MDS-3 EVALUATION SYSTEM FOR METHANE DETECTION INSTRUCTION MANUAL

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MDS-3 EVALUATION SYSTEM FOR METHANE DETECTION INSTRUCTION MANUAL rev. 281014

TABLE OF CONTENTS General Information 3 Application 3 Packaging arrangement 3 Operation conditions 3 Brief Overview of the Components Included 4 Operating instructions 5-6 Precautions 7 Appendices 8 Appendix 1: Lms34LED main parameters 8 Appendix 2: Lms36PD-05 main parameters 9 Appendix 3: Drivers Applicable for the MDS-3 Evaluation System 10 Appendix 4: MDS-3 Testing Results 11 2

GENERAL INFORMATION Application MDS-3 is an evaluation system for CH4 detection based on mid-infrared LED-PD optopair. It is an out-of-the-box solution that can be launched with minimal effort and can provide fast results. Packaging arrangement MDS-3 includes: Three-pass gas chamber that incorporates: o Light-emitting diode Lms34LED o Photodiode Lms36PD-05 o PD preamplifier Built-in driver*/d41/d51 LED Driver (depends on customer request) SDM Synchronous Detector 2-wire cable for LED LED driver connection 4-wire cable for PD preamplifier synchronous detector connection * Built-in driver is incorporated into the gas chamber (in case this driver type is chosen for LED power supply) D-51 LED driver (any other driver can be used) SDM synchronous detector three-pass gas chamber 2-wire cable 4-wire cable light-emitting diode photodiode with preamplifier Operation conditions Indoor operation only. Ingress Protection Rating IP00. 3

BRIEF OVERVIEW OF THE COMPONENTS INCLUDED Three-pass gas chamber. The optical chamber has length of the optical path of 70 80 mm and maximal diameter of 28 mm. Inside the chamber there are: light-emitting diode Lms34LED and photodiode Lms36PD-06, which are placed on spherical mirrors that MDS-3 optical chamber enable triple passage of the LED emission before reaching the PD; PD preamplifier connected to the photodiode; built-in driver (in case this driver type is chosen for LED power supply). Light-emitting diode Lms34LED Standard LMSNT light-emitting diode with 3.4 µm peak wavelength, which is placed on spherical mirror. For detailed information and set of characteristics please refer to Appendix 1. Photodiode Lms36PD-05 Standard LMSNT photodiode with 3.6 µm cut-off wavelength, which is placed on spherical mirror. For detailed information and set of characteristics please refer to Appendix 2. Built-in/D41/D51 LED Driver (depends on customer request) LED Driver is a power supply for Lms34LED. It has a set of adjustable parameters to customise the desired operation mode of an LED. For brief information about drivers, please refer to Appendix 3. For comprehensive information about drivers please refer to the Instruction Manual appropriate to your driver model. D51 LED Driver PD preamplifier PD preamplifier amplifies the current, generated by photodiode, and converts it into voltage signal. There is straight correspondence between PD current and resulting output voltage, i.e. if the photocurrent from photodiode is a meander, the converted signal will be a meander too with the same frequency and pulse duration. SDM Synchronous Detector SDM synchronous detector measures the voltage signal from the output of photodiode preamplifier and converts it to the DC voltage signal proportional to amplitude of voltage from input. For comprehensive information about the synchronous detector please refer to the appropriate Instruction Manual. SDM Synchronous Detector 4

OPERATION INSTRUCTIONS Connections 1. Connect the 2-wire cable to the LED connection terminal block of LED driver. Note! Red wire must be connected to the red dot or + sign of the driver socket. 2. Connect the round connector of the 2-wire cable to the socket of MDS-3 optical chamber marked with LED sign. 2-wire cable socket LED sign round connector 3. Connect the round connector of the 4-wire cable to the socket of MDS-3 optical chamber marked with PD sign. 4. Connect the red and black wires of 4-wire cable to the signal input terminal block of SDM synchronous detector. Note! The red wire must be connected to the + sign of the signal input terminal block of synchronous detector. 5. Connect the white and uninsulated wires of 4-wire cable to the power output terminal block of SDM synchronous detector. Note! The red white must be connected to the + sign of the power output terminal block of synchronous detector. 6. Connect the synchronisation output of the LED driver with the synchronization input of the synchronous detector via synchronization cable. 7. Select the needed mode of the LED driver. Note! You can find out more about driver modes and their adjustment in the appropriate driver Instruction Manual. 8. Connect signal output terminal block with signal observing device (multimeter, oscillograph or PC via ADC). 9. Connect a 12V DC stabilized power supply to the LED driver. It will turn on. 10. Connect a 12V DC stabilized power supply to the SDM synchronous detector. It will turn on. 5

OPERATION INSTRUCTIONS to 12V DC stabilized power supply to a signal observing device (multimeter, oscillograph or PC via ADC) to 12V DC stabilized power supply 9 D-51 LED driver (any other driver can be used) 6 7 synchronisation cable 8 6 1 SDM synchronous detector 10 2 3 5 4 6

