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United States Patent (19) Marchesani 54 CRACK ELIMINATION IN SOAP 75) Inventor: Cesare N, Marchesani, Maywood, N.J. 73) Assignee: Colgate-Palmolive Company, New York, N.Y. (21) Appl. No.: 488,509 (22 Filed: Apr. 25, 1983 Related U.S. Application Data 63 Continuation-in-part of Ser. No. 314,641, Oct. 26, 1981, abandoned. 51) Int. Cl.... B29C 17/14 52 U.S. Cl.... 264/145; 252/109; 252/134; 252/367; 264/75; 264/148; 264/320; 264/325; 425/308; 425/382 R 58) Field of Search...... 264/145, 148, 210.2, 264/75, 320, 325; 425/382 R, 464,308, 310-311, 296-297, 325, 327; 252/134, 367, 109, 90 56) References Cited U.S. PATENT DOCUMENTS 3,784,533 1/1974 Mach... 425/296 3,899,566 8/1975 Murray... 264/245 3,923,438 12/1975 Perla... 425/13.1 3,993,722 11/1976 Borcher et al... 264/75 4,036,775 7/1977 Trautvetter et al.... 264/75 4,067,946 1/1978 Rickert...... 264/150 4,090,829 5/1978 Fischer et al.... 425/73 11 Patent Number: 4,473,522 (45) Date of Patent: Sep. 25, 1984 4,096,221 6/1978 Fischer et al.... 264/75 4,147,053 4/1979 Marchesani... 73/104 4,162,288 7/1979 Hunt et al.... 264/325 4,201,743 5/1980 Perla et al.... 264/75 FOREIGN PATENT DOCUMENTS 2112602 10/1971 Fed. Rep. of Germany... 264/75 7106260 1 1/1972 Netherlands... 264/75 Primary Examiner-Jeffery Thurlow Attorney, Agent, or Firm-Herbert S. Sylvester; Murray M. Grill; John A. Stemwedel 57 ABSTRACT A process for the elimination of wet surface cracking in dual extruded soaps including the steps of extruding two streams of plodded soap from a single cone dual extrusion nozzle, cutting the two streams of plodded soap at right angles to the extrusion axis to form plodder soap blanks or billets of a predetermined size, rotating the plodder soap blanks or billets 90 on the extrusion axis, introducing the rotated plodder soap blanks or billets into a soap press having movable die elements so that the transverse faces of the plodder soap blanks or billets are in registry with the movable die elements, pressing the rotated plodder soap blanks or billets on their transverse faces to form pressed soap bars, and removing pressed soap bars. The process provides soap bars having an essentially laminar or parallel stress pat tern. 6 Claims, 14 Drawing Figures 36

U.S. Patent Sep. 25, 1984 Sheet 1 of 5 4473,522 PROR ART F G1

U.S. Patent Sep. 25, 1984 Sheet 2 of 5 4473,522

U.S. Patent Sep. 25, 1984 Sheet 3 of 5 4473,522

U.S. Patent Sep. 25, 1984 Sheet 4 of 5 4473,522 PRIOR ART 26 PRIOR ART C) \-v-/ Y -v / F G 4 F G5 PRIOR ART 26 \-v- / F G.6 PROR ART PRIOR ART 42 N2/ F G. 7 F G. 8

