TABLE OF CONTENT. 1.0 Introduction Theory Results Discussion Conclusion References

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ABSTRACT This process control laboratory is about to run open and closed loop process. An open loop is run in manual mode while closed loop is run in automatic mode. In this experiment, five closed loop analysis are involved which comprises of Level Control Process (LIC 11), Air Flow Control (FIC 91), Air Pressure Control (PIC 92), Flow Control (FIC 21) and Liquid Flow Process (FIC 31). By using the response curve from the loop analysis, Response Rate (RR), Time delay (T d ) and Time constant (T c ) are calculated by using Reformulated Tangent Method. Then, Ziegler-Nichols and Cohen Coon tuning rule formula are used in order to calculate the optimum value. By using the calculated value based on Ziegler-Nichols, open loop test is running. The process is run in automatic mode. Three main tests have been conducted in each of the open loop which includes tuning test, set point change test and load disturbance test. When we increase the changing in MV value, the value of controller gain, K c will increase and can affect the respond of the process to become more faster and the process become more stable. By decreasing the controller gain, K c it also reduce the oscillatory and make the process become more stable. The integral time, I value is decreased and it accelerates the process to the set point 2

TABLE OF CONTENT TITLES PAGE 1.0 Introduction 4 2.0 Theory 9 3.0 Results 18 4.0 Discussion 24 5.0 Conclusion 26 6.0 References 27 7.0 Appendices 28 3

1.0 INTRODUCTION Process control keeps processes within specified boundaries and minimises variations [5]. Nowadays, wide variety of modern process control systems have been installed progressively in most industrial sites in order to help maintain throughput, quality, yield and energy efficiency as well as to ensure safe and profitable operation. The measurement and control system is the central nervous system of any plant, as it operates at different levels that sense change and initiate actions [5]. Process control system refers to the control of one or more process variables such as ph, level, temperature, flow and pressure. In process control system, the process variables is compared to a set point by the controller and the results of the comparison will be utilized to control the process in such a manner that the process variable will be substantially equal to the set point for the process variable (Robert W. Rutledge, 1980). Nowadays, the applications of the process control are huge in the industrial field. For instance, advanced process control plays an important role in chemical and process industry. PID control, conventional advanced control and linear/nonlinear model predictive control have been used in industry in order to increase the productivity. The industrial PID has many options, tools and parameters for dealing with the wide spectrum of difficulties and opportunities in manufacturing plants. The PID controller is an essential part of every control loop in the process industry (Astrom K., Hagglund T., 2006). Studies have shown that the PID provides an optimal solution of the regulator problem (rejection of disturbances) and with simple enhancements, provides an optimum servo response (setpoint response) (Bohl A., McAvoy T., 1976). Test show that the PID performs better than Model Predictive Control (MPC) for unmeasured disturbances in terms of peak error, integrated error or robustness (McMillan G., 2004). The PID controller in the modern Distributed Control System (DCS) has an extensive set of features and their importance for addressing challenging applications and control objectives for common unit operation applications in the process industry. In the production for most new pharmaceuticals, bioreactors are used due to proteins too complex to be produced by chemical processes. Biopharmaceutical batch processes are predominantly batch because of the concern for the build up of the toxins and genetically deficient cells with continuous processes and the need to get new drugs to market quickly. In bioreactors, ph, temperature and dissolved oxygen are the important loops to be considered. Generally, for a well designed system the allowable controller gain is extremely limited only by the measurement noise because of the ratio of deadtime to time constant is relatively 4

