Grinding polycrystalline diamond using a diamond grinding wheel

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University of Wollongong Research Online University of Wollongong Thesis Collection 1954-2016 University of Wollongong Thesis Collections 2006 Grinding polycrystalline diamond using a diamond grinding wheel Maryam Agahi University of Wollongong Recommended Citation Agahi, Maryam, Grinding polycrystalline diamond using a diamond grinding wheel, MEng, School of Mechanical, Materials and Mechatronic Engineering, University of Wollongong, 2006. http://ro.uow.edu.au/theses/41 Research Online is the open access institutional repository for the University of Wollongong. For further information contact the UOW Library: research-pubs@uow.edu.au

NOTE This online version of the thesis may have different page formatting and pagination from the paper copy held in the University of Wollongong Library. UNIVERSITY OF WOLLONGONG COPYRIGHT WARNING You may print or download ONE copy of this document for the purpose of your own research or study. The University does not authorise you to copy, communicate or otherwise make available electronically to any other person any copyright material contained on this site. You are reminded of the following: Copyright owners are entitled to take legal action against persons who infringe their copyright. A reproduction of material that is protected by copyright may be a copyright infringement. A court may impose penalties and award damages in relation to offences and infringements relating to copyright material. Higher penalties may apply, and higher damages may be awarded, for offences and infringements involving the conversion of material into digital or electronic form.

GRINDING POLYCRYSTALLINE DIAMOND USING A DIAMOND GRINDING WHEEL A thesis submitted in partial fulfilment of the requirements for the award of the degree Master of Engineering Research from University of Wollongong by Maryam Agahi, B. Sc. School of Mechanical, Materials and Mechatronic Engineering 2006

CERTIFICATION I, Maryam Agahi, declare that this thesis, submitted in partial fulfilment of the requirements for the award of Master of Engineering Research, in the Faculty of Engineering, University of Wollongong, is wholly my own work unless otherwise referenced or acknowledged. The document has not been submitted for qualifications at any other academic institution. Maryam Agahi July 13, 2006 ii

TABLE OF CONTENTS CERTIFICATION...II TABLE OF CONTENTS... III LIST OF TABLES...V LIST OF FIGURES... VI GLOSSARY...X ABSTRACT...XII ACKNOWLEDGMENTS... XIII CHAPTER 1 INTRODUCTION AND LITERATURE REVIEW...1 1.1. BACKGROUND...1 1.2. POLYCRYSTALLINE DIAMOND...4 1.2.1. Properties of PCD...5 1.3. GRINDING PROCESS AND WEAR MECHANISMS...8 1.3.1. Material Removal Mechanisms...12 1.3.2. Grinding Wheels...17 1.4. TRUING AND DRESSING...19 1.4.1. Unconventional Truing and Dressing Methods...22 1.5. OTHER METHODS OF MACHINING PCD BLANKS...23 1.6. AVAILABLE MACHINES...25 1.7. WHEEL LIFE...25 1.8. EDGE QUALITY...26 1.9. THESIS OBJECTIVES...27 1.10. THESIS OUTLINE...30 CHAPTER 2 EXPERIMENTAL SETUP...32 2.1. INTRODUCTION...32 2.2. GRINDING MACHINE...32 2.2.1. PCD Samples and Grinding Wheels...38 2.2.2. Truing...39 2.2.3. Dressing...41 2.2.4. Micrometer...42 2.3. DATA COLLECTION AND CONTROL PROCEDURE...44 2.4. MATHEMATICAL DESCRIPTION OF THE GRINDING FORCES...46 2.5. CONCLUSIONS...47 CHAPTER 3 GRINDING AND FORCE ANALYSIS...49 3.1. INTRODUCTION...49 3.2. DESCRIPTION OF EXPERIMENTS...49 3.3. GRINDING FORCES AND IN-FEED...52 3.4. GRINDING FORCES AND THE WORK PIECE POSITION...59 3.5. MATERIAL REMOVAL RATE...64 3.6. GRINDING FORCES AND THE OSCILLATION RATE...67 3.7. CONCLUSIONS...68 CHAPTER 4 TRUING, DRESSING AND GRINDING...71 4.1. INTRODUCTION...71 4.2. DESCRIPTION OF EXPERIMENTS...71 4.3. TRUING, DRESSING AND THE GRINDING FORCES...74 4.4. DRESSING TIME AND SHARPNESS OF THE WHEEL...78 iii

