Workshop IGLEX Andromède & ThomX 23 June 2016, LAL Orsay. The X-line of ThomX.

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Workshop IGLEX Andromède & ThomX 23 June 2016, LAL Orsay The X-line of ThomX jerome.lacipiere@neel.cnrs.fr mjacquet@lal.in2p3.fr

Brightness panorama of X-ray (10-100 kev) sources Synchrotron : not very pratical, limited acces time High power, monochromaticity, coherence. X-ray tube: lab sources Lack of power, monochromaticity, coherence. 1

Brightness panorama of X-ray (10-100 kev) sources CCS (X-ray flux > 10 12 10 14 ph/sec) CCS principle e - beam (MeV) 20-75 MeV θ power laser 30-100 kev X ray beam 2

Brightness panorama of X-ray (10-100 kev) sources CCS (X-ray flux > 10 12 10 14 ph/sec) Compactness (surface ~ 100 m 2 ) Highintensity (10 12 10 14 ph/sec) Energy tunable beam and High X-ray energy High quality beam (brightness 10 11 10 15 ) Some powerful analyzes currently realized at synchrotrons and requiring a high brightness beam could be largely developed in a lab size environment (hospitals, labs, museums). 3

Brightness panorama of X-ray (10-100 kev) sources Next future (supra machines) Near future ( hot machines) Flux Brigthness Transv. source size E X on-axis 10 13 5. 10 11 40-100 μm 30-90 kev 4

The Compton beam e - beam (MeV) 20-75 MeV θ power laser 30-100 kev X ray beam E e = 50 MeV E X ~ 2 4 γ E ph 1 + (γθ) 2 E X (kev) ~20 mrad Univocal relation between energy E X and diffusion angle θ θ(rad) Conical beam Ex: E e = 50 MeV θ ~ 10 mrad 22 kev On axis X-rays 45 kev 5

2 ways to use a Compton beam 1. Using the 2D divergent beam - Pink beam (1% -30% bw) - Flux ~ 10 11-10 13 ph/s Measure large sample with no more need to move it (patient, animals, material ) - Several cm diameter beam 2. Using the central part of the beam after focusing Focus device(refractive lenses (CRL), Capillary optics ) Series of concave lenses IP Toward X-rays Sample Cylindrical holes as small as possible - Quasi-monochromatic beam (~ 0.1% -0.01 % bw) - Flux ~ 10 8-10 10 ph/s - < mm diameter beam 6

The X line Hall D1 Igloo 7

The X line Table 1(igloo) Continuous beam monitoring Focus device Beam transfer Security beam shutter Connection pipe Table 2 (hall D1) Beam characterisation X-user experiments Hall D1 Igloo 7

TABLE 1 Beam monitoring & focusing Connection pipe + radiation protection TABLE 2 X-Ray experiments 8

Thom X X Line Table 1 X-RAY OBTURATOR Valve system Purpose Cutting the beam for all downstream devices Measuring the background noise Design Sliding tungsten shutter + electrical actuator 2 external end-switches Beryllium window + nitrogen flange 9

Thom X X Line Table 1 SLIT SYSTEM Alignment device + Beam shape Purpose Beam selection With slit system #2, alignment of X-line Design Standard JJ X-Ray slit system design Customized stainless steel body ( vacuum tightness) Linear encoders on all movements 10

Thom X X Line Table 1 FLUORESCENT SCREEN Beam detection Purpose Detecting the presence of the beam Design Retractable fluorescent screen CCD camera Si diode (redundant information) 11

Thom X X Line Table 1 Purpose DIODES DETECTOR Intensity variation measurement Measuring beam intensity variations Design 2 Si photodiodes with symmetric translation movement 2 possible positions for the whole detector 12

Thom X X Line Table 1 Purpose BEAM PROFILER Absolute position measurement Measuring beam absolute position Design Translation of a caliper holding 2 tungsten wires inside the beam, along 1 direction 2 possible positions for the whole detector End of the line : Beryllium window + nitrogen flange 13

Thom X X Line Table 1 TRANSFOCATOR Beam collimation & focus Purpose Collimating / focusing the beam core for experiments on table 2 Design Translation of beryllium lenses inside the beam, aligned to the beam axis Independent positioning system Helium or nitrogen flush 14

Thom X X Line Table 1 TRANSFOCATOR HOLDER Alignment of the Transfocator Purpose Independent alignment of the transfocator Design Motorized manipulator with 4 independent movements 2 translations / 2 rotations High accuracy / repeatability 15

