1. Introduction MICROENCAPSULATION PATENTS A SOURCE OF INNOVATION AND TREND ANALYSIS. Microencapsulation WALL
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1 MICROENCAPSULATION PATENTS A SOURCE OF INNOVATION AND TREND ANALYSIS 1. Introduction Bojana Boh Faculty of Natural Sciences and Engineering, University of Ljubljana, Slovenia Microencapsulation CORE WALL INTELLECTUAL PROPERTY knowledge intensive research field COPYRIGHT AND RELATED RIGHTS TOPOGRAPHIES OF INTEGRATED CIRCUITS INDUSTRIAL PROPERTY basic research + industrial applications rapid growth of publications AUTHORS' RIGHTS RELATED RIGHTS PATENTS TRADE MARKS INDUSTRIAL DESIGNS 1
2 Patents: legal protection of inventions Patents: literature source exclusive right to make use of an invention (defined period, limited geographic area), the right to stop others from making, using or selling the claimed invention without authorisation newest information on innovative developments before scientific articles and conferences (no prior disclosure) 70% of information in patents never published elsewhere Databases 2. Materials and methods Web of Science (IZUM) - payable Chemical Abstracts Plus (STN International) - payable Espacenet ( ) - free 2
3 Information methods for patent analysis (1) Value-added processing of a bibliographic part of patent documents for the definition of trends (Kardos et al., 2000) 3. Results and discussion (2) Structuring of data into systems for the analysis of contents - full text documents (Kornhauser, 1989) Patents vs. scientific articles on microencapsulation (CAPlus database) Microencapsulation fields comparison of fundamental vs. industrial research Scientific articles Patents 1:2 Database: Web of science Database: Espacenet 3
4 LEADING COUNTRIES : Patent documents on microencapsulation by country Why microencapsulate? R E L E A S E P E R M E A B I L I T Y M E C H A N I S M Drugs, agrichemicals, food additives... Biotechnology, medicine... Pressure-sensitive copying papers, adhesives... Temperature indicators, deodorants... Light-sensitive recording papers... Instant drinks, soups, washing additives Pharmaceuticals, chemicals... Food and feed... Anti-statics, fragrances... Fire retardsnts... Espacenet Advanced Search : Keyword(s) in title or abstract: microcapsul*or microencap*) AND Publication number / Priority number Light plastic, artificial leather... Selected examples of new industrial developments 1. Electronic ink displays 2. Materials science self healing composite materials 3. Phase change materials (PCM) 4. Scientifically advanced cosmetics 5. Innovative bio-encapsulation delivery systems Bio-microencapsulation applications 4
5 Bio-microencapsulation 5
6 University-Industry Cooperation between University of Ljubljana and Aero d.d. Information system: a core of university-industry cooperation 25 years of cooperation in informationsupported R&D microencapsulation technologies applications in graphics, printing, agrochemicals, food and textiles 1. Structuring of data for designing improved microencapsulation processes 2. Searching for free application niches for R&D of new products 6
7 Structuring of patent information: Hypothetical process backbone (for further laboratory optimisation) Information density (predicting probability) % % % % < 20 % AERO patent YU 1319/84 Applied research linked with M.Sc. work + Aero patent 7
8 Pressure-sensitive copying paper 2. Searching for free application niches for R&D of new products Example 1 Graphics and printing : Self-contained printing ink Fragranced printing ink PAPER MICROENCAPSULATED LEUCO DYE DEVELOPER PRESSURE-SENSITIVE COPYING PAPERS TWO ACTIVE LAYERS ONE ACTIVE LAYER Hypothetical matrix SINGLE MICROCAPSULES DOUBLE MICROCAPSULES
9 US US US US CA GB GB GB EP EP US US DE DE DE US GB CA GB CA GB GB GB US US US CA EP US US US DE DE GB GB CA GB CA GB GB CA US DE DE US CA EP DE US US Identifying two systems with the largest number of innovations: No.1: already known No.4: not considered before Pressure-sensitive printing ink for bank mailers (Aero patent SI ) Pressure-sensitive printing ink for scented repositionable paper notes (microencapsulated fragrances: Citrus, Lavandula, rose, strawberry) Example 2: Food industry: Aromatised tea 9
10 Microencapsulated aromas for tea (Aero patent SI ) Example 3: Agriculture: microencapsulated animal repellents Prolonged release formulations: aqueous microcapsule suspension concentrates (Aromit MK ) thickened pastes coated or impregnated carriers: non-woven textiles, paper Example 4: Antimicrobial fragranced textiles roe deer Capreolus capreolus L. rabbits Lepus europaeus Pallas 10
11 Non-woven textiles with microencapsulated antimicrobial agents Scented woven textiles Example 5: Microencapsulated Phase Change Materials (PCM) Nonvowen polypropylene textile impregnated with microencapsules (SEM, 630x); Growth of new documents on microencapsulation in textiles (CAPlus database) Phase change materials (PCMs) 70 Sub-group of heat storage materials (heat exchange process at the melting point) Number of new documents on microencapsulation in textiles Non-patent Solid to liquid: energy is stored Patent Liquid to solid: energy is released 30 Microencapsulation 20 Applications in textiles: sports wear, diving suits, fire wear, special working clothes, gloves, shoes Years 11
12 Modified in situ polymerisation process patents SI (1995), and EP (1997), Aero d.d. Water + aminoaldehyde resin + anionic polyelectrolyte modifying agent Emulsification Polycondensation of a lipophylic (change of core material temperature (active substance) and ph) Size distribution of microcapsules (small microcapsules 2,5 mm, large microcapsules 6,0 mm) Microcapsule hardening, removal of residual monomers PCM microcapsules resistant to mechanical and thermal stress produced by the modified in situ polymerisation process 4. Conclusions Individual microcapsules of PCMs (SEM, 8000 x). Spray dried granules of microencapsulated PCMs (SEM, 190x). 12
13 Conclusions Microencapsulation - multidisciplinary field, several technologies, numerous application fields Rapid growth of information, large proportion of patents, Ability to analyse and structure large amounts of information; transformation into knowledge Pharmaceutical, biotechnological, chemical companies - a crucial role of industrial intellectual property (competitiveness, identification of market niches) Acknowledgements Aero R&D: E. Knez, M. Kukovič, B. Šumiga The projects were co-financed by the Slovenian Ministry of Science and Technology (MZT), Slovenian Research Agency (ARRS), and Aero Chemical, Graphic and Paper Manufacturers, Celje 13
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