1 a. Project title The Authentication of Sacral Artefacts for Sustaining The Communitarian Viability b. Acronym PATRIPICT c. The Project s abstract The main goal of the project The Authentication of Sacral Artefacts for Sustaining The Communitarian Viability (PATRIPICT) is the providing an innovative service of authentication, studying, evaluation and investigation of sacral artefacts by using an integrated system of modern methods on the bases of the methodology of study and preserving or restoring sacral artefacts. We tackle as the main effect an increasing of the patrimonial value of these artefacts, as well as, an increasing of the cultural touristy interest. We are going to use within the integrated system the following methods: FTIR, RAMAN, UV-VIS, EDAX, RMN, DSC, DTG, raze-x, SEM, AFM, XRF, radiography, biological methods both for the wood support and for the polychrome sheets. The artefacts of this project are icons on wood support dating from the period of 1500-1600 years and are located in Targoviste Stelea Church Romania. d. The general objectives and their future results The fundamental objective of the project is the elaboration of an innovative service of authentication, studying, evaluation and investigation of sacral artefacts by using an integrated system of modern methods. The following steps will be check in order to achieve the fundamental objective: The elaboration of the data library of advanced modern methods involved in the investigation of sacral artefacts; Providing the research methodology in integrated modern methods on fresh and laboratory wetherined wood support and pigments; Providing the research methodology in integrated modern methods wood support and pigments of artefacts; Providing the innovative service as standards and methodologies in integrated methods; The general objectives The elaboration of the data library of advanced modern methods involved in the investigation of sacral artefacts; Providing the research methodology in integrated modern methods on fresh and laboratory wetherined wood support and pigments; Results The state of the art rapport; Providing the research methodology in integrated modern methods wood support and pigments of artefacts; The logical scheme of the modern methods in the integrated system on fresh and laboratory wetherined wood support and pigments; Providing the innovative service as standards and methodologies in integrated methods; Monogarphy about the general standars and methods, specific methodologies succesfuly used in this project. The logical scheme of the modern methods in the integrated system on fresh and laboratory wetherined wood support and pigments; e. The Coordinator of the Project University of Bucharest Bd. Mihail Kogălniceanu, Nr. 36-46,Sector 5,Cod poştal70709, Bucureşti,România, Te/Fax: +40(1)313 17 60, http://www.unibuc.ro f. The partners The first partner P1: The National Institute for Reaserch and Developing of Electrical Engineering ICPE-CA Splaiul Unirii nr. 313, Bucuresti 030138, ROMANIA, Tel.: 0040-21-346.72.31, 346.82.97, Fax: 0040-21-346.82.99, e-mail: office@icpe-ca.ro http://www.icpe-ca.ro
2 The second partner 2: The National Institute for Reaserch for Preserving and Restoring Calea Victoriei 12, sector 3, 030026 Bucureşti Tel./Fax: (4021) 3127225; E-mail: contact@patrimoniul-cultural.ro g. Financial Authority National Center of Programme Management CNMP Programme 4 Consortium in the Priority Research Aria h. the project period 18.09.2007 18.09.2010 i. The activities of the partners Results The state of the art rapport; The logical scheme of the modern methods in the integrated system on fresh and laboratory wetherined wood support and pigments; The logical scheme of the modern methods in the integrated system on fresh and laboratory wetherined wood support and pigments; Monogarphy about the general standars and methods, specific methodologies succesfuly used in this project. Patents. Activities CO The raport about the methods FTIR, RAMAN, EDAX. P1 The raport about the methods DSC, DTG, biologice, AFM, SEM, raze-x P2 The raport about the methods XRF, luminiscenta, fluorescenta. CO Results and area of the methods FTIR, RAMAN, EDAX, microanalysis. Papers and scientific communications. P1 Results and area of the methods DSC, DTG, biologice, AFM, SEM, raze-x. Papers and scientific communications. P2 Results and area of the methods XRF, luminiscenta, fluorescenta. Papers and scientific communications. All partners, know-how. All partners. j. The project`s budget RON 2007 B* 2008 C* B 2009 C B 2010 C B Total C B 45000 290000 290000 115000 740 000 32000 256000 256000 96000 640 000 23000 254000 254000 89000 620 000 100000 800000 800000 300000 2 000 000 B =buget C*=cofinantion * k. Meetings and events C
3-01.10.2007 The kikoff meeting; 15.10.2007 the meeting for listing artefats from Stele achurch Targoviste.
