Introduction to the development of FEFCO Testing Methods for corrugated board and boxes

Introduction to the development of FEFCO Testing Methods for corrugated board and boxes The Testing Methods n 1-7 were officially issued following the approval by national organisations, by the FEFCO General Assembly at the Vienna Congress on 29th April 1966. Since then new Testing Methods were introduced in 1968, 1971 and 1973. The Standards Committee of FEFCO proposed in 1982 to the FEFCO Board to follow several organisations in changing the testing conditions from 20 C and 65 % RH into 23 C and 50 % RH as being a world-wide standard. The approval of the proposal by the Board of FEFCO in 1983 meant consequently that the Testing Methods had to be revised. Doing this the Standards Committee took the opportunity to improve several Testing Methods to a better working level based on the experience with the methods during the past years. Since 1990 some of the Testing Methods have been amended again in order to be in line with the ISO and EN test methods as these cover the same purpose and have been internationally accepted. Altogether this leads to a complete new publication of the Testing Methods. FEFCO intends to pursue its responsibility for improving and developing Testing Methods both on corrugated board and corrugated cases. It is intended that these Testing Methods should be selectively applied, either singly or in combination with others in the series, as may be called for in the FEFCO Classification and/or in National Specifications and Regulations. Regular checking to improve method and instruments will be part of the FEFCO Test Round with the national laboratories. The application of these Testing Methods with the standardisation of instruments and processes to be used in individual laboratory tests will contribute towards providing an ever improving guarantee of the specific characteristics of corrugated board and containers and will engender increasing confidence in the employment of such material in the packaging field throughout Europe. INTRODUCTION - 1

F E F C O T E S T I N G M E T H O D N 1 July 1984 Sampling procedure 1 Scope 3.2. Selection of individual samples To define a procedure for sampling from a batch of corrugated fibreboard in sheets, or from corrugated containers, for the purpose of obtaining a representative sample for testing. The test is applicable to all kinds of corrugated fibreboard. 2 From each batch a number of bundles or pallets will be selected at random. Random means that any item shall have an equal chance of being selected as part of the sample. From each of the bundles or pallets a specified number of individual samples will be picked. From individual samples the test specimens for the various tests will be cut with adequate dimensions. A batch is a quantity of corrugated fibreboard of one sort or type which may be considered homogeneous, and may consist of one or several bundles or pallets. A sample is the total number of individual samples from one batch. An individual sample is a sheet of corrugated fibreboard, or a case, taken from a bundle or pallet. A test specimen is a piece of corrugated board cut from an individual sample. 3 3.1. References Principle Determination of the total number of individual samples The number of individual samples to be taken, as a minimum, from a batch will be determined by the formula : n = 3 N Where: n = total number of individual samples, and N = total number of sheets or cases in the batch. For convenience, the following table may be used: N n 1,000 or less 10 1,001 to 5,000 15 5,001 to 10,000 20 10,001 to 20,000 25 20,001 to 30,000 30 30,001 or more 40 (the minimum in any case will thus be 10, and the maximum 40). Each of the bundles or pallets selected according to Clause 3 will be handled as follows : After removal of the wrapping or strapping materials at least five topmost sheets or cases will be eliminated. Thereupon, so many individual samples will be picked at random from the bundles or pallets that the total number of individual samples thus obtained from the batch will equal «n» as defined in Clause 3.1. An approximately equal number of individual samples shall be taken from each bundle or pallet selected. Handling of individual samples Keep the samples flat, without compression, and protect them from direct sunlight, liquids, or anything liable to alter their condition. Marking of samples Individual samples will be marked in a corner in such a manner as to ensure perfect identification. Repeated sampling If repeated sampling is necessary, it will be done in accordance with the method. Unless it is otherwise specified, and if it is possible, samples shall not be taken from bundles or pallets which have been used for the first sampling. 4 3.3. 3.4. 3.5. Report The report will contain the following information : a Date and place of sampling b Inspector s name c Manufacturer s name d Size of batch e Number and type of bundles or pallets f Number of individual samples pursuant to clause 3.1. g Identification marks on the samples h Details of any deviation from this sampling method i Any other information which may assist in the evaluation of the sample. N 1-1