small. The high controller gain in combination with the extremely slow disturbances translates to exceptionally tight PID control (Ramon V., Antonio V., 2011). In the system, no overshoot at the start of the batch essentially with getting to temperature setpoint as fast as possible is being concerned. If there is no concern about batch cycle time and low temperatures do not cause seed cell degradation, a PID structure of integral mode on error and proportional and derivative modes on PV is used to eliminate overshoot (McMillan G., 2010). It is usually less than ideal for the automation and bioreactor system design. In bioreactor, ph loops and dissolved oxygen will interact whenever the piping and spurger for the injection of oxygen or air for dissolved oxygen control and addition of carbon dioxide for ph control are not completely separated. For this case, the interaction between ph and dissolved oxygen loops can be reduce with the use of half decoupler and enhanced PID. Wireless ph transmitters have been found to eliminate the spikes commonly seen in bioreactor loops (McMillan G., Baril R., 2010). As sliding stem (globe) control stem valves are not suitable for sanitary and sterilization-in-place (SIP), thus, most of bioreactor loops does not use it. The alternative final control elements used may have a poor resolution or sensitivity limit and backlash. Hence, the associated limit cycles can be extinguished with the enhanced PID. Otherwise, enhanced PID can make sample time for a bioreactor batch that takes 1 to 2 weeks fast enough to do closed loop control by dealing with the analyzer cycle time and resolution limits. Chemical reactors set the stage for the production of bulk chemicals, intermediates, petrochemicals, polymers, pharmaceutical chemicals and speciality chemicals (Ramon V., Antonio V., 2011). Batch reactors are commonly used in pharmaceutical industries and in the production of special chemicals and other products predominantly use continuous reactors. The temperature PID is the most important controller since the reaction rate is often an exponential function of temperature via the Arrhenius Equation (Ramon V., Antonio V., 2011). The deadtime to time constant ratio for well mixed continuous reactors and the deadtime to integrating process gain ratio for batch reactors are incredibly small (<0.001) (Ramon V., Antonio V., 2011). The result is a permissible PID gain much larger than users are accustomed to (>50) and exceptionally tight temperature control (Ramon V., Antonio V., 2011). Since the most important task of the utility system is to satisfy the demands of the temperature PID, the transfer of variability by the PID from the reactor temperature to its utility system is maximised. Performance limitation is due to the accuracy of the temperature sensor and the threshold sensitivity and resolution of the final control elements. Premium Resistant Temperature Detectors (RTD) and sliding stem valves with digital positioners should be used to allow the full capability of the PID to be realized [12, 13, 14]. 5

The ph control of neutralizers can be particularly challenging due to the extreme nonlinearity and sensitivity of the ph measurement as a result of the exponential relationship between ph and hydrogen ion activity [9]. The changes in controller gain and the rangeability and threshold sensitivity of the final element needed are extraordinary. PID gain changes of 1000 to 1 and a final element rangeability requirement of 10 000 to 1 are possible with strong acid and base system (Ramon V., Antonio V., 2011). In order to keep waste streams in compliance with environmental regulations, it is necessary to determine the number of neutralization stages by precision of the final element. The limit cycle amplitude from threshold sensitivity and resolution limits can be extremely large due to amplification by the steep slope of the titration curve (McMillan G., 2003). The 7 ph value for a broken electrode or wire and the failure to last value of a coated electrode are insidious (McMillan G., 2003). Some solutions that can be considered in this case are signal linearization, adaptive tuning, split range control, valve position control (VPC) and the enhanced PID. Controlled variable can be translated from ph to reagent demand per the titration curve by using signal linearization. While, changes in the titration curve and process dynamics can be corrected with adaptive tuning. Neutralization with both acids and bases can be handled with split ranged control. Whereas, in order to keep good throttle range for ph control, a VPC can adjust a large (coarse) valve to keep a small (fine) valve. Otherwise, PVC can also maximize the use of waste and low cost reagents. Portable wireless ph transmitters can eliminates spikes from EMI as well as optimize the control location. Finally, the enhanced PID can eliminate oscillations from split range point discontinuities and from valve backlash, threshold sensitivity, and resolution, reduce interactions between the small and large valves, prevent overreaction to ph electrode failures, and extend wireless battery life [11, 16]. Furthermore, liquid level control plays important role in industrial application as in food processing industry, dairy, filtration, effluent treatment, nuclear power generation plants, pharmaceutical industries, water purification systems, industrial chemical processing and spray coating and boilers in all the industries. The typical actuators used in liquid level control systems include pumps, motorized valves, on-off valves and level sensors such as displacement float, capacitance probe and pressure sensor provide liquid level measurement for feedback control purpose so that as per the process requirements the fluids could be controlled (Farhad A., 2011). Basically, the objective of the controller in the level control system is to maintain a level set point at a given value and be able to accept new set point values dynamically. In controlling the level, commonly conventional PID is used to utilize it. A PID gain is tune automatically by auto tuning in a Simulink model containing a PID controller block. By tuning the PID, it allows to achieve a good balance between performance and robustness. It will automatically compute a linear model of the plant. The plant will be 6

