TEST REPORT NO.: SHE Date: 2015/08/26 Page: 1 of 12
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1 TEST REPORT NO.: SHE Date: 25/08/26 Page: 1 of 12 The following sample was collected by the SGS: : WATER AND SLUDGE SAMPLES Buyer Name : Jack Wolfskin Factory Name : Ref Number. : / Received Quantity : / Department No. : SH ENVI LAB Country of Origin : CHINA Country of Destination : CHINA Receiving Date : Test Performing Period : TO 25/08/26 Remarks 1.This test document cannot be reproduced in any way, except in full content, without prior approval in writing by the laboratory. 2.The results shown in this test report refer only to the sampling and the sample(s) tested unless otherwise stated. 3.The factory should fullfill the guideline value (4) which are 20 mg/l for BOD and 80 mg/l for COD, respectively. Signed for and on hehalf of SGS-CSTC Ltd. Eddy SHEN Lab Manager
2 Positive result summary standards of water pollutants for dyeing and finishing of textile Reporting Limit Requirement Indirect Di(2-Ethyl Hexyl) Phthalate(DEH P) With reference to USEPA 8270 or Solvent extraction with GC/MS 1 µg/l ,3 mg/kg 0, Sodium Tetraborate*^ , , , Boron trioxide*^ Boric acid*^ Antimony trioxide*^ Monobutyltin (MBT) N,Ndimethylformam ide* , Total Lead (Pb) Total Mercury (Hg) Total Nickel (Ni) Total Arsenic (As) Total Chromium (Cr) Total Copper (Cu) Total Zinc (Zn) Total Manganese (Mn) Total Antimony (Sb) Total Cobalt (Co)* Acid Digestion with ICP Acid Digestion with ICP Acid Digestion with ICP Acid Digestion with ICP With reference to DIN EN17353 and followed by GC/MS. With reference to USEPA 8260 or Solvent extraction with GC/MS ICP/MS With reference to USEPA 7473 or Acid Digestion with ICP/MS ICP/MS ICP/MS ICP/MS ICP/MS ICP/MS ICP/MS ICP/MS ICP/MS 0,5 µg/l 55,8 121,0 141, ,25 mg/kg 132,22-0,5 µg/l 38,7 83,9 97, ,25 mg/kg 91,64-0,5 µg/l 68,5 149,0 173, ,25 mg/kg 162,33-0,5 µg/l - 408,0 45, ,25 mg/kg 168, - 0, µg/l 0, , mg/kg µg/l ,1 mg/kg µg/l mg/kg 4-0,05 µg/l ,006 mg/kg 0,046-1 µg/l mg/kg 2-1 µg/l mg/kg 1-1 µg/l mg/kg 24-1 µg/l mg/kg 6-1 µg/l mg/kg 19-1 µg/l mg/kg 9-1 µg/l <100µg/L <100µg/L 1 mg/kg µg/l mg/kg - - Page 2 of 13
3 Positive result summary standards of water pollutants for dyeing and finishing of textile Reporting Limit Requirement Indirect Nonylphenol , , , , With reference to DIN EN ISO and followed by LC/MS 1 µg/l ,2 mg/kg 10, NPEO, n=1~2 With reference to DIN EN ISO and followed by LC/MS 1 µg/l ,2 mg/kg 42, NPEO, n=3~ , , , With reference to DIN EN ISO and followed by LC/MS 1 µg/l ,2 mg/kg OPEO, n=1~2 With reference to DIN EN ISO and followed by LC/MS 1 µg/l ,2 mg/kg 3, PFOA With reference to CEN/TS and with LC/MS and GC/MS 0, µg/l ,0 mg/kg 0, PFHXS PFHpA With reference to CEN/TS and with LC/MS and GC/MS With reference to CEN/TS and with LC/MS and GC/MS 0, µg/l ,0 mg/kg 0,007-0, µg/l ,0 mg/kg 0, PFDA With reference to CEN/TS and with LC/MS and GC/MS 0, µg/l ,0 mg/kg 0, HPFUnA With reference to CEN/TS and with LC/MS and GC/MS 0, µg/l - - 0, ,0 mg/kg BOD (5-day) - SM mg/l <20mg/L <150 3 / <50 4 mg/l COD - USEPA or SM <500 3 / 5 mg/l <80mg/L 5220D <200 4 mg/l TSS - SM 2540D 5 mg/l <50mg/L <100mg/L TDS - SM 2540C 5 mg/l Cyanide - APHA 4500 CN B,C & E 0, mg/l , mg/kg 0, Sulfide - SM 4500-S2-D 0,005 mg/l <0.5mg/L <0.5mg/L ph Value - SM 4500H+ - 6,37 5,27 5, USEPA or SM 15.8 Colour B or ISO CU Method D GB/T DF <50 < Page 3 of 13
