MetPrep 4 /PH Grinding/Polishing Systems

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Product Brochure MetPrep 4 /PH Grinding/Polishing Systems Intuitive Operation Durable, Powerful, Reliable 25 Programmable Steps Variable Platen and Sample Speed Central or Individual Sample Force Modes 1

MetPrep 4 /PH Grinding/Polishing Systems The MetPrep 4 Grinding/Polishing machine, when combined with the PH-4 or PH-6 Power Head, is a powerful system for semiautomatic operation, ideal for low to high volume sample preparation requirements. A wide variety of combinations provide ideal solutions that accommodate any application, lab or material. Intuitive operation with user-friendly push-button interface and backlit LCD make it easy to use and program. The microprocessor-based system allows up to 25 programmable steps, including parameters for platen speed, direction (comp/contra), cycle time, fluid selection, sample force, sample rotation speed, platen rinse and force reduction. PH-6 Central Force Configuration A Procedure Development step allows in-process adjustments to platen speed, sample force and sample rotation speed to determine optimum parameters. The jog mode provides convenient one-button activation of the platen without activating the Power Head. Either aluminum or magnetic platens may be used with any plain/adhesive backed or magnetic system disc. MetPrep 4 Features: Touch-pad switches control all functions Backlit 4-line LCD Programmable up to 25 polishing steps, including parameters for platen speed, comp/contra rotation (sample holder/platen), cycle time, fluid selection, sample force (LbF or N), sample rotation speed, water rinse and force reduction (On/Off, %) Variable platen speed, 10 RPM increments (see chart) Variable platen jog speed, 10 RPM increments (see chart) 3 Phase AC motor, single phase AC input with durable reduction gearbox provides constant high-torque output Variable cycle time: 0-60 minutes (15 second increments) Seamless integration with optional AD-5 Fluid Dispenser for fully automatic operation Quick-change platen design, anodized to resist wear and corrosion Electronic coolant control with adjustable flow control valve Bowl flush to prevent debris buildup Emergency shut-off switch Two (2) year warranty Designed & manufactured by Allied in the USA Up to 25 programmable steps Technical Data/Features 115 V 230 V Platen RPM 50-400 40-600 Jog RPM 50-400 40-600 Platen 10" (250 mm)/12" (300 mm) Horsepower 1½ 2 Watts 1100 1500 W 22" (560 mm) Dimensions D 27" (690 mm) H 24" (610 mm) Weight 225 lb. (102 kg) 2

Power Heads The PH-4 and PH-6 Power Heads offer maximum versatility for low to high volume semiautomatic sample preparation, using either central or individual sample force modes. The pneumatic-electric system provides controlled sample force and allows up to twelve (12) samples to be prepared simultaneously, depending on power head, mount and holder size. The unique tilt-up design allows easy, unhindered access to the sample holder and platen, and eliminates the need to reposition the head during the preparation procedure. A variety of sample holders are available for various mount and sample sizes. Sample Holders are sold separately PH Features: Central and Individual sample force modes Soft-start and force reduction control Unique tilt-up feature allows easy access to platen and holder Simple push/pull attachment and removal of sample holders Sample holders available in teardrop, dual-cavity or clamp style Lateral swivel provides versatile sample holder positioning ¼ HP (190 W) DC motor with durable reduction gearbox provides constant high-torque output Variable sample rotation speed: 0-150 RPM (10 RPM increments) Complementary or contra rotation modes Unique tilt-up feature for easy access to sample holder and platen Power Head Specifications PH-4 PH-6 Sample RPM 0-150 Horsepower ¼ (190 W) Individual Force Number of Samples 1-4 1-6 Force Range (LbF/N) 0-22/0-96 0-22/0-96 Maximum Mount Size 2"/51 mm 2"/51 mm Central Force Number of Samples 3-9 3-12 Force Range 5-90/22-394 5-90/22-394 (LbF/N) System Item Numbers Platen Voltage MetPrep 4 Diameter AC PH-4 PH-6 * 10" (250 mm) 12" (300 mm) 115 5-6510 5-6610 230 5-6510-230 5-6610-230 115 5-6512 5-6612 230 5-6512-230 5-6612-230 Use this chart to determine the item number of the system based on the desired platen diameter and power head combination. Platen diameter is determined by sample size and volume to be prepared. *PH-6 Power Head - Maximizes use of the entire 12" abrasive disc when using individual force mode 3