considered by PID tuner to be the combination of all blocks between the PID controller input and output. Other than the controller itself, the plant includes all blocks in the control loop. The main objectives of PID tuner are closed-loop stability (in which system output remains bounded for bounded input), adequate performance (in which closed loop system tracks reference changes and suppresses disturbance as rapidly as possible) and adequate robustness (the loop design has enough gain margin and phase margin to allow for modelling errors or variations in system dynamics (Farhad A., 2011). By adjusting response time, design modes of PID tuner refine the controller design. This makes the closed loop response of the controlled system slower or faster. While, by separately adjust loop bandwidth and phase margin, an extended design mode of PID tuner refine the controller design. The controllers will response faster to changes in the reference or disturbances in the loop whenever the loop bandwidth is larger. The more robust the controller is against modelling errors or variations in plant dynamics if the phase margin is larger. One of the reasons that make Proportional-integral-derivative (PID) controllers is widely used in industrial control systems is due to the reduced number of parameters to be tuned. Zieglar-Nichols method is one of the most popular design techniques that are commonly used. The conventional PID controller is replaced by Ziegler-Nichols tuning PID controller to make them more general and to achieve the minimum steady state error, also to improve the other dynamic behaviour (Rajkumar, A. Patra, Vijay, 2012). Most process industries used PID controller to control the plant (system) for the desired set point. PID control method is the most popular among all control method because of it is flexible and simple. PID controller is tuned by determination of proportional (KP), derivative (KD) and integral (KI) constants. This method is used when the system is in open loop configuration. PID control is the proportion of error (P), integral of error (I), differential of error (D) control. Z- N PID controller is controlling the plant or system by continuously monitoring plant output which is known as process value with the desired process value known as set point of the system [18]. The difference between process value and set point that manipulates by PID controller is known as error. In the conventional controlling method the transfer function of plant should be calculated in order to find out various parameters and the value of PID constants. But in this method there is no necessary to derive the transfer function of the system. Thus, Z-N PID controller is monitoring the plant depending on set point and process value and irrespective of the nature of plant [19, 20]. The main features of PID controllers are the capacity to eliminate steady-state error of the response to a step reference signal because of integral action and the ability to anticipate output changes when derivative action is employed [18]. In a power plant, both active and 7

reactive power demands continually vary the rising or falling trend. Power input must therefore be continuously regulated to match the active power demand, otherwise the machine speed will change with consequent change in frequency, which may be highly undesirable [18]. The excitation of generators must be continuously regulated to match the reactive power demand with reactive generation, failing which the voltage at various system buses may go beyond the prescribed limits [18]. It is necessary to maintain the frequency of the power system constant. The governors adjust the input to bring the frequency with in permissible limits [21]. PID controllers is tuned as to make the plant more general and to achieve the minimum steady state error as well as to improve the other dynamic behaviour. The Ziegler-Nichols step response method provides systematic means to adjust the proportional gain in order to have no overshoot on the closed-loop step-response [18]. In the design of plant control system, the PID controllers can be designed associated with under damped step responses. Instead of transfer function of the system, PID constants are strongly depends on the set point and tune controller feature that can improve the system performance. PID controllers attributed to the controllers effectiveness in a wide range of operation conditions, its functional simplicity, and the ease with which engineers can implement it using current computer technology. Hence, PID control algorithms are popular and offer many benefits such ease of use, new development help to implement other PID controller variants and control for common industry application. 8