4 Date d standards 04 Indirect 1 # Requirement 1 Phthalates 1.1 Di-Butyl Phthalate (DBP) Di(2-Ethyl Hexyl) Phthalate(DEHP) Benzyl Butyl Phthalate (BBP) Di-Iso-Nonyl Phthalate (DINP) , Di-N-Octyl Phthalate (DNOP) Di-Iso-Decyl Phthalate (DIDP) , Di-Iso-Butyl Phthalate (DIBP) Di-N-Hexyl Phthalate (DNHP) Bis(2-methoxyethyl)phthalate (DMEP)* ,2-Benzenedicaboxylic acid, Di-C7-11 Branched and Linear Alkyl Esters (DHNUP)* Di-Iso-Hexyl Phthalate (DIHP)* Di-pentylphthalate (n-, iso-, or mixed) (DPP)* 2 Halogenated Flame retardants Polybrominated biphenyls (PBBs) Monobromo biphenyls (MonoBB) Dibromo biphenyls (DiBB) Tribromo biphenyls (TriBB) Tetrabromo bipenyls (TetraBB) Pentabromo biphenyls (PentaBB) Hexabromo biphenyls (HexaBB) Heptabromo biphenyls (HeptaBB) Octabromo biphenyls (OctaBB) Nonabromo biphenyls (NonaBB) Decabromo biphenyls (DecaBB) Polybrominated diphenyl ethers (PBDEs) 2.11 Monobromo diphenyl ethers (MonoBDE) Dibromo diphenyl ethers (DiBDE) Tribromo diphenyl ethers (TriBDE) Tetrabromo diphenyl ethers (TetraBDE) Pentabromo diphenyl ethers (PentaBDE) Hexabromo diphenyl ethers (HexaBDE) Heptabromo diphenyl ethers (HeptaBDE) Octabromo diphenyl ethers (OctaBDE) Nonabromo diphenyl ethers (NonaBDE) Decabromo diphenyl ethers (DecaBDE) Tris(2,3-dibromopropyl) phosphate (TRIS) Tris(2-chloroethyl) phosphate (TCEP) Hexabromocyclododecane (HBCDD) , , , , Tetrabromobisphenol A (TBBPA) extraction with GC/MS or LC/MS extraction with GC/MS or LC/MS extraction with GC/MS or LC/MS extraction with GC/MS or LC/MS 1 µg/l <1 < ,3 mg/kg 0,3-0,05 µg/l <0.05 <0.05 < ,25 mg/kg < Subgroup: Other Flame Retardants 2.25 Tris(1-aziridinyl)phosphine oxide) (TEPA)* extraction with GC/MS or LC/MS 2.26 Bis(2,3-dibromopropyl)phosphate (BIS)* extraction with GC/MS or LC/MS 2.27 Sodium Tetraborate*^ , , , Acid Digestion with ICP 0,5 µg/l 55,8 121,0 141, ,25 mg/kg 132, Boron trioxide*^ Acid Digestion with ICP 0,5 µg/l 38,7 83,9 97, ,25 mg/kg 91,64 - Page 4 of 13
5 Date d standards 04 Indirect 1 # Requirement 2.29 Boric acid*^ , Acid Digestion with ICP 0,5 µg/l 68,5 149,0 173, ,25 mg/kg 162,33 - Page 5 of 13
6 Date d standards 04 Indirect 1 # Requirement 2.30 Antimony trioxide*^ Acid Digestion with ICP 0,5 µg/l < ,0 45, ,25 mg/kg 168, Tri-o-cresyl phosphate* extraction with GC/MS or LC/MS 2.32 Tris(1,3-dichloro-2-propyl) phosphate (TDCPP)* extraction with GC/MS or LC/MS 3 Amines (Associated with Azo dyes) Aminodiphenyl Benzidine Chloro-o-Toluidine Naphthylamine o-aminoazotoluene Amino-4-Nitrotoluene p-chloroaniline ,4-Diaminoanisole ,4 -Diaminodiphenylmethane ,3 -Dichlorobenzidine ,3 -Dimethoxybenzidine ,3 -Dimethylbenzidine ,3 -Dimethyl- 4,4 diaminodiphenylmethane p-cresidine ,4 -Methylene-Bis(2-Chloroaniline) ,4 -Oxydianiline ,4 -Thiodianiline o-toluidine ,4-Toluylenediamine ,4,5-Trimethylaniline o-anisidine p-aminoazobenzene ,4-Xylidine ,6-Xylidine Subgroup: Carcinogenic Dyes 4.1 Acid Red 26* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Basic