4.5. CONCLUSIONS...84 CHAPTER 5 GRINDING WHEEL WEAR...86 5.1. INTRODUCTION...86 5.2. DESCRIPTION OF EXPERIMENTS...87 5.3. MATERIAL REMOVAL RATE (MRR) AND VOLUMETRIC WHEEL WEAR RATE (VWWR)...87 5.3.1. In-feed in Steps...91 5.4. DRESSING EFFECT ON THE WHEEL WEAR...92 5.5. WORK PIECE HARDNESS AND THE WHEEL WEAR...97 5.6. CONCLUSIONS...99 CHAPTER 6 GRINDING AND EDGE QUALITY...102 6.1. INTRODUCTION...102 6.2. DESCRIPTION OF EXPERIMENTS...103 6.3. IN-FEED, MRR AND EDGE QUALITY...107 6.4. GRINDING WHEEL TYPE AND QUALITY...115 6.5. GRINDING USING MACHINE 1 AND MACHINE 2...121 6.6. CONCLUSIONS...123 CHAPTER 7 CONCLUSIONS AND RECOMMENDATIONS FOR FUTURE RESEARCH...125 7.1. CONCLUSIONS...125 7.2. FUTURE WORK...128 BIBLIOGRAPHY...131 iv

LIST OF TABLES Table 2.1 Measurement error using the micrometre... 44 Table 3.1 Experimental settings... 50 Table 6.1 Range of spindle speed used in quality experiments...106 v

LIST OF FIGURES Figure 1.2.1 PCD work piece... 5 Figure 1.2.2 Properties of cutting tool materials [36]... 6 Figure 1.2.3 Thermal conductivity of cutting tool materials [36]... 7 Figure 1.2.4 Tool fabrication and performance properties [36]... 8 Figure 1.3.1 Structural relationship between input and output values in PCD grinding [8, 15, 16]... 9 Figure 1.3.2 Kinematics and forces in grinding PCD [4-6]... 10 Figure 1.3.3 Schematic representation of selected types of wear [8]... 13 Figure 1.3.4 Wear modes in PCD grinding, adapted from [4]... 14 Figure 1.3.5 Relationship between material removal rate and normal force in PCD grinding using constant contact force, adapted from [4]... 15 Figure 1.3.6 Relationship between G-ratio and normal force in PCD grinding using constant contact force, adapted from [4]... 15 Figure 1.3.7 Qualitative relationships between grinding parameters [8]... 16 Figure 1.4.1 Conventional truing and dressing process [53]... 21 Figure 2.2.1 Grinding machine setup... 33 Figure 2.2.2 Axes orientation of the grinding machine... 34 Figure 2.2.3 Giving in-feed in Y-direction using a dial indicator... 35 Figure 2.2.4 Top view of the grinding system... 36 Figure 2.2.5 The second grinding machine used to grind PCD... 37 Figure 2.2.6 Top view of the second grinding machine setup... 38 Figure 2.2.7 PCD samples... 39 Figure 2.2.8 Grinding wheels (1) Metal bond (2) Vitrified bond... 39 Figure 2.2.9 Truing device... 40 Figure 2.2.10 Truing configuration... 41 Figure 2.2.11 Aluminium oxide dressing stick... 42 Figure 2.2.12 Dressing configuration... 42 Figure 2.2.13 Manual micrometres...43 Figure 2.2.14 Optical microscope and the electronic micrometre... 43 Figure 2.2.15 Material removal measurements... 44 vi

Figure 2.3.1 DSP soft ware flow chart [35]... 45 Figure 2.4.1 Kinematics and forces in grinding of Polycrystalline Diamond... 47 Figure 3.3.1 Normal force vs. time for different in-feeds... 53 Figure 3.3.2 Magnified normal force vs. time with respect to the contact position... 54 Figure 3.3.3 Maximum tangential force and the corresponding normal force against in-feed... 55 Figure 3.3.4 Maximum tangential force against maximum normal force... 56 Figure 3.3.5 Ratio of the maximum tangential to the corresponding normal force against in-feed... 57 Figure 3.3.6 Normal force vs. time for number of in-feeds given in each experiment... 58 Figure 3.3.7 Peaks of normal force vs. in-feed selected from Figure 3.3.6... 59 Figure 3.4.1 Normal force vs. time, without moving the work piece, for different contact positions and 15 µ m in-feed... 60 Figure 3.4.2 Normal force vs. time for different in-feeds in grinding cemented carbide... 61 Figure 3.4.3 Maximum grinding forces against in-feed in grinding cemented carbide... 62 Figure 3.4.4 Maximum tangential force against the maximum normal force for different contact zones... 63 Figure 3.4.5 Maximum normal force against in-feed for different contact zones... 63 Figure 3.4.6 Ratio of the maximum tangential force to the maximum normal force against in-feed for different contact zones... 64 Figure 3.5.1 Relationship between material removal rate and in-feed for different contact zones... 65 Figure 3.5.2 Relationship between material removal rate and normal force for different contact zones... 67 Figure 3.6.1 Relationship between the normal force and oscillation rate for 2 different in-feeds... 68 Figure 4.3.1 Normal force vs. time, using a blunt wheel, without moving the work piece, for different contact positions and 15 µ m in-feed... 74 Figure 4.3.2 Maximum normal force against in-feed, for different grinding wheel conditions... 75 vii