F E F C O T E S T I N G M E T H O D N 2 April 1966 (amended July 1985) Determination of the basis weight of corrugated fibreboard 1 Scope 8 Procedure To define the apparatus and procedure used to determine the basis weight of corrugated fibreboard for packing cases bearing the manufacturer s certificate. The test is applicable to all kinds of corrugated fibreboard. 2 FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 3 Test specimens of given area, taken from a representative sample of corrugated fibreboard, are brought into equilibrium with a standard atmosphere and are then weighed on a suitable accurate balance. Test results (basis weights) are expressed in g/m 2. 4 A balance with sensitivity of 0.5 g, or better, over the entire measuring range, shall be used to make the determinations. 5 References Principle Apparatus Sampling Sample in accordance with FEFCO Testing Method N 1. The testing shall be carried out in the standard atmosphere, defined in Clause 6. Each test specimen will be separately weighed and the weight recorded to the nearest 0.5 g. Unless otherwise stipulated, at least ten determinations are to be made. 9 For each determination the basis weight will be calculated by the formula: g x 10 6 G = a x b Where : G = basis weight in g/m 2 g = weight of test specimen in g a = length of test specimen in mm b = width of test specimen in mm 10 Calculation of basis weight Test report The test report will contain the following details : a Date and place of testing b Description and identification of the product tested c Results of individual tests to the nearest g/m 2 d Arithmetic mean and standard deviation of all the replicate tests e Details of any deviation from this testing method f Any other information which may assist in the interpretation of the test results. 6 Conditioning The samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1C, 50 % ± 2% r.h.). 7 Preparation of test pieces Representative samples from corrugated fibreboard to be tested shall be large enough to permit the cutting of test specimens of 500 cm2 area (200 mm ± 0.5 mm x 250 mm ± 0.5 mm). Test specimens shall be free from machine marks and other irregularities ; the surface must be free from printing or other treatments which may affect the weight ; and the edges must be cut clean and square. N 2-1

F E F C O T E S T I N G M E T H O D N 3 April 1966 (amended July 1985) Determination of the thickness (calliper) of corrugated fibreboard 1 Scope 7 Preparation of test pieces To define the apparatus and test procedure to measure the thickness (calliper) of corrugated fibreboard used in packing cases bearing the manufacturer s certificate. The test is applicable to all kinds of corrugated fibreboard. This method is applicable to all types of corrugated fibreboard. Individual samples selected from the batch must be large enough to permit the cutting of test specimens with an area of 500 cm 2 (200 mm x 250 mm). Test specimens must be free from converting machine marks, damage, or other irregularities. 8 Procedure 2 References FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. The testing shall be carried out in the standard atmosphere defined in clause 6. The plunger is to be lowered slowly, without impact. Two measurements are to be made on each test specimen, at least 50 mm from an edge, and at least ten test specimens shall be measured. 3 The thickness (calliper) of corrugated fibreboard is the distance in millimetres measured between two plane parallel faces of a micrometer, between which the test specimen is subjected to a specified pressure. 4 Principle Apparatus The measuring apparatus shall be a dead-weight dial gauge micrometer with a plane circular anvil and a concentric plane plunger. The area of the anvil and of the plunger shall be 10 cm 2 ± 0.2 cm 2. The measuring surfaces shall be parallel within 0.001 of their diameter, and the dead-weight loading of the plunger shall be 20 ± 0.5 kpa. 9 Test report The test report will provide the following information : a Date and place of testing b Description and identification of the material tested c Number of individual measurements d Arithmetic mean of all measurements in millimeters e Details of any deviation from this testing method f Any other information which may assist in the interpretation of the test results ; in particular whether any areas compressed by printing or converting machines are involved. Recommendations : the measuring capacity of the dead-weight dial gauge micrometer should be at least 20 mm. The depth of throat of the micrometer should be not less than 50 mm. The instrument shall be sufficiently accurate to permit measurement to be made to the nearest 0.05 mm. 5 Sampling Sample in accordance with FEFCO Testing Method N 1. 6 Conditioning Samples shall be conditioned accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2 % r.h.). N 3-1

