INVESTIGATION OF IMPACT DAMAGE OF CARBON FIBER- RAINFORCED PLASTIC (CFRP) BY EDDY CURRENT NON- DESTRUCTIVE TESTING

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International Workshop SMART MATERIALS, STRUCTURES & NDT in AEROSPACE Conference NDT in Canada 2011 2-4 November 2011, Montreal, Quebec, Canada INVESTIGATION OF IMPACT DAMAGE OF CARBON FIBER- RAINFORCED PLASTIC (CFRP) BY EDDY CURRENT NON- DESTRUCTIVE TESTING K.Koyama 1, H.Hoshikawa 1 and T.Hirano 2 1 College of Industrial Technology, Nihon University, Japan kiyoshi.koyama@nihon-u.ac.jp 2 Graduates School of Nihon University, Japan ABSTRACT Presentation paper describes the use of eddy current testing (ECT) method for the inspection and detection of impact damage in carbon fiber-reinforced plastics (CFRP). Inspection of impact damage in CFRP by ECT method was investigated. Scanning experiments were carried out using eddy current theta probe, which is developed by the authors, at test frequency of 1MHz. CFRP samples of 3.0mm in thickness with artificial impact damage were used. As a result, it has been confirmed that eddy current theta probe can be detected the impact damage, that produced the energy of 0.25J, with high signal-to-noise ratio rather than conventional eddy current probe. Keywords: Eddy current testing, Carbon fiber-reinforced plastic (CFRP), Eddy current theta probe, Impact damage

INTRODUCTION This paper reports the results of the detection of defects in CFRP by ECT, a non-destructive testing method using electromagnetic induction. Composite materials present the combined advantage of high strength, high fatigue resistance and very low weight. They are used to a great extent in the aerospace industry. However, fiberreinforced composite materials can show poor resistance to impact. In order to maintain the high level of quality and safety required by the aerospace industry, the use of Non-destructive Evaluation (NDE) techniques is a major factor in the quality assessment for these new materials. An external impact causes delamination of CFRP, resulting in reduced mechanical properties. Non-destructive testing is performed to detect defects. Ultrasonic testing, which requires a contact medium, is used as a non-destructive testing method for CFRP. ECT method is a nondestructive testing method where electric induction is used, and has advantages in the inspection of CFRP that are not available with other testing methods[1]-[6]. In this method, change of electric current in a test material by a test coil, where an alternating current is applied, are monitored as change of impedance of the test coil or another detecting coil. Distinctive feature of this method is an ability of fast and contact-free inspection of defects that affect local electric conductivity of the sample. This method is widely used for detecting cracks and corrosion in metals, or checking their electric conductivity. Because carbon fiber in CFRP has electric conductivity, ECT method has a potential to inspect the defects. However, electric conductivity of CFRP is much smaller than that of metals. Moreover, from the view of the eddy current probe, CFRP to be checked looks as a inhomogeneous conductive materials where conductive fibers are bundled and laid up, and this is completely different situation comparing with metal samples that are homogeneous. Therefore there are several problems to be solved for applying ECT method to CFRP such as proper selection of test frequency, shape of probe, or signal processing. The authors developed an ECT probe that takes into account the anisotropic conductivity of CFRP, and reported that the probe can detect artificial defects with a high signal-to-noise ratio[7]. In this study, we artificially introduced simulated defects into the specimens by applying an impact, performed defect detection, and examined the correlation between the impact force and the detection signal. We also examined correlations with the results of ultrasonic testing and observation of the cloth section of the damage zone by radiography testing. APPLICATION OF THE ELECTROMAGNETIC INDUCTION NON-DESTRUCTIVE METHOD TO CFRP