Red 9* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Basic Violet 14* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Blue 6* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Red 28* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Black 38* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 3* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Orange 11* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 23* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Orange 149* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Solvent Yellow 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Solvent Yellow 2* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Solvent Yellow 3* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Solvent Yellow 14* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Basic Blue 26* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Basic Violet 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Brown 95* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Blue 15* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Blue 218* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Acid Red 114* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Acid Violet 49* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg <0.1 - Subgroup: Allergenic Disperse Dyes 4.23 Disperse Blue 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 3* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 7* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 26* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 35* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 106* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Blue 124* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Brown 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg <0.1 - Page 6 of 13
7 Date d standards 04 Indirect 1 # Requirement 4.32 Disperse Orange 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Orange 3* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Orange 37/76* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Red 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Red 11* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Red 17* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 1* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 3* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 9* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 39* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg < Disperse Yellow 49* Solvent extraction with LC/MS 0,1 µg/l <0.1 <0.1 < ,1 mg/kg <0.1-5 Organotin compounds 5.1 Monobutyltin (MBT) Dibutyltin (DBT) Tributyltin (TBT) Triphenyltin (TPhT) Dioctyltin (DOT) Monooctyltin (MOT) Diphenyltin (DPhT) Tetrabutyltin (TeBT) Tricyclohexyltin (TCyT) NA 5.10 Tripropyltin (TPT) NA 5.11 Tetraethyltin (TeET) Bis(tributyltin) oxide (TBTO)* Dibutyltin dichloride (DBTC)* Triphenyltin (TPT)* Dibutyltin hydrogen borate (DBB)* Chloro- Benzenes Dichlorobenzenes 6.1 1,2-Dichlorobenzene ,3-Dichlorobenzene ,4-Dichlorobenzene Trichlorobenzene 6.4 1,2,3-Trichlorobenzene ,2,4-Trichlorobenzene ,3,5-Trichlorobenzene Tetrachlorobenzene ,2,3,4-Tetrachlorobenzene ,2,3,5-Tetrachlorobenzene ,2,4,5-Tetrachlorobenzene Pentachlorobenzene Hexachlorobenzene Chloro-Toluenes chlorotoluene* chlorotoluene* chlorotoluene* ,3-dichlorotoluene* ,4-dichlorotoluene* ,5-dichlorotoluene* ,6-dichlorotoluene* ,4-dichlorotoluene* , µg/l 0, <0. < , mg/kg <0. - Page 7 of 13
