Manufacturing Metrology Team

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The Team has a range of state-of-the-art equipment for the measurement of surface texture and form. We are happy to discuss potential measurement issues and collaborative research Manufacturing Metrology Team L4 143 Coates Building The University of Nottingham University Park Nottingham, NG7 2RD Please visit: www.nottingham.ac.uk/research/manufacturing-metrology for more information and/or register for a free measurement of your sample

Alicona G5 focus variation measuring instrument The Alicona G5 Infinite Focus is a focus variation measuring instrument. It vertically scans the object's surface and captures a stack of 2D microscope images. For each image, the sharpness of each pixel is calculated. Detection of the object's surface, for each pixel, is achieved by finding the corresponding z-location having the highest sharpness. Advantages: Wide applications: form and surface texture measurement Relatively fast measuring time Up to 5-axis measurement. Beneficial for complex geometries, e.g. micro-tool measurement True colour of measured object's surface Limitations: Difficult to measure very smooth surfaces with Ra< 10 nm Difficult to measure optical or transparent surfaces

Specifications: Objective Unit 2.5 5 10 20 50 100 Lateral sampling distance μm 3.25 1.76 0.88 0.44 0.18 0.09 Min. lateral μm 58.71 23.48 11.74 8.8 6.4 4.4 resolution Min. μm 6.92 3.49 1.75 0.88 0.64 0.44 Repeatabilit y (vert.) Vertical nm 2300 410 100 50 20 10 resolution Working distance mm 8.8 23.5 17.5 13 10.1 3.5 Field of μm 5716 2858 1429 715 286 143 view X Field of μm 4351 2175 1088 544 218 109 view Y Max. height mm 8 22 16 12 9 3.2 Step height accuracy % - 0.05 0.05 0.05 0.05 0.05 Min. meas. nm 7000 1200 300 150 60 30 roughness (Ra) Min. meas. nm 3500 600 150 75 30 15 roughness (Sa)

Mitaka MLP-3SP point autofocus measuring instrument The Mitaka MLP-3SP is a point autofocus measuring instrument. It measures surface texture by automatically focusing a laser beam at a point on a specimen surface, moving the specimen surface in a fixed measurement pitch using an XY scanning stage, and measuring the specimen surface height at each focused point. During measurement the autofocus sensor detects the laser spot displacement and feeds back the information to the autofocus mechanism in order to keep the objective at in-focus position. Advantages: Large measuring range with high resolution High speed contour measurement Capable of measuring steep angles over 45 High autofocus repeatability (nanometre level) Immune to surface reflectance properties Limitations: Long 3D measurement time compared to typical areal measurement instruments Smaller acceptable slope angle for specular surfaces Only one objective lens can be mounted

Specifications: axis moving range scale resolution measuring accuracy X 120 mm 10 nm ±4.4 μm / 120 mm Y 120 mm 10 nm ±4.4 μm / 120 mm Z 130 mm 10 nm ±4.6 μm / 130 mm AF 40 mm 1 nm ±2.8 μm / 40 mm positioning repeatability 3 μm p-v 3 μm p-v 3 μm p-v σ=0.015 (100 ) σ=0.015 (50 ) θ 360 0.0002 ±0.01 ±0.005 μm μm

Nub3D fringe projection system The Nub3D fringe projection system is used to scan objects from different views and re-create the 3D point cloud of the scene from the perspective of an integrated camera. Registration of the different views is carried out automatically with photogrammetry targets that can be attached to the object or the rotary table. Unlike traditional laser triangulation scanners, this instrument uses full frame image capture via use of phase shifting spatial profiles (fringes) to determine the depth information of every pixel in the image. The instrument can be used on multiple materials with the condition that they produce a high enough amount of diffuse reflection and objects of up to (550 390 200) mm in volume. Advantages: Fast measurement of large areas Flexibility of instrument configuration Multi-materials measurement Limitations: Limited to macro form measurement Difficult to measure surfaces with a high degree of specular reflection

Specifications: Measuring Volume 1 Volume 2 Volume 3 Volume 4 volume type Volume (120 80 X60) mm (200 150 90) mm (340 260 X200) mm (550 390 240) mm Optics 28 mm 20 mm 20 mm 20 mm Accuracy 0.011 mm 0.015 mm 0.023 mm 0.038 mm Precision 0.006 mm 0.007 mm 0.011 mm 0.019 mm (1σ) Points 0.075 mm 0.75 mm 0.25 mm 0.375 mm spacing Working 330 mm 330 mm 700 mm 1200 mm distance Measurement points (per photo) 1,400,000 1,400,000 1,400,000 1,400,000

