Dynamic Light Scattering Particle Size Distribution Analyzer LB-500
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1 Dynamic Light Scattering Particle Size Distribution Analyzer LB-500
2 At Last, Routine Particle Size Distribution Measurement Enters the realm of the Nanometer Horiba has refined its expertise in developing state-of-the-art particle size distribution measuring equipment for more than 20 years. Building on this wealth of experience and technology, we have developed the LB-500 Dynamic Light Scattering Particle Size Distribution Analyzer. Advanced application of dynamic light scattering theory has enabled HORIBA to reach a wide measurement range, spanning from the infinitesimal 3 nm, up to 6 micro meter. The handy cell-type system and user-friendly software combine to bring you remarkable ease of operation. In addition, the unit provides excellent capabilities for monitoring effects due to temperature and concentration of the sample, making the LB-500 ideally suited for both quality control and research applications. Point 1: High accuracy measurement of microscopic particles Point 2: Measurement of a wide range of sample concentrations and at concentrations near or equal to that of the original dispersion Point 3: Outstanding ease of operation Efficient, easy to use cell-type system. Optimal performance in measuring valuable or extremely small samples. Point 4: Feature-Loaded Software Many new features have been included in the software, such as 3D display, learning, on-line help, print layout, and a cell check, among others. Recommended for Customers: Already using dynamic light scattering particle size equipment who need to measure high concentration samples. Already using laser diffraction or dynamic light scattering particle diameter distribution measuring equipment who need to measure smaller size particles than possible on the equipment currently being used. Working in fields for which a micron sized particle is already considered to be a "large" particle. Who want to know the variation in cohesion of distributed particle diameter vis-a-vis concentration strength. Who want to know the change in sample properties vis-a-vis temperature. Applications: Advanced Materials Science, R&D, Quality Control Abrasive slurries such as CMP and diamond Carbon black High resolution ink UV blocking cosmetics (foundation, emulsions, etc.) Inks etc. Paints, dyes and pigments Latexes
3 Supporting Simplicity, Accuracy,and Unmatched ease of operation The cell-type system is optimal for measuring precious experimental materials or extremely small samples An easy to use celltype system has been adapted for use as the sampleholding vessel (a rectangular glass container). Simply pour the sample solution into the cell and it is ready to be measured with full accuracy. A 2 cc quantity of sample dispersion is sufficient. What's more, the dispersion can be reclaimed after measurement, preserving valuable samples. Optional unit provides greater accuracy through precise temperature control. In order to allow measurement of samples whose size distributions are sensitive to temperature changes, the temperature of a sample can be adjusted via a heater or an electronic cooler (temperature adjustable model). Compared to the temperature bath controlled type, the data sampling function is much smoother. The temperature can be effectively controlled in the o C range. Software Flexibility, Versati Frequently Used Data Lists and Function-Click once and Measure Properties of the dispersion medium required for measurement, such as refractive Index, viscosity calculation formula, etc. are stored in advance in list format. When you are ready to make a measurement, just select the name of the dispersion medium from the menu. Applied Dynamic Light Scattering Theory allows measurement f Applying dynamic light scattering theory, we bring you measurement capability over a wide range, from 3 nm to 6 µm. Moreover, the time required from the start of the measurement to the displaying of the results is a speedy 2 minutes. Able to Handle High-Concentration Measurements, and a Wider Range of Dispersion Concentrations Laser diode Laser collimator lens Lens Pinhole filter Sample particles contained in cell Mirror with hole Lens Mirror surface Light collecting detection lens Scattered laser light collecting lens Detector Signal converter CPU PC LB-500 Optics System Light irradiated from a laser is passed through a lens and focused onto particles contained in the cell. The focal point of the lens is positioned on the inner wall of the cell, concentrating maximum light in order to suppress multiple-dispersions' that occurs when high concentration dispersion are measured. In addition, a pinhole filter removes errant beams, assuring that only light scattered from the focal point will be sent to the detectors. A signal is generated corresponding to the Brownian movement (vibration) of the particles. The frequency of a particle s vibration is dependent on number of factors including the size of the particle. Through analysis of the frequency component, the particle size distribution can be determined.