8 Date d standards 04 Indirect 1 # Requirement ,3,6-trichlorotoluene* ,4,5-trichlorotoluene* Benzotrichloride* alfa,2,4-trichlorotoluene* alfa,2,6-trichlorotoluene* alfa,3,4-trichlorotoluene* alpha, alpha, 2,6-tetrachlorotoluene* alpha, alpha, alpha, 2- tetrachlorotoluene* alpha, alpha, alpha, 4- tetrachlorotoluene* ,3,4,5,6-pentachlorotoluene* Chlorinated solvents 7.1 Dichloromethane Chloroform Tetrachloromethane ,1,2-Trichloroethane ,1-Dichloroethane ,2-Dichloroethane Trichloroethylene Perchloroethylene ,1,1-trichloroethane ,1,1,2-Tetrachloroethane ,1,2,2-Tetrachloroethane Pentachloroethane ,1-Dichloroethylene Other VOCs 7.14 Methyl-ethyl ketone* Benzene* Toluene* Ethylbenzene* Xylene* Styrene* Cyclohexanone* ethoxyethylacetate* ,2,3-trichloropropane* Acetophenone* N,N-dimethylformamide* methyl-2-pyrrolidone* phenyl-2-propanole* Bis-(2-methoxyethyl) ether* N,N-dimethylacetamide* µg/l <1 <1 < mg/kg <2-1 µg/l <1 <1 < mg/kg <10-1 µg/l <1 <1 < mg/kg <10-1 µg/l <1 < ,1 mg/kg <0.1-1 µg/l <1 <1 < mg/kg <50-1 µg/l <1 <1 < mg/kg <20-1 µg/l <1 <1 < mg/kg <20 - Page 8 of 13
9 Date d standards 04 Indirect 1 # Requirement 8 Chloro- Phenols 8.1 Pentachlorophenols (PCP) Tetrachlorophenols (TeCP) ,3,4,5-Tetrachlorophenol ,3,4,6-Tetrachlorophenol ,3,5,6-tetrachlorophenol Trichlorophenol (TriCP) ,4,6-trichlorophenol ,3,4-trichlorophenol ,3,5-trichlorophenol ,3,6-trichlorophenol ,4,5-trichlorophenol ,4,5-trichlorophenol Dichlorophenols (DiCP) ,3-dichlorophenol ,4-dichlorophenol ,5-dichlorophenol ,4-dichlorophenol ,5-dichlorophenol Mono Chlorophenol Various Short Chain Chlorinated Paraffins (SCCP) with C10 C13 Short Chain Chlorinated Paraffins (SCCP), C 10 -C 13 Solvent extraction with GC/MS or GC/ECD 0,4 µg/l <0.4 <0.4 < , mg/kg < Heavy Metals 10.1 Total Cadmium (Cd) ICP/MS 0,1 µg/l <0.1 <0.1 < mg/kg < Total Lead (Pb) ICP/MS 1 µg/l 2 <1 < mg/kg Total Mercury (Hg) With reference to USEPA 7473 or Acid Digestion with ICP/MS 0,05 µg/l <0.05 <0.05 < ,006 mg/kg 0, Total Nickel (Ni) ICP/MS 1 µg/l mg/kg Total Hexavalent Chromium (Cr-VI) Solvent extraction and derivatisation followed by UV 1 µg/l <1 <1 <1 ND 2 ND 2 1 mg/kg < Total Arsenic (As) ICP/MS 1 µg/l <1 1 < mg/kg Total Chromium (Cr) ICP/MS 1 µg/l mg/kg Total Copper (Cu) ICP/MS 1 µg/l 2 3 < mg/kg Total Zinc (Zn) ICP/MS 1 µg/l mg/kg Total Manganese (Mn) ICP/MS 1 µg/l mg/kg Total Antimony (Sb) ICP/MS 1 µg/l < <100µg/L <100µg/L 1 mg/kg 140 <100µg/L Total Cobalt (Co)* ICP/MS 1 µg/l <1 1 < mg/kg <1-11 Alkylphenols (APEOs) 11.1 Octylphenol , , With reference to DIN EN ISO and followed by LC/MS 1 µg/l <1 <1 < ,2 mg/kg <0.2 - Page 9 of 13