2.0 THEORY PID controllers are capable stabilizing processes at any set point by utilizing a mathematical function in the form of the control algorithm [1]. Process stability of a PID control loop depends upon the proportional, integral and derivative constants used [1]. An optimum proportional (P), integral (I) and derivative (D) values can be obtained using several simple techniques performed on an open loop test. Open loop test can be done with several steps, firstly by stabilizing the process in manual mode. Then, making step change ( MV) of 5 to 20% to the controllers output and record the initial as well as the final MV value. Finally, response of the process variable is recorded until the process reaches a new steady state level. An open loop test might be in self regulating process or non self regulating process. In open loop process identification, there are several quick and easy techniques that can be approached. These techniques include tangent method, reformulated tangent method and numerical method. Those methods extract most vital information about the process dynamic, namely process dead time (T d ) and the response rate (RR). This information then is used in the tuning rules, such as Zieglar-Nichols in order to estimate the optimum P, I and D for the controller. In the tangent method, an optimum PB, I and D is found at the maximum slope. The process dead time (T d ) and the response rate (RR) are analyzed by drawing a tangent line to the steepest point of the response curve. By the definition, the process dead time (T d ) is a period of time between starting point of step input and the intersection of old steady state baseline and tangent line [2]. Figure 2.1 shows the step change made ( MV), the drawn tangent line and the estimated process dead time (T d ). 9

Figure 2.1: A step change of MV (bottom) and the self regulating process response curve (top). (Abdul Aziz Ishak, 2011) The process response rate (RR) is defined [1,2] as, RR = PV/ t MV maximum slope = MV - - - - - (1) Where, RR = response rate, 1/time PV = change in measurement, % t = change in time, time MV = change in controllers output, % T d and RR are incorporated in the tuning rule for the optimum PID calculation [1]. In the reformulated tangent method, the open loop response curve is analyzed and viewed in different perspective. This method is based on tangent method but utilized trigonometry to estimate the gradient [2]. Figure 2.2 shows the same response curve as in Figure 2.1 but is being analyzed in different perspective. 10

Figure 2.2: Transforming process rate into trigonometric form [1]. (Abdul Aziz Ishak, 2011) Based on the Figure 2.2, the process response rate (RR) of equation (1) is then reformulated by, PV/ t MV = y/ x MV - - - - - (2) But the right-hand side and the left-hand side of the equations are dimensionally incorrect. Thus, by balancing the units and place the appropriate scaling factors to the right hand side of the equation, equation (2) will transforms into equation (4). % time = lengt h lengt h PV/ t MV = y a x b MV ( % lengt h ) ( time lengt h ) - - - - - (3) - - - - - (4) Where, a = scaling factor for y-axis, % / length b = scaling factor for x-axis, time / length 11

As y x = tan θ, equation (4) transforms into, RR = PV/ t MV tan θ a = MV b - - - - - (5) T d (time) = T d (length) b - - - - - (6) T c (time) = T c (length) b - - - - - (7) Time constant formulation based on Reformulated Tangent Method [2]. Figure 2.3: Reformulated tangent method for time constant (Abdul Aziz Ishak, 2011). PV nss PV oss tan θ = Tnss Td ( b a ) - - - - - (8) PV nss PV oss tan θ = Tc ( b a ) - - - - - (9) T c = b a nss PV oss (PV ) - - - - - (10) tan θ 12

Dead time formulation based on Reformulated Tangent Method [2]. Figure 2.4: Reformulated Tangent Method for dead time (Abdul Aziz Ishak, 2011) PV nss PV oss tan β = Tnss ( b a ) - - - - - (11) Tnss = PVnss PVoss tan β ( b a ) - - - - - (12) T d = T nss T c - - - - - (13) PV nss PV oss T d = tan β ( b PV nss PV oss ) a tan θ ( b a ) - - - - - (14) T d = (PV nss PV oss ) ( b a ) { 1 tan β 1 tan θ } - - - - - (15) 13