F E F C O T E S T I N G M E T H O D N 4 November 1994 (amended March 1997) Determination of the bursting strength of corrugated fibreboard 1 To define the apparatus and test procedure used to determine the bursting strength of corrugated fibreboard. The test is applicable to all kinds of corrugated fibreboard. 2 FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 3 The test specimen of corrugated fibreboard is firmly clamped between annular surfaces and uniformly increasing pressure is applied to one side, by pumping liquid under a flexible diaphragm, over a circular free testing area, until the specimen bursts. The maximum pressure sustained by the specimen is recorded. 4 4.1. Type of Burst Tester A hydraulic motor-driven burst tester shall be used. 4.2. Clamping Device Scope References Principle Apparatus The burst tester must be fitted with a clamping device in which test specimens can be held without damage, other than crushing of the flutes, and without slippage, whilst the test is carried out. The clamping pressure shall be measurable. The clamping rings must be mounted parallel, and accurately centred. Diaphragm The diaphragm shall be made of highly elastic material, should be clamped securely with its upper surface about 5.5 mm below the top plane of the lower clamping plate and have the following distension / load properties : Bulge height Pressure range 10 mm 170 to 220 kpa 18 mm 250 to 350 kpa Pumping rate The pressure under the diaphragm shall be produced by an electrohydraulic pump delivering technically pure, air-free glycerine, or other suitable liquid with analogous properties, at a rate of 170 ± 15 ml per minute. Pressure measurement The total measuring capacity shall extend from 0 to 5000 kpa. Pressure measuring devices shall be fitted with the means to record maximum value. Those devices shall be calibrated 5 4.4. 4.5. 4.6. Sampling Sample in accordance with FEFCO Testing Method N 1. 4.3. Clamping Rings 6 Conditioning The internal diameter of the upper and lower clamping rings shall be 31.5 mm ± 0.1. mm. The samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2% r.h.). The edges of the clamping surfaces shall be slightly rounded. The rings shall be strong enough to withstand the clamping stresses without deformation. 7 Preparation of test pieces The internal edge at the lower face of the lower clamping ring shall be rounded, to prevent damage to the diaphragm. The clamping surfaces must be flat and should have circular or spiral grooves 0,2 mm to 0,5 mm deep to increase clamping efficiency. A sufficient number of representative samples of the corrugated fibreboard to be tested shall be available to permit the stipulated number of replicate tests to be carried out without overlap of the clamped areas. For convenience of handling, the board may be cut into specimens 150 mm x 250 mm ; this will allow one test from each side of each specimen. N 4-1/2

8 Procedure The testing shall be carried out in the standard atmosphere defined in clause 6. The specimen is placed in the clamping device and clamped with a pressure not less than 700 kpa. The maximum reading device is set to zero and the tester operated until the specimen bursts. Test results should be recorded to 3 significant figures. Unless otherwise stipulated, 10 tests are to be made from each side of the corrugated fibreboard. 9 Test Report The test report should contain at least the following points : a b c d e f g h i Date and place of testing Reference to this FEFCO testing method Description and identification of the product tested Value of each test Arithmetic mean and standard deviation of all replicate test results Clamping pressure in kilopascal Details of any deviation from this testing method Any other information which may help in the interpretation of the test results Name and signature of the operator. N 4-2/2