10 Date d standards 04 Indirect 1 # Requirement 11.2 Nonylphenol , , , , NPEO, n=1~ NPEO, n=3~ , , , OPEO, n=1~ OPEO, n=3~18 12 PFCs (Perfluorocarbon / Polyfluorinated Compounds) , , PFOA PFNA PFBS , PFOS POSF :2 FTOH :2 FTOH :2 FTOH :2 FTOH PFHXS PFHXA PFOSA N-Me-FOSA N -Et-FOSA N-Me-FOSE alcohol N-Et-FOSE alcohol PFBA PFPeA PFHpA PFDA PFUnA PFDoA PFTrA PFTeA PFHpS PFDS :2 FTA :2 FTA :2 FTA PF-3,7-DMOA HPFHpA HPFUnA H, 1H, 2H, 2H- PFOS Ortho- Phenylphenol 13.1 o-phenylphenol (OPP) With reference to DIN EN ISO and followed by LC/MS With reference to DIN EN ISO and followed by LC/MS With reference to DIN EN ISO and followed by LC/MS With reference to DIN EN ISO and followed by LC/MS With reference to DIN EN ISO and followed by LC/MS 1 µg/l <1 <1 < ,2 mg/kg 10,2-1 µg/l <1 <1 < ,2 mg/kg 42,3-1 µg/l <1 1 < ,2 mg/kg <0.2-1 µg/l <1 <1 < ,2 mg/kg 3,1-1 µg/l <1 <1 < ,2 mg/kg <0.2-0, µg/l <0. <0. < ,0 mg/kg 0, , µg/l <0. <0. <0. 0,0 mg/kg < , µg/l <0. <0. < ,0 mg/kg 0,007-0, µg/l <0. <0. < ,0 mg/kg 0,5-0, µg/l <0. <0. < ,0 mg/kg 0,005-0, µg/l <0. <0. 0, ,0 mg/kg < ,5 mg/kg <0.5 - Page 10 of 13
11 Date d standards 04 Indirect 1 # Requirement 14 Polycyclic Aromatic Hydrocarbons (PAHs) 14.1 Bezno[a]pyrene (BaP) Anthracene Pyrene Benzo[ghi]perylene Benzo[e]pyrene Indeno[1,2,3-cd]pyrene Benzo[j]fluoranthene Benzo[b]fluoranthene Fluoranthene Benzo[k]fluoranthene Acenaphthylene Chrysene Dibenz[a,h]anthracene Benzo[a]anthracene Acenaphthene Phenanthrene Fluorene Naphthalene General Chemistry 15.1 BOD (5-day) - SM mg/l < <20mg/L <150 3 / <50 4 mg/l 15.2 COD - USEPA or SM 5220D 5 mg/l < <80mg/L <500 3 / <200 4 mg/l 15.3 TSS - SM 2540D 5 mg/l <50mg/L <100mg/L TDS - SM 2540C 5 mg/l Cyanide - APHA 4500 CN B,C & E 0, mg/l <0. <0. < , mg/kg 0, Sulfide - SM 4500-S2-D 0,005 mg/l < <0.005 <0.5mg/L <0.5mg/L ph Value - SM 4500H+ - 6,37 5,27 5, USEPA or SM 2120B or ISO Colour - Method D 5 CU GB/T DF <50 < Total phenolics - SM 5530B 0,0 mg/l <0.0 <0.0 < Ca Hardness - SM 2340B 5 mg/l <5 <5 < Mg Hardness SM 2340B 5 mg/l <5 <5 < AOX - ISO 9562 or HJ/T mg/l <0.8 <0.8 < Percentage moisture - in-house method % 71,6 - Remark: *Best current testing technology using lowest detection ^The test result is based on the calculation of selected element(s) and to the worst-case scenario # The sample is tested base on wet mass 1) Wastewater that discharge into the municipal wastewater treatment plant, or discharge from the municipal wastewater pipeline, must meet the requirement of direct discharge. 2) The discharge monitoring location is in the workshop or production facility wastewater outfall. 3) The guideline value (3) is applicable to the wastewater solely generated from the textile (without mixing with wastewater from other sources), and discharged into a centralized treatment plant in the industrial zone (including industrial park, development zone, or cluster of ) where is specified for dyeing and finishing wastewater collection and treatment only. The effluent from centralized treatment plant must meet the guideline value in remark (4). 4) The guideline value (4) is suitable for the other indirect discharge scenarios. 5) The factory should fullfill the guideline value (4) which are 20 mg/l for BOD and 80 mg/l for COD, respectively. ***End of Report*** Page 11 of 13
12 PHOTOGRAPHS INLET AFTER TREATMENT BEFORE TREATMENT SLUDGE Page 12 of 13
13 PIPING PLAN Page 13 of 13
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