Numerical analysis on openloop response data Figure 2.5: Numerical formulation for response rate, RR (Abdul Aziz Ishak, 2011) PV 1 PV 1 Slope = 2 h - - - - - (16) Therefore, the response rate, RR becomes: RR = slope MV = PV 1 PV 1 2 h MV - - - - - (17) Figure 2.6: Numerical formulation for dead time, T d (Abdul Aziz Ishak, 2011) 14

Slope at (T d, PV oss ) = slope at (t 1, PV 1 ) PV 1 PV oss t1 Td PV 1 PV 1 = 2 h - - - - - (18) T d = t 1-2 h [ PV 1 PV oss PV 1 PV 1 ] - - - - - (19) Figure 2.7: Numerical formulation for time constant, T c (Abdul Aziz Ishak, 2011) Slope at (T nss, PV nss ) = slope at (t 1, PV 1 ) PV nss PV oss Tnss Td PV 1 PV 1 = t1 t 1 - - - - - (20) T c = 2 h [ PV nss PV oss PV 1 PV 1 ] - - - - - (21) 15

Ziegler-Nichols open loop tuning rule (Abdul Aziz Ishak, 2011) Takahashis openloop tuning rule (Abdul Aziz Ishak, 2011) 16

Cohen Coons openloop tuning rule (Abdul Aziz Ishak, 2011) 17

3.0 RESULT 3.1 Summary of process dynamics of various control loops Control Loop Parameters Reformulated Tangent Method Response rate, RR (s -1 ) 0.03 Level Control (LIC 11) Deadtime, T d (s) 3.75 Time Constant, T c (s) 36.25 Response rate, RR (s -1 ) 1.796 Air Mass Flowrate (FIC 91) Deadtime, T d (s) 3.75 Time Constant, T c (s) 1.25 Response rate, RR (s -1 ) 0.67 Liquid Flow (FIC 21) Deadtime, T d (s) 1.25 Time Constant, T c (s) 2.5 Response rate, RR (s -1 ) 0.0885 Gas Pressure Control (PIC 92) Deadtime, T d (s) 3.75 Time Constant, T c (s) 21.25 Response rate, RR (s -1 ) 0.431 Liquid Water Flowrate and Level Control (FIC 31) Deadtime, T d (s) 3.0 Time Constant, T c (s) 3.04 Table 3.1: Summary of process dynamics of various control loops 18

3.2 Summary of optimum controller settings for PI controller based on Ziegler-Nichol s and Cohen-Coon for Reformulated Tangent Method. Control Loop Parameters Reformulated Tangent Method Ziegler-Nichols Cohen-Coon Level Control (LIC 11) Proportional Band, PB % 12.5 11.14 Controller Gain, K c 8.18 8.97 Integral Time, I (s) 12.49 10.27 Air Mass Flowrate (FIC 91) Proportional Band, PB % 748.26 529.18 Controller Gain, K c 0.134 0.1889 Integral Time, I (s) 12.49 2.09 Liquid Flow (FIC 21) Proportional Band, PB % 93.05 80.11 Controller Gain, K c 1.075 1.25 Integral Time, I (s) 4.16 2.07 Gas Pressure Control (PIC 92) Proportional Band, PB % 36.87 32.66 Controller Gain, K c 2.71 3.06 Integral Time, I (s) 12.49 9.15 Liquid Water Flowrate and Level Control (FIC 31) Proportional Band, PB % 143.65 118.35 Controller Gain, K c 0.696 0.84 Integral Time, I (s) 9.99 3.43 Table 3.2: Summary of optimum controller settings for PI controller based on Ziegler-Nichol s and Cohen-Coon for Reformulated Tangent Method. 19

3.3 Tuning Test, Set point Test and Load Disturbance Test Control Loop Parameters Tuning Test Level Control (LIC 11) Air Mass Flowrate (FIC 91) Liquid Flow (FIC 21) Gas Pressure Control (PIC 92) Controller Gain, K c 8.18 Integral Time, I (s) 12.49 Controller Gain, K c 0.134 Integral Time, I (s) 12.49 Controller Gain, K c 1.07 Integral Time, I (s) 4.16 Controller Gain, K c 2.71 Integral Time, I (s) 12.49 Table 3.3: Result for Tuning Test Control Loop Parameters Old New Level Control (LIC 11) Set Point (mm) 500 550 Air Mass Flowrate (FIC 91) Set Point (kg/h) 25 27.5 Liquid Flow (FIC 21) Set Point (m 3 /h) 3.99 4.39 Gas Pressure Control (PIC 92) Set Point (psig) 9.8 11.0 Table 3.4: Result for Set Point Test 20