CFRP contains carbon and is electrically conductive. Its conductivity is 10 4 to 10 6 less than that of metals. This conductivity value is measurements by the material manufacturer. ECT can be applied to CFRP because of its conductivity. Fig.1 shows the probe[8][9] (called a theta probe) used in ECT of CFRP. The theta probe consists of a circular exciting coil and a rectangular vertical detecting coil. The exciting coil generates an eddy current in the specimen by electromagnetic induction. The detecting coil detects the magnetic flux produced by the eddy current induced by a defect, and generates a signal. Detecting coil Test material Exciting coil Fig.1: Structure of eddy current theta probe. The principle of the detection of defects in cloth CFRP is described below. CFRP is conductive in the xy-direction in the plane of the CF sheet. If there is no defect in the specimen, the eddy current flows through the winding of the exciting coil. The sum of the magnetic flux crossing the detecting coil is zero, and no voltage is induced in the detecting coil; that is, no signal is generated without a defect. If there is an interlaminar defect, as shown in Fig.2, the eddy current is prevented by the defect from flowing, and the flow of the eddy current around the defect changes, generating a signal in the detecting coil. As shown in Fig.2, the current flows in the detecting coil in one direction when the detecting coil is placed above the defect, and in the opposite direction when it is placed below the defect. The polarity of the signal detected changes accordingly. Detecting coil Defect Eddy current Fig.2: Eddy current flow with defect in CFRP.

EXPERIMENTAL METHOD The specimens used were a 3 mm thick, cloth CFRP plate laminated with layers of 0.2 mm thick, woven CF sheets; and a 3 mm thick, quasi-isotropic CFRP plate [45/0/-45/90]2s laminated with 0.2 mm thick, unidirectional fiber CF sheets. Artificial impact defects were introduced by dropping a 1 kg steel ball, from different heights, onto a 3 mm drill bit placed on the CFRP specimen. The drop heights used were 0.25, 0.5, 0.75, 1.0, 1.5, and 2.0 m, which correspond to impact energy of 0.25, 0.5, 0.75, 1.0, 1.5, 2.0 J. The exciting coil of the theta probe used was 9 mm in outer diameter, with a winding crosssection of 1 mm 2. The detecting coil was 7 mm wide and 7 mm high, with a winding crosssection of 1 mm 2. The theta probe was two-dimensionally scanned without contact at a constant distance (0.5 mm) from the CFRP specimen. The scan range was ±25 mm in the x- and y- directions, and the scan interval was 0.5 mm. The intensity of the eddy current induced in the specimen is determined by the product of the test frequency and the electromagnetic characteristic of the specimen. The test frequency was set to 1 MHz, taking into account the conductivity of the CFRP. Ultrasonic testing and Radiography testing observation of the cross-section of the damage zone were performed to evaluate the detection signal in ECT in detail. In ultrasonic testing, the immersion/reflection technique was employed, using a 5 MHz probe. The probe was twodimensionally scanned at 0.1 mm intervals. EXPERIMENTAL RESULT Results of the detection of defects in the cloth CFRP Fig.3 shows images of the detection signal of each impact defect in the cloth CFRP specimen. In ECT, a sine wave alternating current is applied, and thereby, the complex voltage of the inphase component having the same phase as the exciting current and the 90-degree phaseadvanced quadrature components is obtained. The amplitude of the detection signal is shown in the figure. The probe has been shown to have the capability to detect impact damage corresponding to an impact energy of up to 0.25 J with a high signal-to-noise ratio. The signal in the y-direction (shown by the arrow in Fig.3) passing through the maximum point of the signal amplitude is shown in Fig. 4 of the complex voltage plane. The signal amplitude and the signal phase were obtained from the figure. Fig. 5 shows the change in the signal amplitude and the signal phase with impact energy changes. Though the signal amplitude is nearly the same for 0.5 and 0.75 J, the display area of the signal is larger for 0.75 J than for 0.5, as shown in Fig. 3. The signal phase varies with impact energy.

0.75 1.95 - - - (a) energy 0.5J (b) energy 0.75J (c) energy 1.0J Fig.3: Image display of ECT flaw signal amplitude for cloth CFRP. Quadrature component, V 1 0-1 Impact energy 1.0J 0.75J 0.5J 0.25J -1 0 1 In-phase component, V Fig.4: ECT flaw signal patterns when different impact damage. Defect signal amplitude, V 2 1 0 0 0.2 0.4 0.6 0.8 1 Impact Energy, J Defect signal phase, deg 140 120 100 80 60 0 0.2 0.4 0.6 0.8 1 Impact Energy, J (a) impact damage signal amplitude (b) impact damage signal phase Fig.5 : Detection signal amplitude and phase vs. impact energy.