F E F C O T E S T I N G M E T H O D N 5 July 1985 (reapproved and improved version of 1966) Determination of the puncture resistance of corrugated fibreboard 1 To define the apparatus and test procedure use to determine the puncture resistance of corrugated fibreboard used in packing cases bearing the manufacturer s certificate. The test is applicable to all kinds of corrugated fibreboard. 2 FEFCO testing method n 1 : sampling procedure. EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 3 Scope References Principle A representative sample of corrugated fibreboard is subjected to puncture by a triangular pyramid puncture head attached to a pendulum. The energy required to force the puncture head completely through the sample i.e. - to make the initial puncture, and to tear and bend open the fibreboard - is measured in J (N.m). One of the edges of the base of the pyramid shall be parallel to the axis of rotation of the pendulum, and the opposite corner of the base shall point towards the axis of rotation. The axis through the effective point of the puncture head shall be vertical when its mid-point passes through the horizontal plane through the axis of the pendulum. [1]. At release point the pendulum shall be in the horizontal position, which is determined by measuring through an angle of 90 from the pendulum with its centre of gravity at rest. 4.3. Measuring ranges By the use of interchangeable weights which can be attached to the pendulum, several ranges of energy are to be provided. The range selected should be such that the test result will be between 20 % and 80 % of the maximum value of the corresponding scale. 4.4. Release mechanism A safety catch must be provided to prevent accidental release of the pendulum. The release mechanism must not impart any acceleration or deceleration to the pendulum. 4 Apparatus 4.5. Collar 4.1. Type of puncture tester The instrument to be used produces an impact by means of a pendulum. The bed plate of the frame of the instrument must be firmly attached to a strong base to prevent energy losses. The instrument must be accurately levelled, and it must not vibrate during the test. The instrument must be so designed that the energy contained in the pendulum in each of the measuring ranges corresponds to the respective scale. This condition is the responsibility of the instrument manufacturer to whom appeal shall be made if there is any doubt as to the accuracy of the instrument, particularly if it is suspected that changes have occurred in the distribution of the pendulum, including the supplementary weights. 4.2. Pendulum and puncture head The pendulum shall be fitted with an arm, having the shape of a 90 circular arc, to which the puncture head is attached. Both pendulum and arm must be strong enough to preclude deformation and to minimise vibration when the test is carried out. The puncture head shall be a triangular, height 25.0 ± 0.7 mm the edges of which, meeting at the vertex, form right angles. All edges between sides are to be rounded off, radius = 1 mm. The neck of the puncture head shall be fitted with a close fitting collar designed so as to slip off its seating and to keep open the aperture in the test specimen after the puncture head has passed through. This is to prevent the fibreboard from springing back on the arm and braking the pendulum, thus altering the test result. The loss of energy due to friction when the collar is forced off its seating shall be measurable and shall not exceed 0.25 J. This loss of energy shall be compensated for in the reported test result. 4.6. Clamping device To hold the test specimen, two horizontal clamping plates shall be provided, the upper plate being fixed. The lower face of the upper clamping plate -which contacts the test specimen- shall be on the horizontal plane through the axis of the pendulum, or up to 7 mm above it. Both clamping plates must be sufficiently rigid to withstand the clamping forces employed, without deformation. [1] To permit the use of existing instruments, the axis through the effective point of the puncture head may be vertical when its mid-points is within ± 12.5 mm of the horizontal plane through the axis of the pendulum. N 5-1/2