Figure 4.3.3 Ratio of the maximum tangential force to the maximum normal against in-feed, for different grinding wheel conditions... 76 Figure 4.3.4 Maximum tangential against maximum normal force, for different grinding wheel conditions... 77 Figure 4.4.1 Normal force vs. time, commencing with a dressed wheel with 20 µ m in-feed per section... 78 Figure 4.4.2 Material removal rate against normal force, commencing with a dressed wheel with 20 µ m in-feed... 79 Figure 4.4.3 Normal force vs. time, using a wheel dressed for different dressing times, 10 µm in-feed per section... 80 Figure 4.4.4 Normal force vs. time, using a wheel dressed for different dressing times, 20 µm in-feed per section... 81 Figure 4.4.5 Maximum normal force against dressing time, for 10 and 20 µm in-feed... 82 Figure 4.4.6 Material removal rate against dressing time, for 10 and 20 µm in-feed... 83 Figure 5.3.1 G-ratio and MRR against normal force, commencing with a dressed wheel with 20 µ m in-feed per experiment... 87 Figure 5.3.2 MRR and VWWR against normal force, commencing with a dressed wheel with 20 µ m in-feed per experiment... 88 Figure 5.3.3 G-ratio and MRR against in-feed... 90 Figure 5.3.4 MRR and volumetric wheel wear rate against in-feed... 91 Figure 5.3.5 Volumetric wheel wear rate against in-feed for different in-feed steps... 92 Figure 5.4.1 MRR and volumetric wheel wear rate against dressing time, for 10 µ m in-feed... 93 Figure 5.4.2 MRR and volumetric wheel wear after dressing against dressing time, for 10 µ m in-feed... 94 Figure 5.4.3 MRR and volumetric wheel wear rate against dressing time, for 20 µ m in-feed... 94 Figure 5.4.4 MRR and volumetric wheel wear after dressing against dressing time, for 20 µ m in-feed... 95 Figure 5.4.5 G-ratio against dressing time, for 10 and 20 µ m in-feed... 96 Figure 5.4.6 Volumetric wheel wear rate against dressing time, for 10 and 20 µm infeed... 97 viii

Figure 5.5.1 MRR and volumetric wheel wear rate against in-feed, in grinding cemented carbide... 98 Figure 5.5.2 Comparison of volumetric wheel wear rate against in-feed, for grinding of PCD and cemented carbide... 98 Figure 6.2.1 Upper and lower surfaces of the PCD work piece...103 Figure 6.2.2 Two different ways of positioning the work piece (a) Area A upward (b) Area B upward (refer to Figure 6.2.1)...104 Figure 6.3.1 Typical representation of where the following photos refer to...107 Figure 6.3.2 10 µ m in-feed, scale 380 µ m...109 Figure 6.3.3 20 µ m in-feed, scale 380 µ m...111 Figure 6.3.4 30 µ m in-feed, scale 380 µ m...112 Figure 6.3.5 40 µ m in-feed, scale 380 µ m...113 Figure 6.3.6 50 µ m in-feed, scale 380 µ m...114 Figure 6.4.1 10 µ m in-feed, scale 380 µ m...116 Figure 6.4.2 20 µ m in-feed, scale 380 µ m...117 Figure 6.4.3 30 µ m in-feed, scale 380 µ m...118 Figure 6.4.4 40 µ m in-feed, scale 380 µ m...119 Figure 6.4.5 50 µ m in-feed, scale 380 µ m...120 Figure 6.5.1 Photo of edge quality using Machine 2, scale 380 µ m...123 ix