Central Force Holders Designed for preparing three (3) or more samples at one time. They are easier to clean and handle compared to individual holders, and are recommended for high-volume preparation requirements. Custom shapes and sizes can be designed and manufactured upon request. Teardrop Sample Holders allow flexibility in the shape and size of the sample that can be held. Dual-Cavity Sample Holders feature a single tightening point, for rapid insertion and removal of up to two round or irregular shaped specimens per cavity. An advantage of the design is that it can hold either one or two samples in a common cavity. 5-33XX Series Holders Use with 10" or 12" diameter platens. Outside diameter = 140 mm 5-3301 Sample Holder Blank Disc w/heating Stage for securing unmounted samples using wax 5-3330 (6) 1-1¼" Samples, Teardrop 5-3340 (5) 1"-40 mm Samples, Teardrop 5-3361 (6) 1-1¼" Samples, Dual-Cavity 5-3380 Sample Loading Fixture, for 5-33XX Holders 5-34XX Series Holders Use with 10" or 12" diameter platens. Outside diameter = 160 mm 5-3401 Sample Holder Blank Disc w/heating Stage for securing unmounted samples using wax 5-3435 (6) 1-1½" Samples, Teardrop 5-3440 (3) 1-2" Samples, Teardrop 5-3445 (9) 1-1¼" Samples, Teardrop 5-3460 (8) 1-1¼" Samples, Dual-Cavity 5-3461 (6) 1"- 40 mm Samples, Dual-Cavity 5-3465 (3) 2" x 1¼" (50 x 32 mm) Rectangular 5-3490 (5) 2.18" x 1.21" (55 x 31 mm) Rectangular 5-3480 Sample Loading Fixture, for 5-34XX Holders 5-36XX Series Holders Use with 12" diameter platens. Outside diameter = 200 mm 5-3601 Sample Holder Blank Disc w/heating Stage for securing unmounted samples using wax 5-3605 (12) 1-1¼" Samples, Dual-Cavity 5-3635 (6) 1-1½" Samples, Teardrop 5-3650 (3) 2l" x 3.7" (54 x 94 mm) Rectangular 5-3661 (8) 1¼"-40 mm Samples, Dual-Cavity 5-3662 (6) 40 mm-2" Samples, Dual-Cavity 5-3680 Sample Loading Fixture, for 5-36XX Holders 4

Sample Holder Compatibility Chart Sample holder selection is based on platen diameter and sample preparation procedure requirements. Sample holders are characterized by function - either Central or Individual force. Individual Force Holders Platen Diameter 10" 12" Function Series (250 mm) (300 mm) Central Individual 5-33XX X X 5-34XX X X 5-36XX - X 5-37XX X X 5-39XX - X Designed to allow as few as one or up to multiple samples to be prepared simultaneously. The advantage of individual preparation is that it allows removal of any number of samples during the grinding/polishing operation without affecting balance of the system. They are ideal for applications where small geometry and site-specific cross-section requirements make alignment of more than three (3) samples to a common plane extremely challenging. Recommended when preparing fragile materials or materials requiring lighter force (EBSD). 5-37XX Series Holders Use with PH-4 Power Head 5-3735 (4) 1" (25 mm) Mounts 5-3740 (4) 30 mm Mounts 5-3745 (4) 1¼" (32 mm) Mounts 5-3750 (4) 1½" (38 mm) Mounts 5-3755 (4) 40 mm Mounts 5-3760 (4) 50 mm Mounts 5-3765 (4) 2" (51mm) Mounts 5-39XX Series Holders Use with PH-6 Power Head 5-3935 (6) 1" (25 mm) Mounts 5-3940 (6) 30 mm Mounts 5-3945 (6) 1¼" (32 mm) Mounts 5-3950 (6) 1½" (38 mm) Mounts 5-3955 (6) 40 mm Mounts 5-3960 (6) 50 mm Mounts 5-3965 (6) 2" (51mm) Mounts PH-6 Individual Force Configuration: six (6) individual pistons apply force to the mount(s) (1.5" mounts shown). Large, rigid mount pads produce flatter samples. Central force sample holders feature a stable, low profile design allowing observation on an upright microscope (shown on a Zeiss AxioImager Microscope) 5

