X-ray Detectors at DESY

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X-ray Detectors at DESY (Contribution given at the FEL2006 meeting in Berlin) DESY

The European XFEL Time structure: difference with others Electron bunch trains; up to 3000 bunches in 600 μsec, repeated 10 times per second. Producing 100 fsec X-ray pulses (up to 30 000 bunches per second). 600 μs 100 ms 100 ms 99.4 ms 30 000 bunches/s but 99.4 ms (%) emptiness 200 ns X-ray photons 100 fs FEL process

Consequences of Time structure Either: < 10Hz or > 1.5 khz; best 5 MHz All photons arrive in 100 fsec integrating detectors. Experiments should profit from high luminosity (30 000 shots/sec). Every shot is a new experiment (jitter, sample destruction,..)

The Experiments TDR has 8 different application areas 5areas need 2D X-ray detectors: Pump-Probe non-crystalline diffraction Pump Probe crystalline diffraction Coherent Diffraction Imaging Single Particle Imaging X-ray Photon Correlation Spectroscopy

Typical requirements: Direct Holographic Inversion 1.59nm RCP diffraction from magnetised film and pinhole S. Eisebitt, J. Lüning, W. Schlotter, M. Lörgen, O. Hellwig, W. Eberhardt and J. Stöhr, Nature 432, 885-888 (2004)

Typical requirements: Coherent k Diffraction from Crystals Fourier Transform h

Typical requirements: DETECTOR CDI: MUST Total detector angle 120 degrees Pixel Size 0.1 mrad Number of Pixels 20k x 20k Single photon resolution yes (Poisson limit) Tiling tolerated yes Signal rate/pixel/bunch up to 10 6 Timing luminosity optimized Photon energy range [kev] 3-12 Quantum efficiency >0.8 Environment vacuum (input window?) Radiation Hardness 10 16 X-rays Harmonics Discrimination no

How to solve the challenge?

Results of Call for EoI 6 EoIs received: 1 headed by DESY (HPAD) 2 others with DESY as partner (SDD) 1 by Industry Detector Advisory Committee meets on October 23+24 Decision end October (invitation for full proposals).

Hybrid Pixel Array Detector (HPAD) Diode Detection Layer Fully depleted, high resistivity Direct x-ray conversion Silicon, GaAs, CdTe, etc. X-rays Connecting Bumps Solder or indium 1 per pixel CMOS Layer Signal processing Signal storage & output Gives enormous flexibility!

Basic idea: Integrating system Configurable analog frontend Analog Pipeline Pixel Chip Store images of micro-bunches on caps in the pixels (5MHz switching) Readout the images during the 100ms gap Predecessor Chips: Hybrid Pixel Array Detector (HPAD) HEP: H1 strip Analog Pipeline Chip (APC), CMS & Atlas strip and others X-ray Pixel: APAD Cornell We do not start from scratch

Cornell Analog PAD Diode +60V Input Stage IR Rapid framing (SE, IR closed) 1. select storage cap C1 2. Open IR switch (Frame integration begins) 3. Deselect Storage cap (Integration ends) 4. Close IR repeat with C2 C8 Pixel Read (open SE, close RE) Connect storage caps in sequence with output Pixels and caps both independently addressable 2 pf SE Storage Stage RE Output Stage C1 C2 C3 C4 C5 C6 C7 C8 Vb CB C1 - C8: 130 ff

Gasoline fuel injector spray Courtesy Sol Gruner X-ray beam CHESS Beamline D-1 6 kev (1% bandpass) 2.5 mm x 13.5 mm (step sample to tile large area) 10 9 x-rays/pix/s 5.13 μs integration (2x ring period) Fuel injection system Cerium added for x-ray contrast 1000 PSI gas driven 1 ms pulse 1 ATM Nitrogen 13.5 mm 2.5 mm Collaboration: Jin Wang (APS) & S.M. Gruner (Cornell) Injector Beam Fuel Spray (hollow cone) See: Cai, Powell, Yue, Narayanan, Wang, Tate, Renzi, Ercan, Fontes & Gruner Appl. Phys. Lett. 83 (2003) 1671.

Gasoline fuel injector spray Courtesy Sol Gruner 1.8 ms time sequence (composite). 105 images 5.13 μs exposure time. (15.4 μs between frames) 88 frames (11 groups of 8 frames), Avg. 20x for noise. 1000 x-rays/pixel/μs Data taken with 4 projections.

New concepts wide dynamic input range multiple (3) scaled feedback capacitors reduced ADC resolution (8 bit instead of 10 bit) analog + digital (2 bit) pipeline in-pixel CDS? C3 C2 C1 control logic dig. pipeline n x 2 1.5 bit (MSBs) discr. Vthr = VADCmax trimdac leakage comp. analog pipeline ADC 8 bit (L (column ADC or off-chip)

New concepts keep C f fixed scale input current with configurable current mirror: M i = 1, 16, 64 increase dynamic range beyond 10 4 (i > 3) could be implemented in less area switches to override current mirror Cf analog pipeline (column ADC or off-chip) ADC 8 bit discr. Vthr = VADCmax trimdac leakage comp. M : 1 adaptive input current mirror (casoded? additional pmos bias source?) control logic dig. pipeline n x 2 (column ADC or off-chip) 1.5 bit (MSBs)

Analog Pipeline Pixel Rough dimensions: ~ 20 um 2 / cap cell -> 1000 caps (frames) ~ 140 x 140 um 2 -> Pixel size ~ 160 x 160 um 2 500 caps (frames) ~ 100 x 100 um 2 -> Pixel size ~ 120 x 120 um 2 100 caps (frames) ~ 44 x 44 um 2 -> Pixel size ~ 65 x 65 um 2 Readout system: Programmable and flexible pipeline control (Off Chip): Number of X-ray pulses to be stored before readout (1, 10, or n-frames) Adding of X-ray pulses (2 together, every 3 rd pulse, )

Analog Pipeline Pixel: Chip Architecture 32 128 pixels 32 128 32 x 128 = 4096 pixels of 100-1000 caps each 4*10 6 cells F ro = 40 MHz T ro = 10 ms 4 x 32 x 128 = 4096 pixels of 100-1000 caps each 4*10 6 cells F ro = 40 MHz T ro = 10 ms 40 MHZ 10 bit ADC 4 differential analog output ports 40 MHZ 10 bit ADC Parallel Readout Xilinx Rocket IO

Analog Pipeline Pixel: System Architecture

Hybrid Pixel Array Detector (HPAD) Courtesy Christian Broennimann

The SDD project Courtesy Lothar Strueder Silicon Drift Detectors (with DEPFET s) DEPFETs 200 ns i.e. 4.000 µm 200 ns DEPFETs V max 100 µm / ns, V exp 20 µm / ns That means: Δt= 3 ns, Δx = 60 µm total area max : 80 x n 8 mm 2, CHC: unlimited (almost)

SDD (with DEPFET s) Courtesy Lothar Strueder 8 mm ASIC, signal processor PCB Bond connections On-chip electronics Drift of the signal electrons incoming radiation monolithic detector wafer, incl. first amplifying device

Some of the challenges Large dynamic range with low noise (gain switching may be needed) Radiation hardness (in 3 years up to 10 16 photons per pixel) High instantaneous flux (10 4 X-rays in 100 fsec in a few micron of Si) Storing 3000 images inside pixel, while keeping pixel small (100 micron) Very high overall data rate.

Summary We know how to do it, it is difficult and challenging, but doable and interesting Now we wait for the review by the DAC and the decision by the European Project Team for the XFEL