U.S. Patent Sep. 25, 1984 Sheet 5 of 5 4473,522 PRIOR ART PRIOT ART

1 CRACKELMINATION IN SOAP CROSS-REFERENCE TO RELATED APPLICATION This is a Continuation-in-Part application of Ser. No. 06/314,641, filed Oct. 26, 1981 and now abandoned. BACKGROUND OF THE INVENTION 1. Field of the Invention This invention relates to the art of soap making, and more particularly to a process for elimination of wet cracking and stress cracking in soap. 2. Description of the Prior Art New test methods for evaluating soap bar and cake wet cracking problems are disclosed in U.S. Pat. No. 4,147,053. Based on the application of these new tests and the observations of the results, it has been discov ered that toilet soap bars made by the single extrusion process showed a somewhat laminar or parallel crack pattern in the cross sectional test. These bars, in general, did not develop severe wet surface cracks when sub jected to the wash room usage test. Contrastingly, bars made by the dual extrusion process have a generally non-parallel crack pattern with radical spurs radiating always preferentially to one side and across the short axis of the bars. These bars, when field tested, would consistently develop severe wet surface cracks always significantly more on one side than the other. The prior art dual extrusion process leads to problems in the for mation of wet surface cracks during use of the bars since the stress pattern of the bars is such that upon use with water, the forces which tend to hold the lamina in the bar together are weakened, and, hence, there was a need to devise a means for imparting a laminar or paral lel crack pattern to finished soap bars made via the dual extrusion process. In the past, high moisture containing soap bars have been produced by plodding a soap mass and forcing it through a compression cone with a dual extrusion noz zle so that the two streams of plodded soap which may be divided into plodder soap blanks or billets which can be fed into a duplopress to provide increased line speed and efficiency. However, changes in the soap formula (i.e., lowering the moisture) and different selections of bar shapes generally result in finished soap bars with unusual and excessive surface cracking on the faces of the bars with one side having a more pronounced crack ing pattern than the other. This problem is directly related to the dual extrusion soap plodding process and the conventional method of pressing the plodder soap blanks or billets on their internal cut faces and external cut faces. SUMMARY OF THE INVENTION It is an object of the invention to overcome the diffi culties of the prior art. It is another object of the invention to produce fin ished soap bars which will not develop wet cracking during use. It is still another object of the invention to produce finished soap bars having parallel or laminar stress pat ters. These and other objects will be met as the description of the invention proceeds. The invention provides a process for the elimination of wet surface cracking in dual extruded soaps compris ing the steps of extruding two streams of plodded soap 4,473,522 10 15 20 25 30 35 40 45 50 55 60 65 2 from a single cone dual extrusion nozzle, cutting the two streams of plodded soap at right angles to the extru sion axis to form plodder soap blanks or billets of a predetermined size, rotating the plodder soap blanks or billets of a predetermined size, introducing the rotated plodder soap blanks or billets into a soap press having movable die elements so that the transverse faces of the plodder soap blanks or billets are in registry with the movable die elements, pressing the rotated plodder soap blanks or billets on their transverse faces to form pressed soap bars, and removing the pressed soap bars. BRIEF DESCRIPTION OF DRAWINGS Other advantages of the invention will hereinafter become more fully apparent from the detailed descrip tion of the preferred embodiments of the invention when considered in conjunction with the accompany ing drawings throughout which like reference charac ters indicate like parts and in which: FIG. 1 is a perspective view of the process of the prior art; FIG. 2 is a perspective view of the process of one embodiment of the invention; FIG. 3 is a perspective view of the process of a sec ond embodiment of the invention; FIG. 4 is a cross sectional view showing laminar stress present in prior art dual extruded soap billets; FIG. 5 is a cross sectional view showing laminar stress present in prior art dual extruded soap billets of another shape; FIG. 6 is a cross sectional view showing laminar stress present in prior art dual extruded soap billets of still another shape; FIG. 7 is a perspective view of a conventional banded soap bar; FIG. 8 is a cross sectional view of the bar of FIG. 7 taken on line 8-8. FIG. 9 is a perspective view of a conventional pillow or pin die shaped soap bar; FIG. 10 is a cross sectional view of the soap bar of FIG. 9 taken on line 10-10. FIG. 11 is a perspective view of a banded soap bar in accordance with the invention; FIG. 12 is a cross sectional view of the soap bar of FIG. 11 taken on line 12-12. FIG. 13 is a perspective view of a pillow or pin die shape soap bar in accordance with the invention; and FIG. 14 is a cross sectional view of the soap bar of FIG. 13 taken on line 14-14. DETAILED DESCRIPTION OF INVENTION To more fully understand present invention, it is necessary to specify the meaning of some terms. By "direction of extrusion' or "extrusion axis' or "ma chine direction', reference is made to the direction of the plodded material passing through the compression cone out of the extrusion orifice. This movement is usually in a horizontal plane. The "shearing' or "cut ting plane' is that plane between the two streams of the dually extruded material that is parallel to or defines the "medial' or "internal cut face'. Normally, the shearing plane is vertical to provide side-by-side streams, rather than horizontal which would yield top and bottom streams. This plane is parallel to the "lateral' or exter nal cut face. The transverse plane defines the trans verse faces' of the plodded extruded material. This