Ultrasonic testing and Radiography testing observation of the cross-section of the damage zone were performed to evaluate the detection signal in ECT in detail. Fig6 shows display images of the detection signal in ultrasonic testing (UT). The display area of the signal increases with increasing impact energy, and shows a good agreement between ECT and UT. Signals were observed near the surface for 0.25 and 0.5 J, and across the thickness of the specimen for 0.75 and 1.0 J. 0mm 11.7mm 0mm 22.5mm 0mm 29.2 9.2mm 11.7mm 22.5mm 22.9mm (a) energy 0.5J (b) energy 0.75J (c) energy 1.0J Fig.6: Image display of UT signal with different impact energy. Fig.7 shows Radiography testing images of the cross-section of the damage zone. The damage becomes larger in the thickness direction with increasing impact energy. Since the signal phase varies with impact energy, there probably is a correlation between the phase of the detection signal in ECT and the development of damage in the thickness direction. 5. 11.8mm (a) energy: 0.5J (b) energy 0.75J 12.5mm (c) energy 1.0J Fig.7: Cross section radiographic testing images of CFRP damages

Results of the detection of defects in the quasi-isotropic CFRP Fig.8 shows display images of the signal amplitude of each impact defect in the quasi-isotropic specimen. Under the test conditions used, impact defects in the specimens subjected to an impact energy of less than 1.0 J were difficult to detect due to a low signal-to-noise ratio. Those in the specimens subjected to an impact energy of 1.0 J or more were detected with a high signal-tonoise ratio. Ultrasonic testing and X-ray observation of the cross-section of the damage zone will be performed later. 0.25 0.6 - - (a) energy 1.0J (b) energy 1.5J 0.6 - (c) energy 1.0J Fig.8: Image display of ECT flaw signal amplitude for quiasi-isotropic CFRP. CONCLUSION The authors performed a test to detect artificially introduced, simulated impact defects with the eddy current theta probe, and examined the correlation between the impact force and the detection signal. We also examined correlations with the results of ultrasonic testing and X-ray observation of the damage zone. No correlation was found between the amplitude of the detection signal and the impact force. The phase of the detection signal varied with the impact

force. This suggests that there is a correlation with the damage development in the thickness direction of CFRP. More data will be collected and analyzed in detail. REFERENCE 1. A.R Valleau, Eddy current nondestructive testing of graphite composite material, Materials Evaluation 48-2, p.230-1990. 2. M.Gvishi, A.H.Kahn, and M.L.Master, Eddy current testing of carbon-carbon composite, Review of Progress in QNDE, Plenum Press 11, p.289-1992. 3. M.P. de Goeje and K.E.D. Wapenaar, Non-destructive inspection of carbon fiber-reinforced plastics using eddy current methods, Composites 23-3, pp.147-157 1992. 4. R.Lange and G.Mook, Structural analysis of CFRP using eddy current methods, NDT&E International 27-5, p.241-1994 5. X.E.Gros and W.Lowden, Electromagnetic testing of composite materials, Insight 37-4, pp.290-293 1995 6. K.Koyama, K.Miki, and H.Hoshikawa, Eddy Current Non-Destructive Testing for CFRP, US-Japan Conference on Composite Materials 2008, SHM-11, pp.1-6 2008 7. K.Koyama, H.Hoshikawa and G.Kojima, Eddy current non-destructive testing for carbon fiber-reinforced composites (CFRP), Proceeding of the ASME 2010 Pressure Vessels and Piping Conference 2010 8. H.Hoshikawa and K.Koyama, A New Eddy Current Probe with Minimal Liftoff Noise and Phase Information on Discontinuity Depth, Materials Evaluation 61-3, pp.423-427 2003 9. H.Hoshikawa, K.Koyama, and H.Karasawa, Study on a New Eddy Current Testing Probe with Minimal Liftoff Noise, J. Japanese Society for Non-Destructive Inspection 50 (11), pp.736-742 2001 (in Japanese).