Control Loop Parameters Old New Level Control (LIC 11) MV, % 47.3 57.3 Air Mass Flowrate (FIC 91) MV, % 33.2 43.2 Liquid Flow (FIC 21) MV, % 64.6 74.6 Gas Pressure Control (PIC 92) MV, % 69.4 79.4 Table 3.5: Result for Load Disturbance Test 21

3.4 Numerical method for FIC 31 Times PV (m 3 /hr) PV (%) MV (%) Z-N Z-N Z-N C-C C-C C-C RR, 1/s Td, s Tc, s PB, % Kc I u=td/tc PB, % Kc I 11:30:37 0 1.0056 33.52 40 11:30:38 1 1.0056 33.52 40 0.000 11:30:39 2 1.0056 33.52 40 0.000 11:30:40 3 1.0056 33.52 45 0.203 11:30:41 4 1.0664 35.55 45 0.431 3 3.04 143.65 0.696 9.99 0.99 118.35 0.84 3.43 11:30:42 5 1.1349 37.83 45 0.348 11:30:43 6 1.1709 39.03 45 0.180 11:30:44 7 1.1889 39.63 45 0.060 11:30:45 8 1.1889 39.63 45 0.045 11:30:46 9 1.2025 40.08 45 0.045 11:30:47 10 1.2025 40.08 45 0.000 11:30:48 11 1.2025 40.08 45 0.000 11:30:49 12 1.2025 40.08 45 Table 3.6: Result of FIC 31 for numerical method 22

3.5 Numerical Method for TIC 91 Times PV ( C) PV (%) MV (%) Z-N Z-N Z-N Z-N C-C C-C C-C C-C RR, 1/s Td, s Tc, s PB, % Kc,s I,s D,s u=td/tc PB, % Kc,s I,s D,s 10:12:20 0 30.0273 15.0137 5.672 10:12:10 1 30.0273 15.0137 5.672 0.000 10:12:00 2 30.0273 15.0137 5.672 0.001 10:11:50 3 30.0508 15.0254 10.67 0.007 10:11:40 4 30.1758 15.0879 10.67 0.021 10:11:30 5 30.4766 15.2383 10.67 0.030 10:11:20 6 30.7773 15.3887 10.67 0.027 10:11:10 7 31.0195 15.5098 10.67 0.031 10:11:00 8 31.3906 15.6953 10.67 0.034 4.046 5.8726 11.325 8.827 8.0922 2.0231 0.689 8.19 11.30 8.14 1.32 10:10:50 9 31.6914 15.8457 10.67 0.030 10:11:40 10 32.0000 16.0000 10.67 Table 3.7: Result of TIC 91 for numerical method 23