3 plane is perpendicular to the shearing plane which it meets at the extrusion axis. By "soap' or "soapbar' the composition of the mate rial includes soaps, detergents, or other washing agents and mixtures of such materials, FIG. 1 shows a dual extrusion plodder of the type known in the prior art which has a compression cone 20 which compacts the plodded soap material as it ap proaches nozzle plate 22, which has a predetermined cross sectional area. The extruded soap mass 24 being advanced in the machine direction is divided into two streams, having their cross sections determined by the geometry of noz zle plate 22. As seen at 26, the cross sections show asym metric stress patterns which are mirrored across the shearing plane. The separate streams 24 are cut into plodder soap blanks or billets 30 by conventional means (not here illustrated) at right angles to the machine direction. The plodder soap blanks or billets 30 are then pressed at 36 in a soap press (not shown) on their cut edges and other edges in the direction of the arrows as shown in the figure. Typical dual extruded plodder soap blanks or billets have cross sections and stress patterns of the type as shown in FIGS. 4, 5 and 6. When pressed into bars 40 or 50, the finished soaps have asymmetric stress patterns 42 or 52 which will lead to surface stress cracking or wet cracking when the bars are subjected to SC In accordance with the process of the invention, a conventional plodder 20 with an extrusion nozzle 22 with a cross section that is predetermined in view of the desired end shape and processing parameters is used to extrude soap mass 24 having stress pattern 26. The plod ded soap mass 24 is cut into plodder soap blanks or billets 30. The plodder soap blanks or billets are rotated 90 about the extrusion axis as shown by the curved arrows 31 to align the plodder soap blanks or billets as shown at 32 so that the stress patterns of these plodder soap blanks or billets will be positioned as shown at 34. The rotated plodder soap blanks or billets are then pressed on their transverse faces in the direction shown by the arrows at 36 in FIGS. 2 and 3. The resulting soap bars are resistant to wet surface cracking. FIGS. 11 through 14 illustrate the finished soap bars of the invention. FIG. 12 shows banded soap bar 60 which is preferably made by the process illustrated in FIG. 2 wherein the plodder soap blank or billet is a generally rectangular prism which is pressed so that the stress pattern of the bar has a folded in or compressed U-shaped pattern 62 as is shown in FIG. 12, rather than the open out stress pattern of the prior art which is shown in FIG. 8. To make banded soap bars using a conventional die box press, it is preferred that the major dimension of the rectangular prism be coincident with the axis of extru sion and the minor dimension be the distance between the transverse faces so that the inside cut face and the outside face of the plodder soap blank or billet are against the sides of the die box and the movable dies act against the transverse faces. By the same token, the pin die or pillow shaped soap 70 of FIG. 13, which is preferably made by the process of FIG. 3 wherein the plodder soap blanks or billets have almost equal transverse dimensions and lateral and medial dimensions, sometimes referred to as "semi square' (because the transverse faces have arcuate sur faces) and are pressed in a capacity die on their trans verse sides giving the stress pattern 72 which is also of 4,473,522 10 5 20 25 30 35 40 45 50 55 60 65 4. a folded in or compressed U-shape as illustrated in FIG. 14 rather than the open pattern of the prior art as shown in FIG, 10. Thus the invention allows for the formation by dual extrusion of pairs of soap plodder blanks or billets for virtually all soap formulas while forming a laminar or parallel stress pattern in the finished soap bars which are essentially free from stress surface cracks and objection able wet cracking. Use of the invention permits dual extrusion to be utilized in all soap production thereby increasing production rates while reducing cost and delivering a better product. The production of striped, striated, marbleized or multicolored soaps can be facili tated with the process of the invention. The unexpected improvement in the stress pattern of the finished soap bars due to the 90 rotation of the soap plodder blanks or billets and subsequent pressing on the transverse faces to impart a parallel or laminar stress pattern and thus eliminate stress surface cracks and wet Surface cracking is the result of the invention. This process is especially suitable for use with soap presses having multiple cavities so that more than one finished bar can be made per pressing cycle. While the basic principle of the method of this inven tion has been illustrated and described herein, it will be appreciated by those skilled in the art that variations in the disclosed arrangement, both as to its details and as to the organization of such details, may be made without departing from the spirit and scope thereof. Accord ingly, it is intended that the foregoing disclosure and drawings will be considered only illustrative of the principles of the invention and not construed in a limit ing sense. I claim: 1. A process for the elimination of wet surface crack ing in dual extruded soaps comprising the steps of: extruding two streams of plodded soap from a single cone dual extrusion nozzle, such streams of plod ded soap having asymmetric stress patterns mir rored across the shearing plane of the single cone dual extrusion nozzle and transverse faces perpen dicular to the shearing plane, cutting the two streams of plodded soap at right an gles to the extrusion axis to form plodder soap blanks or billets of a predetermined size, rotating the plodder soap blanks or billets 90 to the shearing plane on an axis parallel to the extrusion axis, introducing the rotated plodder soap blanks or billets into a soap press having movable die elements so that the transverse faces of the plodder soap blanks or billets are in registry with the movable die ele ments, pressing the rotated plodder soap blanks or billets on their transverse faces to fold the asymmetric stress pattern upon itself to form crack-resistant pressed Soap bars, and removing pressed soap bars from the soap press. 2. The process of claim 1 wherein the soap press is provided with multiple cavities to simultaneously form more than one finished soap bar per pressing cycle. 3. The process of claim 1 wherein the plodder soap blanks or billets are rectangular prisms whose major dimension is in the machine direction and whose mini mum dimension is the distance between the transverse faces.

4,473,522 5 6 4. The process of claim3 wherein the plodder soap whose transverse dimension and medial or lateral di blanks or billets are pressed in a die box to form banded mension are about equal. soap bars. 5. The process of claim 1 wherein the plodder soap 6. The process of claim 5 wherein the plodder soap blanks or billets are solids with arcuate transverse faces 5 blanks or billets are pressed on a pin die press. whose major dimension is in the machine direction and 3k k k sk xk 10 15 20 25 30 35 40 45 50 55 60 65