4 lity at Your Fingertips On-line Help Function allows you to check operating procedures, functions and data quickly Find refractive index data for 1500 sample types and 800 types of dispersion media, in addition to operation procedures, quickly and easily using the on-line help function. One-click Automated Operation Streamlines Routine Workloads Parameter settings necessary for measurement and operation procedures can be registered in advance, enabling one-click automated operations. The learning wizard provides convenient entry for data and operation procedures. With 3D Display of Related Data, Changes are readily detected at a glance Comparative measurement results as well as variations in agglomeration due to changes in temperature,can be viewed via the 3D display. The Real Time display makes changes in position readily detectable at a glance. The Print Layout Function Provides Easy Format Customization for Reports Graphs, measurement results, etc. can be arranged as you like on the display screen. There is also a function enabling the insertion of a company name and logo. Measurement data reports can be presented clearly and professionally to meet your every need. Layout screen Output example rom Nanometer-to-Micron Range Allows for The Measurement of Samples of Inks, Paints and other Particles with Pronounced Color Properties High Accuracy Measurements over a Wide Range of Particle Sizes Combines with the LA Series to Form a System Covering the Full Range of Particle Sizes for Particle Diameter Distribution Measurement The LB-500 can be combined with the LA series (920 and 300) laser diffraction/light scattering particle diameter measurement equipment to form a system. When combined with the LA-920, the resulting system covers the full range of particle diameters between 3 nm and 2 mm. Data from both units can be read into the computer simultaneously and comparative measurement data displayed on a single screen. Able to measure red, blue, and 3 types of yellow inks without dilution. Measurement Range for the LB µm and 0.2 µm polystyrene latex compound sample. Sample mixture was analyzed precisely and separated into 2 peaks. Measurement Range for the LA-920 (laser diffraction/light scattering) 1nm 10nm 100nm 1 µm 10 µm 100 µm 1mm 2mm
5 Measurement Results Screen Calculation results Measurement results data Data table Particle diameter dispersion graph Memory graph Measurement Screen Automatic check for cell contamination Real time sample concentration display Simple particle diameter distribution graph
6 Specifications Standard type Measurement principle Range of particle size displayed Measurement time Amount of dispersion required for measurement Possible dispersing media Communications Measuring unit Laser Type Operation environment Cell holder Power Dimensions Weight Dynamic light scattering theory 3 nm - 6 µm. Approximately 2 minutes under normal conditions (from start of measurement to display of results) Approximately 2-4 ml Water, organic solvents SCSIII (between PC and analyzer) 50pins Optical system: Light Source: 650 nm laser diode, 5 mw Photo-cell detector: Silicon photo diode Cell: Cuvette cell,interior length 10 x 10mm,Exnterior length 12.5 x 12.5mm Class 1 15 o C (59 o F) -35 o C (95 o F), less than 85% RH (no condensation) Attachable to a constant-temperature water bath AC 100/120/230 V 50/60 HZ, 60 VA 300(W) x 420(D) x 320(H) mm (excluding the protruding structures) 11.8(W) x 16.5(D) x 12.6(H) in Approximately 18 kg, 40 lb Data processing, Operation unit: PC: An IBM compatible PC/AT that runs Windows 95 or 98 OS: Windows 95 or 98 SCSI board: ADAPTEC recommended Printer: A Windows 95 or 98 compatible printer Monitor: A Windows 95 or 98 compatible monitor Operation: Data entry with keyboard and mouse under Windows 98 Data Processing: Real-time display of scattered light intensity and particle size distribution