4.0 DISCUSSION Practically, this experiment has been run open loop test for Level control process (LIC 11), Air flow control (FIC 91), Air pressure control (PIC 92) and flow control (FIC 21). By using the response curve from the loop test, Response Rate (RR), Time delay (T d ) and Time constant (T s ) are calculated by using Reformulated Tangent Method formula. Then, Ziegler- Nichols and Cohen Coon tuning rule formula are used in order to calculate the optimum value. As Pressure, Level and Flow is fast process, so that PI formula is used in order to calculate the optimum value for the fast control process. From the comparison that has been made, it s only a small difference between the value that calculated by using Ziegler-Nichols method and the value using Cohen Coon method. Then, values calculated using PI formula for Ziegler-Nichols is used to running the closed loop control. After set up and running the process control system in Auto mode, enter the value of controller gain (K c ) and integral time (I) that has been calculated manually using Ziegler- Nichols into the system control. During the process, the response curve is observed and analyzed. Whenever the response curve is oscillating and active, the process is tuned until the response curve is stable and process is closed to the set point. Tuning is the process of setting control loop gains or other control variables to achieve optimum value and stable performance. The value of controller gain, K c and integral time, I are the control variables that was considered to achieve optimum controller setting. In this experiment, there is no exact value for the process to achieve an optimum performance. Under steady state condition, when the graph line of set point and process (PV) variable is equal then it is considered as optimum performance. In tuning process, whenever the response curve are oscillate very fast, the value of the controller gain, K c have to be reduce by divide the original value by 2 or 4 and increase the integral time, I value by multiply by 2 or 4 or with other value. For the Level Control (LIC 11), the value of open loop test was entered at the closed loop test. In the close loop test, the response of the graph that getting from the open loop is oscillate. The value of K c is divided by 4, so that the value of K c entered now is 8.18. The response curve now became stable. Then, set point test is made. Set point is increase from 500 to 550 and then waits until the response curve stable. Next, by performed the load disturbance test, the value of MV is increased from 47.3 to 57.3%, and observes the response curve as well as wait until the response curve become stable. Summary for all control loop and all test result in table 5, 6 and 7. 24

The same method is used for Air Flow Control (FIC 91), Air Pressure Control (PIC 92) and Flow Control (FIC 21). For Air Flow Control (FIC 91), value for controller gain, K c now is 0.134 and the value of integral time, I is 12.49s. As the response curve is fluctuation and not stable, the K c value is divided by 2, 0.535 and multiply the I value by 2, 16s. By decrease the controller gain, K c value, the process become slower and less oscillatory, but by increased the integral time, I value, and it will accelerate the process towards the set point. The process is waiting until it become stable. The set point test is run by increased the SP value from 25 to 27.5 kg/h and wait for the process until it became stable before proceed with the load disturbance test. By increase the MV value from 33.2 to 43.2, it can be seen that the process line will increase rapidly for a moment, then being decreased and become stable. For Air Pressure Control (PIC 92), value for controller gain, K c now is 2.71 and the value of integral time, I is 12.49 s. The process curve is stable and reaches the set point. Then, continue with set point test by increased the value of set point from 9.8 to 11.0 psig. Once the process is stable, continue with load disturbance test by increase the MV value from 69.4 to 79.4%. For Flow Control (FIC 21), value for controller gain, K c now is 1.075 and the value of integral time, I 4.16 s. Due to fluctuation and the response curve is not stable, then the value of K c is divided by 2, 1.875 while the I value is multiply by 2, 26.70s. The response curve is now stable and near to the set point. Then, make the set point test by increase the set point from 3.99 to 4.39 m 3 /h. It can be observed the MV curve is increased rapidly before decreased and become stable. Once the process curve is stable, continue the test with load disturbance test by increasing the MV value from 64.6 to 74.6%. Set point is the desired value for the operating variable. After run the steady state experiment, the initial set point value was changed by an increment of 5%. These changes represent the situation in which the plant operator occasionally changes the value of set point and allows the considerable time for the control system to respond. In this experiment, all the graphs showed that the process line has the same reaction where it moves towards the set point and after a while it will reached stability where the process value and set point value is almost equal. Under load disturbance, the system will experienced disturbance that cause a large, sustained deviation of the controlled variable from its set point. In this test, the initial load disturbance value was also increased by 5%. Before entering the value, the system is change in manual mode and after the value was entered, the system is quickly changed back 25

into auto mode. Through the result, it can be seen that the longer time needed for the process line to return to the set point, the process will become more unfavourable since it affect the process line and also the production rate. The output lines also need to be considered because if the output line is not smooth and stable then the utilities are high. 5.0 CONCLUSION As a conclusion, this experiment had achieved its objective which is to find the optimum PI for Level Control Process (LIC 11), Air Flow Control (FIC 91), Air Pressure Control (PIC 92) and Flow Control (FIC 21) by using the Reformulated Tangent Method and by using Ziegler-Nichols tuning rules. When we increase the changing in MV value, the value of controller gain, K c will increase and can affect the respond of the process to become more faster and the process become more stable. By decreasing the controller gain, K c it also reduce the oscillatory and make the process become more stable. The integral time, I value is decreased and it accelerates the process to the set point. 26

