHz NMR spectrometer Spectral width: at least containing - ppm through ppm Pulse angle: 90 o Delay between pulses: 45 seconds HNMR: HCl Lot RM-0-0, 0MHz 9 8 Dimethylfumarate Dimethylfumarate Methanol Methanol TMS Page of 5
3 . GAS CHROMATOGRAPHY/MASS SPECTROMETRY Sample Preparation: Dilute analyte ~ mg/ml base extracted into CHCl. Instrument: Column: Carrier Gas: Temperatures: Agilent gas chromatograph operated in split mode with MS detector HP-5 MS (or equivalent); 0m x 0.5 mm x 0.5 m Helium at ml/min Injector: 80 o C MSD transfer line: 80 o C MS Source: 0 o C MS Quad: 50 o C Oven program: ) 00 o C initial temperature for.0 min ) Ramp to 80 o C at o C/min ) Hold final temperature for 9.0 min Injection Parameters: Split Ratio = 5:, L injected MS Parameters: Mass scan range: amu Threshold: 00 Tune file: stune.u Acquisition mode: scan Retention Time: 4.66 min EI Mass Spectrum: HCl, Lot RM-0-0 Intensity [x 0 6 ] EI m/z Intensity [x 0 4 ] EI m/z Page of 5
4 Page 4 of 5. INFRARED SPECTROSCOPY (FTIR) Insrument: FTIR with diamond ATR attachment ( bounce) Scan Parameters: Number of scans: Number of background scans: Resolution: 4 cm - Sample gain: 8 Aperture: 50 FTIR ATR (Diamond, Bounce): HCl, Lot RM-0-0) Wavenumber (cm-) %Transmittance Wavenumber (cm-) %Transmittance
5 4. ADDITIONAL RESOURCES No Literature available as of 0/06 Page 5 of 5
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