Median diameter, surface area, mode diameter, average particle size, standard deviation, CV value, span value, cumulative particle size % (for a maximum of 10 points), % on cumulative particle size (for a maximum of 10 points) Particle size distribution graph, chart display, frequency distribution, cumulative distribution, oversize distribution, undersize distribution, Distribution base on number, length, area, volume. Overlay graphic display (up to 17 data), graph axes settings (3 types: linear x-linear y; linear x-log y; linear y-log x) Refractive index, calculation of data in response to change in the viscosity coefficient Operations procedures are programmable; and can be carried out automatically. File conversion function (particle distribution data files can be converted to text file format.) Data from a particle size distribution graph can be copied to the clipboard. Supports importing and displaying of measurement data files created by LA-920/300 software Temperature control type A temperature control unit equipped with a heater and an electronic cooler is attached to the LB-500 at the factory when ordering. It provides the customer to specify the temperature of samples. Temperature control range Power Weight (Measuring unit) External dimensions (Unit: mm) o C Supplying Cooling water is required depending on the operating environment conditions or temperature setting (The flow rate of the cooling water is approximately 0.4 l/min is required). 150 VA Approximately 20 kg. The LB-500 employs with a Class 1 Laser Horiba continues contributing to the preservation of the global environment through analysis and measuring technology. Please read the operation manual before using this product to assure safe and proper handling of the product. The contents of this catalog are subject to change without prior notice, and without any subsequent liability to this company. The color of the actual products may differ from the color pictured in this catalog due to printing limitations. It is strictly forbidden to copy the content of this catalog in part or in full. HORIBA, Ltd. Head Office Miyanohigashi, Kisshoin Minami-ku, Kyoto, Japan Phone: 81 (75) Fax: 81 (75) Tokyo Sales Office Higashi-Kanda Chiyoda-ku, Tokyo, Japan Phone: 81 (3) Fax: 81 (3) HORIBA INSTRUMENTS INCORPORATED Irvine Facility Ann Arbor Facility Armstrong Avenue 5900 Hines Drive Irvine, CA 92614, U.S.A. Ann Arbor, MI Phone: 1 (949) U.S.A. Fax: 1 (949) Phone: 1 (734) Fax: 1 (734) HORIBA EUROPE GmbH Head Office Hauptstrasse 108 D Sulzbach Germany Phone: 49 (6196) Fax: 49 (6196) Leichlingen Facility Julius-kronenberg Strasse D Leichlingen Germany Phone: 49 (2175) Fax: 49 (2175) Beijing Representative Office Room No. 410, No. 33 Cheng Fang Street, Xicheng District, Beijing P.R.O.C T.O.D. Beijing Phone: /5 Fax: HORIBA / STEC INCORPORATED 1080 E. Duane, Suite. A Sunnyvale, CA U.S.A. Phone: 1 (408) Fax: 1 (408) HORIBA FRANCE Rue L. et A. Lumière Technoparc F St-Genis-Pouilly France Phone: 33 (4) Fax: 33 (4) Taiwan Representative Office No.15 Alley6, Lane 485, Sec. 1, Kuang Fu Rd., Hsin-Chu, Taiwan, R.O.C. Phone: (886) Fax: (886) HORIBA GmbH Kaplanstrasse 5 A-3430 Tulln, Austria Phone: 43 (2272) Fax: 43 (2272) HORIBA SWEDEN Hertig Carlsv ag S Södertälje Sweden Phone: 46 (8) Fax: 46 (8) HORIBA KOREA L t d Sogong-Dong Choong-ku, Seoul, Korea Phone: 82 (2) Fax: 82 (2) HORIBA CZECHIA Organizachi slozka Praha Petrohradska 13 CZ Praha 10, Czech Republic Phone: 420 (2) Fax: 420 (2) HORIBA ITALY Europalace Corso Torino 43/ Orbassano,Torino,Italy Phone: 39 (11) Fax: 39 (11) HORIBA INSTRUMENTS Pte. LTD. 31 Kaki Bukit Road 3, #06-12 Techlink Singapore Phone: Fax: HORIBA INSTRUMENTS LIMITED Kyoto Close Summerhouse Road Moulton Park, Northampton NN3 6FL, U.K. Phone: 44 (1604) Fax: 44 (1604) Bulletin:HRE-3649B Printed in Japan ZH-R(SK)14
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