PRECAUTIONS Turn on the power supply of the LED Driver and SDM synchronous detector only after all connections are made and tested. Do not switch driver regimes during operation. Do not disassemble the optical chamber; otherwise the optical system will be damaged. Do not use multimeter to control and adjust current of the LED. Note! Please refer to your provider if you have any questions. 7

APPENDIX 1 Lms34LED Main Parameters (QCW operation mode, f=0.5 khz, T=24 C) Parameters Units Conditions Ratings Min Typ Max Peak emission wavelength m T=300 K, I = 150 ma qcw 3,30 3,40 3,49 FWHM of the emission band nm I = 150 ma qcw 400 500 600 Quasi-CW Optical Power W I = 200 ma qcw 25,0 35,0 45,0 Pulsed Peak Optical Power W I=1 А, f=1 khz, duty cycle 0.1% 320 400 480 Voltage V T=300 K, I=200 ma 0,2-0,5 Switching time ns T=300 K 10 20 30 Spectra at different currents (qcw, T=300 K) Spectra at different temperatures (qcw, I=150 ma) Intensity, a.u. 60 50 40 30 20 10 50mA 100mA 150mA 200mA 0 2700 3000 3300 3600 3900 4200 Wavelength, nm Intensity, a.u. 70 60 50 40 30 20 10 2 C 22 C 50 C 0 2700 3200 3700 4200 Wavelength, nm LED Power Characteristic (quasi-cw mode, T=300K) 250 200 Current, ma 150 100 50 0-1000 -500 0 500 1000 1500-50 Voltage, mv LED Typical Current-Voltage Characteristics (T=300K) 35,0 30,0 25,0 Power, W 20,0 15,0 10,0 5,0 0,0 0 50 100 150 200 Current, ma 8

APPENDIX 2 Lms36PD-05 Main Parameters (T=24 C) Photodiode Parameters Conditions Symbol Value Units Cut-off wavelength T=300 K λ cut 3.6 mm Max. sensitivity wavelength (>90%) T=300 K λ p 2.2 3.4 mm Dark current T=300 K, Vr=-0,1 V I d 0.5 1 ma Shunt resistance T=300 K, Vr=-10 mv R sh 0.2 0.8 kω Capacitance T=300 K, λ=λp C 600 1400 pf Sensitivity T=300 K, λ=λp S 1.0 1.5 A/W Detectivity T=300 K, λ=λp D* (4-14)*10 9 cm. Hz 1/2. W -1 Sensitivity, arb. u. Spectral response (typical) 1 0,8 0,6 0,4 0,2 0 2000 2500 3000 3500 4000 Wavelength, nm Sensitivity, arb. u. 1 0,8 0,6 0,4 0,2 Temperature shift of spectral response 11 С 25 С 50 С 0 3000 3200 3400 3600 3800 Wavelength, nm 9

APPENDIX 3 Drivers Applicable for the MDS-3 Evaluation System LED driver D-41 D-41 Driver provides Pulse mode operation. Using this mode it is possible to choose one of five current values (0.2, 0.6, 1, 1.5, 1.9 A) and select one of four frequencies (0.5, 2, 8 and 16 khz) and choose pulse duration within four values (2, 5, 10 and 20 µs). LED driver D-51 D-51 Driver has the same characteristics as D-41 but also has another important feature: Temperature control possibility to define LED p-n junction temperature using current-voltage dependence. Driver generates the low current signal for plugged LED, measures and outputs the voltage. Using the obtained voltage value it is possible to calculate the intrinsic LED temperature. Built-in driver Built-in driver can be chosen instead of D-41/D-51 drivers in case the customer needs more compact design of the evaluation system. Built-in driver is incorporated into the CDS-3 optical chamber and works in optimal driving mode for the LED: 1 A current, 500 Hz frequency and 20 µm pulse duration. 10

APPENDIX 4 MDS-3 testing results Signal Output with Different Methane Concentration and 90% relative humidity (RH) Gas MDS-3 Methane Detection Results at ppm Level and 90% Relative Humidity ppm Signal Output (V) Net Signal Output (mv) Standard Deviation (mv) Noise (mv) Resolution (ppm) Air (Dry Bottled) 0 1.1638-0.0466 0.4801 1.3937 (NA) CH4 + Air 500 1.1571 6.6679 0.6196 1.8589 279 CH4 + Air 1000 1.1560 7.8138 0.8170 2.4511 627 CH4 + Air 10000 1.1267 37.1290 0.7471 2.2413 1207 CH4 (50% LEL) 25000 1.0957 68.0611 1.8914 5.6743 4169 CH4 (~90% RH) 25000 1.0732 90.5848 1.3851 4.1554 2294 Testing conditions: Settings of the D-51 driver: pulse current 1A; pulse width 20 μs; pulse frequency 500 Hz. Settings of the SDM synchronous detector are: input polarity inversion jumper open; averaging time 100μs; output signal gain 1. 11