Unique Scattering Measurements Using the Agilent Universal Measurement Accessory (UMA)

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Click to edit Master title style Unique Scattering Measurements Using the Agilent Universal Measurement Accessory (UMA) mark.fisher@agilent.com

Click to edit Master title style Rapid, Automated, Quality Control of Diffraction Grating Efficiency

Agenda The Problem : How can we can we determine Grating Efficiency faster and with greater control? Solution : Cary 7000 UMS(Universal Measurement System) or Cary 5000 with UMA(Universal Measurement Accessary) Results : 300, 1200, 1800, 3600 lines per mm Gratings Conclusions 3

Cost Control, Quality Control The goal to produce high quality diffraction gratings, can rapidly, and cost effectively, be assisted by timely and specific feedback throughout the production process. High quality automated spectrophotometric characterization tools can be used to help; o test the optic against it s design intent throughout coating stages o steer end product batches toward consistent quality o monitor and control the production process Multi-angle spectrophotometric measurements can ensure Diffraction Gratings o yields are maximize o waste is reduced o product quality is better controlled o time is saved down time reduced 4

Orientation of Sample

Cary UMS Measurement Modes 6 Modes 1 System Perform all these measurements on the Cary 7000 UMS

Technical Aspects of UMA Automated Wired grid polarizer Silicon/InGaAs Sandwich Detector Horizontal/vertical apertures Optical Encoder

UMS Measurement Modes Automated Control of sample angle, detector position and polarization Sample sits at center of rotatable stage (360 rotation) Detector can move in arc around sample

UMS Measurement Modes Baseline One baseline is needed for all %R and %T measurements, at all angles for a given polarization Absolute Reflection & Transmission Only difference between baseline and measurement is the sample itself.

UMS Measurement Modes Absolute Reflection and Transmission Without moving the sample the detector can be rotated to collect %R and %T Consistency & accuracy because incident light position, angle and shape is fixed for both %R and %T

Grating Efficiency Measurement Mounting of Sample Right : 300 lines per mm grating mounted on Cube Beam Splitter Sample Holder. Below : Sample Holder placed onto the sample stage in the UMA. Detector held at 10. Grating mounted in Edward Mount Grating mounted inside the Cary 7000 Universal Measurement Spectrophotometer 11

Grating Efficiency Measurement Basic Instrument Paraments used to Collect the Data for the Diffraction Gratings Parameter Value Angle of incidence Wavelength-dependent Detector angle 10 Wavelength and Angle of Incidence were Read from a Text File (number of data points was determined by the grating measured) Wavelength range Data interval Spectral bandwidth* Signal averaging time 250 2500 nm 10 and 1 nm, respectively 2 nm 0.5 sec Two Different Data Intervals were used to Demonstrate how to Improve Data Collection Time Polarization s-and p-polarization Incident beam aperture 3 x1 (vertical x horizontal) Baseline correction On 12

Initial Screen with Options

After Instrument SetUp Button Pressed

After D Collect SetUp Button Pressed

Spectral Results for 300 Lines per mm Gratings

Spectral Results for 1200 Lines per mm Gratings

Spectral Results for 1800 Lines per mm Gratings

Spectral Results for 3600 Lines per mm Gratings

Overlay of Spectral Results for 1200 lines per mm Grating Data Interval of 1 nm and 10 nm Overlay of P-Polarization Data Interval of 1 nm and 10 nm Red data interval = 1 nm Black data interval = 10 nm

Overlay of Spectral Results for 1200 lines per mm Grating Data Interval of 1 nm and 10 nm Overlay of S-Polarization Data Interval of 1 nm and 10 nm Red data interval = 1 nm Black data interval = 10 nm

Comparison of SBW of 2 nm and 5 nm Sample 300 lines per mm

300 lines per mm Grating Overlay of P-Polarization of SBW 2 nm and SBW 5 nm Green SBW= 2 nm Red SBW= 5 nm

300 lines per mm Grating Overlay of S-Polarization of SBW 2 nm and SBW 5 nm Red SBW= 2 nm Blue SBW= 5 nm

Grating Lines per mm Data interval = 1 nm Summary and Conclusions Data interval = 10 nm Total Elapsed Time Number of Data Total Elapsed Time Points 300 5 hrs 29 min 15 sec 1601 34 min 38 sec 161 Number of Data Points 1200 4 hrs 21 min 30 sec 1251 28 min 57 sec 126 1800 2 hrs 52 min 50 sec 826 18 min 34 sec 83 3600 1 hr 41 sec 290 7 min 57 sec 29 The Cary 7000 UMS was demonstrated as a fast and accurate analytic tool for the characterization of diffraction gratings. The UMA gives the user the flexibility to characterize gratings either at a given angle of incidence (the sample stage rotates), as shown here, or at a given reflection/transmission angle (the detector moves) depending on the supposed application. The complete collect is fully automatic with minimal user interaction and the use of an ADL code increases the measure capabilities of the Cary 7000 UMS. 9

Click to edit Master title style Thank You Questions? mark.fisher@agilent.com