GLOSSARY C Conc. CVD/PCVD Diamond d K d S DOS DSP ECD Concentration Coolant concentration Chemical vapour deposited polycrystalline diamond Grit diameter Cup wheel diameter Disc operating system Digital signal processor Electrochemical in-process controlled dressing ECDM/ECAM/EEDM Electro chemical discharge machining EDG EDM ELID F A F d FFG F N /Fn F R F T /Ft G-ratio/G HPAWJ HSS Electrical discharge grinding Electro discharge machining Electrolytic in-process dressing Contact force Force in X direction Form and finish grinding Normal cutting force Radial force Tangential force Grinding ratio High pressure abrasive water jet High-speed steel x

I/O Matlab MMC MRR/Q W PcBN/PCBN PCD RAM R P SEM SRG t d TI V C /V S v d /V W VWW VWWR WC WEDM δ α Input/output Matrix laboratory Metal matrix composite Material removal rate Polycrystalline cubic boron nitride Polycrystalline diamond Random access memory Peak to mean line height Scanning electron microscope/microscopy Stock removal grinding Sharpening cycle Texas Instrument Peripheral speed X-axis velocity/oscillation rate Volumetric wheel wear during dressing Volumetric wheel wear rate during grinding Cemented tungsten carbide Wire electrical discharge machining Truing feed Vertical angle between the work piece and the grinding wheel centre µ m Micron µ Grinding coefficient xi

ABSTRACT Application of ultrahard cutting tool materials is continuously expanding. One example of an ultrahard cutting tool material is polycrystalline diamond (PCD), which is widely used in tool making and machining. However, because of the high wear resistance of PCD it is characterised by low grindability and machinability. So, any mechanism used to machine PCD has to meet specific requirements. Grinding with a diamond grinding wheel is one of the economic ways to machine PCD compacts. This thesis considers the grinding of polycrystalline diamond using a conventional grinding machine and makes machining parameter recommendations to support the optimisation of PCD grinding. The PCD grinding forces are mathematically analysed. These grinding forces are measured using a force sensor installed on a conventional grinding machine. The forces produced during grinding are investigated as a function of in-feed, contact zone, material removal rate (MRR) and oscillation rate. Wheel conditioning, another major aspect of PCD grinding, is studied and optimised in order to reduce the grinding forces, increase the cutting efficiency and achieve maximum removal rates and minimum wear ratios. Grinding wheel wear is investigated as a recognized problem in PCD grinding. A series of experiments are conducted in which the material removal rate, the rate of wheel wear and the grinding forces are measured. The effects of in-feed, sharpening process and work piece hardness on the wheel wear are studied. The edge quality of the PCD compacts is investigated as an important issue in tool making. Factors affecting PCD grinding quality include the in-feed, material removal rate, the condition of the diamond grinding wheel and the rigidity of the grinding machine. These are all studied to find their effect on edge quality. The work presented in this thesis also shows that the capability of a conventional grinding machine designed for non-pcd is sufficient to grind PCD with acceptable quality. xii

ACKNOWLEDGMENTS Most of all, I would like to thank my supervisor Professor Chris Cook for his kind support and priceless guidance throughout my research. The opportunity he gave me not only increased my knowledge but also allowed me to meet such wonderful and unique people at the university. His perpetual encouragement and invaluable advice are greatly appreciated. I would like to give special thanks to Dr. Marta Fernandes, my on-site supervisor. Her endless ideas opened the closed doors and enlightened me about the problems I faced. Whenever I needed help she gave me the energy and motivation to finish what I had started. I would like to thank her for being such a wonderful friend even in her absence. I would like to thank Mr. Jeff Moscrop, my co-supervisor for his priceless help. Jeff s friendly availability for the successful completion of this thesis is deeply acknowledged. Many thanks to all general staff who helped me complete my research. Special thanks to Mr. Brian Webb for preparing my experimental setup and to Mr. Greg Tillman and Mr. Stuart Rodd who helped me use the various equipments. I would like to give special thanks to Dr. John Simpson for his valuable and helpful comments in solving problems with the grinding machine and also to Ms. Neda Zamani for helping me learn C programming. Thanks also to Ms. Catherine Todd for her comments in writing up my thesis and to Ms. Lorelle Pollard for her kindness and inspirational smile. To my dear parents who always gave me the confidence and strength to work on my thesis. Their warm voices always gave me fresh energy and inspiration. It is due to their unconditional support that I have been able to reach my goal. Last but not least, I would like to thank Mehrdad, my dear husband, for his love and never-ending support, for always being with me whenever I needed him and for having faith in me. I want to thank him for his encouragement when I was desperate or not focused. Without his patience I would not be able to finish this thesis. xiii