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6 - The shooting raports of the WP I. The WP I raport, 05.12.2007 WP. I. 18.09.2007-10.12.2007 The state of the art about the integrated system, artefacts listing - the consortium meeting on 15.12.2007 about the strategy of the WP II; WP. II The integrated system on wood support of artifacts Result - Raport about the methodology of studying wood support in the integrated system; Activity II.1 Sampling methodology; Activity II.2 The integrated methods on fresh and laboratory wethered wood support; Activity II.3 The integrated methods on artefacts wood support; Activity II.4 Disemintion Scientific papers. Activity II.5 Scientific communication. - The meeting on 05.01.2008 for approving the time table of the WP. II. WP. II / 2008 Time table WP. II Activity II.1 Sampling methodology; II.1.1.Sampling fresh wood, rosin, wax bees; II.1.2. Sampling wood from artifacts; Activity II.2 The integrated methods on fresh and laboratory wethered wood support; II.2.1. Analysis separately and in integrated systems on fresh wood. II.2.2 Results and standard on fresh wood. Activity II.3 The integrated methods on artefacts wood support; II.3.1. Analysis separately and in integrated systems on artifacts. II.3.2 Results and standard on wood artifacts. Activity II.4 Disemintion Scientific papers. Activity II.5 Scientific communication. 01 02 03 04 05 06 07 meet ing meet ing working working 08 09 10
7 - work-shop 21 may 2008, 1600 organized by the coordonator, amf. R2, Univeritatea Bucuresti The painting technique on wood support BUCURESTI 2008 University of Bucharest The Orthodox Faculty of Theology PATRIARHUL JUSTINIAN PROFESSOR COORDINATOR Prof. Univ. Dr. EMANDI ANA STUDENTS BOCA CRISTINA CATALINA, BRAGADIRU MARIANA ENE ELENA, JIPA ANDREIA NASTASE ANASTASIA, PARUS BEATRICE - Dissemination WP.II - working MEETING ATTENDENCE Institutia coordonatoare: Universitatea Bucuresti Bd. Mihail Kogălniceanu, Nr. 36-46,Sector 5,Cod poştal70709, Bucureşti,România, Te/Fax: +40(1)313 17 60, http://www.unibuc.ro 27th Meeting of Dyes in History and Archaeology Istanbul, 8th till 11th October 2008 http://www.dha27.com/ REGISTRATION FORM Name Ana Emandi Title Institution University of Bucharest, Faculty of Chemistry, Department of Inorganic Chemistry Address 23 Dumbrava Rosie, district 2, Bucharest, Romania Tel. 04 0788 465 287; 04 021 2231242 E-mail Emandi1988@ARtelecom.net or ancae@b.astral.ro Fax Professor 04 021 2231242 I wish to contribute a poster x Please give the exact title of your oral presentation or your poster Integrated Methods in Studying Wood Support Weathering of Some Sacral Oil Paints from Stelea-Targoviste Church Authors: Ana Emandi, Ioan Stamatin, Iulian Iordache, Irina Petroviciu, Gheorghe Niculescu Integrated Methods on Studying Wood Support Weathering of Some Sacral Oil Paints from Stelea-Targoviste Church Authors: *Ana Emandia, Ioan Stamatinb, Iulian Iordachec, Irina Petroviciud, Gheorghe Niculescud
8 University of Bucharest, Faculty of Chemistry, 23 Dumbrava Rosie, 010184, Bucharest, Romania, University of Bucharest, Faculty of Physiscs, 405 Atomistilor, Magurele-Ilfov, Bucharest, Romania c INCDIE ICPE - CA Splaiul Unirii, Nr. 313, Sector 3 74204, Bucharest Romania d INCDCR, 12 Calea Victoriei, cod 030026, Bucharest, Romania a b * author for cprrespondence emandi1988@artelecom.net or ancae@b.astral.ro Abstract The purpose of this study is clarifying the degradation type of artefacts wood support of ~450 years old, actually wethered by embedding rosin and bees wax 50 years ago. Thus, changes in the infrared spectra of wood samples due to the decay were recorded. Ass the sub-purpose, possibility of the application of the integrated methods: infrared and Raman spectroscopy, EDAX, XPS, AFM to the measurement of the degree of this decay were examined. Changes in infrared spectra have been recorded with the comparison to wood belongs to different periods of time, fresh bees wax and rosin [1]. Consequently, it had been expected from this study that some changes in molecular structures of wood components would appear even at the initial stage of decay. The shift of the bands at 1730, 1380 and 1050 cm-1 in the FTIR spectra would be better correlated with FT-Raman spectra and the EDAX, XPS, AFM methods [2-4]. Considering the complex decay of rosin, bees wax and wood fiber of the support we developed a paralell the standard protocol of these integrated methods on different types of frash and laboratory weathered wood, bees wax and rosin samples. [3-4]. References 1. İsmail Aydin., Applied Surface Science, Vol. 233, 1-4, 2004, p. 268-274 2. B. Hendarto, E. Shayan, B. Ozarska, R.Carr., The International Journal of Advanced Manufacturing Technology., Publisher Springer London, 28, 7-8, 2006 3.C. Paris, C. Coupry., Journal of Raman Spectroscopy, 36, 1, P. 77 82, 2004 4. J. J. Suñol, D. Miralpeix, J. Saurina, F. Carrillo, X. Colom, Journal of Thermal Analysis and Calorimetry, 80, p. 117 121, 2005 ROLE OF METAL ELECTRONIC PROPERTIES TOWARD THE SECOND-ORDER NONLINEAR OPTICAL RESPONSE A HOMOLOGOUS SERIES OF (DIHYDROXYAZOBENZENE PAINTING AZOPIGMENTS) (Cu, Zn) COMPLEXES *Ana Emandi1, I. Iordache2, I. Stamatin2, Silvia Hodorogea2, Vasilica Chivu1, Mirela Calinescu1 1Universitatea Bucureşti, Bd.Mihail Kogălniceanu nr.36-46, sector 5, Bucharest, Romania 2Institutul National De Cercetare Dezvoltare Pentru Inginerie Electrica, Incdie ICPE-CA, Splaiul Unirii 313 sector 3 CP 030138, Bucharest, Romania SCIENTIFIC PAPERS SUBMITEENG in WORKING l. links - legislatie in domeniul patrimoniului UE si Romania -pagini complementare de institutii si proiecte P1 partner chair dr. Chim. Petru Budrugeac e-mail sanda_budr@yahoo.com P2 partner chair dr. Fiz. Gheorghe Niculescu e-mail niculescu.geo@gmail.com m. The project`s director adressesses Director de Proiect: prof. univ. dr. Ana Emandi University of Bucharest, Faculty of Chemistry 23 Dumbrava Rosie Street, District 2, cod: 020462, Bucharest - Romania Tel: 0788 465 287; tel/fax : 004021 212 48 47 Fax: 004021 2231242 E-mail: ancae@b.astral.ro emandi1988@artelecom.net