6.0 References 1. Abdul Aziz Ishak & Muhammed Azlan Hussain, (2000). Reformulation of the tangent method for PID controller tuning. Process Control Engineering Online, May 2013, http://aabi.tripod.com 2. Abdul Aziz Ishak (2011), Process Control Practices note. 3. http://www.controlguru.com/pages/table.html 4. http://www.amazon.com/principles-practices-automatic-process- Control/dp/0471431907 5. http://www.carbontrust.com/media/147554/ctv063_industrial_process_control.pdf 6. Astrom K., Hagglund T. (2006) Advanced PID Control, ISA, Research Triangle Park (Industrial application of PID) 7. Bohl A., McAvoy T. (1976) Linear feedback vs. time optimal control. II. The regulator problem, Ind. Eng. Chem., Process Des. Dev., Vol. 15, No. 1 (Industrial application of PID) 8. McMillan, G. (2004) Models Unleashed, ISA, Research Triangle Park (Industrial application of PID) 9. Ramon Vilanova, Antonio Visioli (2011), PID Control in the third Millennium: Lessons Learned and New Approaches, Springer. (Industrial application of PID) 10. McMillan G., (Dec. 8, 2010) Exceptional opportunities in process con-trol, ISA short course, Saint Louis http://www.modelingandcontrol.com/2010/12/exceptional_opportunities_in_p_18.html (Industrial application of PID) 11. McMillan G., Baril R. (Aug. 2010) ph measurement and control, Chemi-cal Engineering (Industrial application of PID) 12. McMillan G., (Dec. 8, 2010) Exceptional opportunities in process con-trol, ISA short course, Saint Louis http://www.modelingandcontrol.com/2010/12/exceptional_opportunities_in_p_18.html (Industrial application of PID) 13. McMillan G., (Dec. 9, 2010) Measurement and valve errors - Sources and impact, Emerson website entry, Austin http://www.modelingandcontrol.com/2010/12/measurement_and_valve_errors_-.html (Industrial application of PID) 14. McMillan G., (Dec. 16, 2010) Star performers in minimizing life cycle costs, Emerson website entry, Austin 27

http://www.modelingandcontrol.com/2010/12/star_performers_in_minimizing.html (Industrial application of PID) 15. McMillan, G. (2003) Advanced ph Measurement and Control, ISA, Re-search Triangle Park 16. McMillan G., (Aug. 2010) DeltaV v11 PID enhancements for wireless, Emerson white paper, Austin 17. Farhad Aslam, Mohd. Zeeshan Haider (2011) An implementation and Comparative Analysis of PID Controller and their Auto Tuning Method for Three Tank Liquid Level Control, International Journal of Computer Applications (0975-8887), Vol. 21 18. Rajkumar Bansal, A. Patra, Vijay Bhuria (2012), Design of PID Controller for Plant Control and Comparison with Z-N PID Controller, International Journal of Emerging Technology and Advanced Engineering, Vol. 2, Issue 4. 19. Mr. S. S. Gade, Mr. S. B. Shendageand Mr. M. D. Uplane, On Line Auto Tuning of PID Controller Using Successive Approximation Method, 2010 International Conference on Recent Trends in Information, Telecommunication and Computing, pp. 272-280 20. Gade S.S, Kanase A B, ShendageS. B. and Uplane M. D., Design and Development of Universal on Line Auto Tune PID controllers, in Proc. Of Int. Conf. on Control, Communication and Power Engineering 2010, pp. 291-295.. 21. Vinay Gupta, AshisPatra, Design of Self-Tune PID Controller for Governor Control to Improve Dynamic Characteristics International Conference (ICITM-2011) to be held on 3rdJuly2011 at Ranchi, India 7.0 APPENDICES 28

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