Accessories Aluminum platens are used with plain or adhesive back SiC discs or adhesive back, multiple-use grinding/polishing discs. If using with multiple-use grinding/polishing discs, it is recommended that one platen per disc be used. Magnetic Platens feature a non-slip magnetic foil which is permanently adhered to an aluminum platen and used with Magnetic System grinding and polishing discs. They provide a convenient method for quick and easy changing of the disc without the need to exchange or invest in multiple platens. Paper holding bands are used to secure plain back abrasive discs to aluminum platens. The inside of the band edge is designed to accommodate discs that may overhang the platen edge so the paper does not fold onto itself. They are adjustable to fit metric and imperial size platens. Platen Aluminum Magnetic Paper Diameter Platen Platen Holding Band 10"/250 mm 5-6010 5-6010M 125-10012 12"/300 mm 5-6005 5-6005M 125-10013 Aluminum Platen Magnetic Platen Platen/Disc/Cloth Storage Cabinet Durable aluminum cabinet accomodates up to ten (10) aluminum trays/shelves (reversible) for storage of platens, discs or cloths. Hinged, clear plastic door with magnetic lock prevents dust contamination. Can be stacked or wall mounted. Supplied with five (5) trays. Item Description 5-8100 Storage Cabinet for Platens, Discs or Cloths up to 12" diameter 5-8105 Tray/Shelf for #5-8100 Cabinet Specifications: Dimensions: 14" W x 14" D x 14" H (355 x 355 x 355 mm) Weight: 25 lb. (11 kg) (Shown with door removed for visual clarity) Material Removal Measuring Instrument Measuring instrument to determine material removal from samples mounted in central force sample holders. Features include a digital indicator with 1 µm (Metric) or 0.00005" (Imperial) resolution and plunger cable for remotely lifting the indicator tip. Item Description 5-3385 Measuring Instrument, for Material Removal using 5-33XX Sample Holders 5-3485 Measuring Instrument, for Material Removal using 5-34XX Sample Holders 5-3685 Measuring Instrument, for Material Removal using 5-36XX Sample Holders 6

AD - 5 Fluid Dispenser Item Custom Label each step Data displayed during operation Description 25 programmable steps 5-7000 AD-5 Fluid Dispenser, 115 V 5-7000-230 AD-5 Fluid Dispenser, 230 V Includes: Operation Manual, Power Cord (country specific), bottle labels Specifications: Dimensions: 8" W x 25" D x 9" H (203 x 635 x 228 mm) Weight: 28 lb. (13 kg) The AD - 5 Fluid Dispenser provides automatic, unattended application of polishing suspensions or lubricants. Its function can be controlled through Allied s MetPrep 3, MetPrep 4 and DualPrep 3 grinders/ polishers, or can be used with ANY brand polishing machine as a stand-alone system. Timed, volume-controlled, variable-frequency dispensing guarantees reproducible results by eliminating inconsistencies between operators, increasing productivity and efficiency in the lab. Intuitive navigation and simple-logic programming make the dispenser easy-to-use. The AD - 5 features five (5) dispensing positions, two of which include a flush cycle to prevent clogging when using colloidal suspensions. Peristaltic pump technology offers mist-free drip delivery to the polishing surface. Features: Five (5) dispensing positions, 16 oz. (500 ml) capacity User-defined labeling of each step (abrasive type & size, lubricant, cloth, material, and step name) One-touch priming function allows quick, initial charging of new cloths One-touch activation independent of step for simple operation Allows dispensing of colloidal suspensions (silica, silica/alumina and alumina) with rinse/flush function to avoid clogging Sequential programming of steps Peristaltic pump controlled dispensing 25 programmable steps Two (2) year warranty Designed & manufactured by Allied in the USA 7

Equipment is subject to change due to innovations/improvements at any time. Document No: D5-6PXXPBV1.0 Allied Equipment and Fixtures are Designed and Manufactured by Allied in the United States 2376 East Pacifica Place, Rancho Dominguez, California 90220 USA (800) 675-1118 (US/Canada) (310) 635-2466 (worldwide) www.alliedhightech.com