Nikon MCT225 computed tomography system The Nikon MCT 225 is an X-ray computed tomography system for metrology of the external and internal features of samples. The instrument takes a number of 2D X-ray images at varying angles around the sample to capture the internal and external geometries of the sample. These 2D images are then reconstructed to form a 3D model, which can then be used to perform dimensional measurements of the sample. Advantages: The most accurate method of measuring internal geometry non-destructively Measurement of pore morphology and distribution is possible STL output for reverse engineering via additive manufacturing Specific metrology focussed system with quoted maximum permissible error of 9 μm + L/50 and 2 μm feature detectability Limitations: X-ray penetration of part materials limits part size Increased X-ray power required for higher attenuation samples reduces accuracy

Specifications: Accuracy (μm) MPE Sample size (maximum) Sample weight (maximum) Manipulator travel Source to detector Detector 9+L/50 (L in X-ray mm) source Diameter 250 X-ray spot mm, height 450 mm 5 kg Enclosure temperature X 480 mm, Y 450 mm, Z 730 mm R 360 1165 mm (nominal) 16 bit 4 Mpx (2000 px 2000 px) Ambient temperature Radiation protection (DIN 54113-2, IRR 99) Enclosure dimensions Magnification 1.6 to 150 System weight Feature 2D detectability radiography 2 (minimum) μm 225 kv/225 W open tube 3 μm microfocus 19 to 21 C 17 to 25 C < 1 μsv/hr W 2214 mm S 1275 mm H 2205 mm 4200 kg

BRUKER Atomic Force Microscope D3100 The Bruker D3100 atomic force microscope is a scanning probe microscope that measures nanometre-scale 3D surface topography. It works by raster scanning a cantilever with a sharp tip across the surface and monitoring the deflection of the cantilever due the presence of surface features. There are three main modes for the AFM to collect surface information: contact mode, tapping mode and magnetic mode. Advantages: There is no optical diffraction limitation Additional information beside surface texture data, e.g. surface elastic modulus, surface hardness, magnetic and electrical properties Almost any type of surface can be measured, even organic (soft) surfaces Ability to measure a very smooth and transparent surfaces Limitations: Very limited areal scanning range Need longer measuring times compared to optical instruments Limited vertical and lateral scanning ranges Not effective for very rough surfaces due to the physical and mechanical limitations of the cantilever

Specifications: Operating mode Maximum travel range (X Y Z) Electronic resolution (analogto-digital) Z-resolution Accuracy Stylus tip diameter Maximum sample size Tapping mode, contact mode and magnetic mode (90 90 6) mm 16 bits (all axes) 50 nm (for 90 μm scan size) 2 nm (for 10 μm scan size) 1% for all axes approximately 10 nm (100 125 50) mm

Zygo NewView 8300 coherence scanning interferometer The Zygo New View 8300 coherence scanning interferometer is a 3D optical surface profiler and provides powerful versatility in non-contact optical surface profiling. All measurements are nondestructive, fast, and require no sample preparation. Advanced software tools characterize and quantify surface roughness, step heights, critical dimensions, and other topographical features, with excellent precision and accuracy. Advantages: Profile heights can range from < 1 nm up to 20000 µm, at high speeds Sub-nanometre surface topography repeatability Measure a wide range of surface types, including smooth, rough, flat, sloped, and stepped Limitations: Measurement uncertainty of surface texture may increase for highly sloped and rough surfaces due to the fundamental limitation of CSI

Specifications: Vertical Scan Range Surface Topography Repeatability Repeatability of RMS Optical Lateral Resolution Spatial Sampling Maximum Data Scan Speed Step Height Repeatability 0.1% Height Response Linearity 30 nm Objective lens Specifications: 150 μm with precision Piezo drive; 20 mm with extended scan 0.12 nm 0.01 nm 0.34 μm (100X objective) 0.04 μm (100X objective 2X zoom) 96 μm/sec Vertical Scan Range 150 μm with precision Piezo drive; 20 mm with extended scan Surface Topography 0.12 nm Repeatability Repeatability of RMS 0.01 nm Optical Lateral Resolution 0.34 μm (100X objective) Spatial Sampling 0.04 μm (100X objective 2X zoom) Maximum Data Scan Speed 96 μm/sec Step Height Repeatability 0.1% Height Response Linearity 30 nm Vertical Scan Range 150 μm with precision Piezo drive; 20 mm with extended scan