Thom X X Line Table 1 GRANIT TABLE Support of the TABLE 1 Purpose Alignment of the whole line of detectors on table1 Design Motorized assembly with 4 independent movements, 5 granite tables High range translation : extracting the whole table. High accuracy / repeatability 16

Thom X X Line Table 1 STATUS OF TABLE 1 Manufacturing & assembly All detectors, but transfocator Transfocator holder : assembly in progress Tests Table 1 : movements are OK, accuracy & repeatability to be checked All detectors : to be tested at ESRF FAME beamline in September 17

Thom X X Line Connection pipe RADIATION PROTECTION Beam Shutter + Lead Shield Purpose Safety element : protection of people inside the X-hutch Design Beam shutter is connected to the lead shield Lead shield is adjusted to the connection pipe TABLE 1 Beam monitoring & focusing Connection pipe + radiation protection TABLE 2 X-Ray experiments 18

Thom X X Line Connection pipe Connection pipe Decoupled of the X-Hutch elements Minimizing air switches Primary vacuum chain : 10-3 mbar 19

Thom X X Line Table 2 y x z Igloo wall Kapton windows?m 300mm 1m RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm 1 2 3 4a 4b 5 6 7 8 Tzf Tzp Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) TABLE 1 Beam monitoring & focusing TABLE 2 EQUIPMENT Purpose : X-ray experiments Status Still under definition no CAD design yet Highly versatile equipment Goniomètre Connection pipe + radiation protection TABLE 2 X-Ray experiments 20

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 CONNECTION PIPE HOLDER Design Adjustable holder refurbished from ESRF 2 degrees of freedom Goniomètre 21

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 SLIT SYSTEM #2 Purpose Beam selection With slit system #1, alignment of X-line Design Custom JJ X-Ray slits, aperture 150 150mm Goniomètre 22

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 GRANIT TABLE On the ground Reference horizontal surface for all devices Allowing horizontal movements with rails or air cushion Goniomètre 23

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 MONOCHROMATOR Purpose Beam wavelength selection Design Hexapod will allow 3 rotations around «Monochromator IP» Manual translation along X axis (insertion / extraction) Goniomètre 24

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 SLIT SYSTEM #3 Purpose Cleaning the beam, limiting diffusion Design Under definition, aperture 30 30mm 300mm translation along beam axis Goniomètre 25

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 GONIOMETER Fentes N 2 Moving plate + embedded systems 0-25 2 movements Rotation around vertical axis, centered on monochromator IP Vue de dessus Translation along beam axis to put sample origin on monochromator IP 26

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 SAMPLE HOLDER Purpose : Sample positioning and orienting Design Goniomètre Hexapod allowing 6 degrees of freedom (orbital movement + 3 translations), working volume 300 300 300mm Turntable allowing 360 rotation around axis perpendicular to hexapod table 27

Thom X X Line Table 2 y?m 1m x z Igloo wall Kapton windows 300mm RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 DETECTOR HOLDER 2 primary movements Rotation around vertical axis crossing sample origin Horizontal translation Goniomètre 2 secondary movements 2 concurrent rotations for slit system 28

Thom X X Line Table 2 y x z Igloo wall Kapton windows?m 300mm 1m RX PI Mono X 100mm Sample origin Tzg 1125mm Ty1 Tx1 Ty2 Tx2 Txm Tzf Ryp (centrée sur PI Mono) Ryg (centrée sur l échantillon) Tzp 1 2 3 4a 4b 5 6 7 8 STATUS OF TABLE 2 Goniomètre Work in progress 29

Outlook coming next PI Mono X Beam monitoring Highly versatile equipment 30

Outlook coming next Det Beam monitoring Dosimetry - Beam characterisation (Johann Plagnard) 31

Outlook coming next Sample 2D Det Beam monitoring Dosimetry - Beam characterisation (Johann Plagnard) Imaging - Therapy (Alberto Bravin) 32

Outlook coming next PI Mono X Sample 2D Det Beam monitoring Dosimetry - Beam characterisation (Johann Plagnard) Imaging - Therapy (Alberto Bravin) Fluorescence - Diffraction (Philippe Walter) 33

Outlook coming next Dosimetry - Beam characterisation Imaging - Therapy Fluorescence - Diffraction Thank you 34