The effective clamping dimensions of the clamping plates shall be not less than 175 mm x 175 mm. The upper clamping plate shall have a centrally positioned regular triangular aperture with sides 100 mm ± 2 mm in length. Whilst it is recommended that the aperture in the lower plate should be identical and coincident with that in the upper plate, a centrally positioned circular aperture, with a diameter 90 mm ± 2 mm, is permissible. [2]. 4.7. Clamping force The force holding the test specimen between the clamping plates shall be at least 400 N and not more than 1000 N. If the instrument has no device for measuring the clamping force, the force applied must in any case be sufficient to ensure that the test specimen does not slip when the test is carried out. 4.8. Indication of the measured result The test result shall be indicated by a peak-indicator, e.g. a friction loaded pointer operating over a dial on which the several scales, corresponding to the energy ranges, are engraved. The scale divisions should be calibrated in J (N.m). In case of a friction loaded pointer, the friction mounting of the pointer should be sufficient to ensure smooth operation without over-run. 4.9. Adjustment of the instrument For all measuring ranges the effective point of the puncture head shall be within ± 5 mm of the horizontal plane through the axis of rotation of the pendulum, when the centre of gravity of the pendulum is at its lowest point. 4.10. Instrument checks No compensation for loss of energy due to friction should be made in the calibration of the measuring scales. Energy loss due to friction in the bearings of the pendulum and air resistance must not exceed 1 % of the measuring scale. To measure energy loss due to collar friction a slip-off device must be provided which catches the collar when the pendulum is allowed to swing freely from the release point. Energy losses due to pointer friction shall be determined by allowing the pendulum to make two free swings from the release position. The first swing should carry the pointer close to the scale zero. The second free swing, made without resetting the pointer, should carry the pointer nearer to the zero reading. The difference between the two readings will represent the energy loss due to pointer friction. When making readjustments to the settings of the measuring scales the following checks should be made: Allow the pendulum to come to rest, with its centre of gravity at the lowest point, then move the pointer towards the maximum scale value. If, in the position, the drive pin of the pendulum just touches the pointer, the setting is correct. An analogous check should be carried out with the pendulum in the horizontal position, 180 from the release point, when the pointer should indicate zero. 6 Samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2 % r.h.). 7 Test specimens with minimum dimensions 175 mm x 175 mm shall be prepared from a representative sample of the corrugated fibreboard to be tested. These test specimens must be free from conversion machine marks, irregularities, or damage. In no instance shall the puncture area be less than 60 mm from the edge of the sample, or from any crease, score, or printed area. If for some reason a printed area is used for the test, then this must be clearly stated in the test report. 8 The testing shall be carried out in the standard atmosphere defined in clause 6. The test specimen will be placed between the clamping plates and clamped with a constant force which should be recorded if the instrument is equipped with a clamping force measuring device. The pendulum mass shall be adjusted, using the supplementary weights as necessary, to operate over the energy range which will contain the expected test result within 20 % and 80 % of its maximum value. The release mechanism shall then be operated and the puncture head will completely pierce and pass through the test specimen. The amount of energy used, representing the work in puncturing the test specimen is to be read from the appropriate scale. Scale readings should be to the nearest 0.1. J for the measuring ranges up to 12 J, and to the nearest 0.2 J for measuring ranges above 12 J. The test result shall then be compensated for predetermined energy losses caused by friction in the apparatus (pointer friction, forcing off the pyramid collar, etc). Unless otherwise stipulated, ten replicate tests are to be made from each side of the corrugated fibreboard ; five tests from each side with the flutes parallel with the axis of rotation of the pendulum ; and five tests from each side with the flutes at right angles to the axis of rotation of the pendulum. 9 Conditioning Preparation of test pieces Procedure Test report The test report will contain the following information : a Date and place of testing b Description and identification of the material tested c Number of replicate tests carried out d Arithmetic mean of all the replicate test results in J (N.m) e Standard deviation of the arithmetic mean in J (N.m) f Clamping force in N g Details of any deviation from this testing method h Any other information which may assist in the interpretation of the test results. 5 Sampling 10 Note Sample in accordance with FEFCO Testing Method N 1. [2] To permit the use of certain existing types of instruments, the lower plate may have a centrally positioned circular aperture with a diameter up to 100 mm. Interlaboratory tests showed, that the puncture resistance of corrugated boards tested in different laboratories may be assumed to be identical with a high degree of probability if the difference of the arithmetic mean is less than ca. 7... 8%. N 5-2/2

F E F C O T E S T I N G M E T H O D N 6 July 1985 (improved version of 1966) Determination of the flat crush resistance of corrugated fibreboard 1 Scope 4.3. Relative speed and force To define the apparatus and test procedure used to determine the flat crush resistance of corrugated fibreboard used for packing cases bearing the manufacturer s certificate. The test may be carried out on single face and double face (single wall) corrugated fibreboard. It is not suitable for testing the flat crush resistance of double-double face (double wall) board. 2 References The relative speed between the two platens shall be 12.5 mm ± 2.5 mm per minute (with testers operating on the principle of beam deflection this is equivalent to an increment of force of 67 ± 23 N per second when the platens are in contact with each other). 4.4. Cutting instrument An instrument having a circularly guided knife to cut specimens with area of 100 cm 2 (diameter 112.8 ± 0.5 mm), or an area of 50 cm 2 (diameter 79.80 ± 0.5 mm) shall be used. The cut edges must be clean and perpendicular to the facings of the board. FEFCO testing method n 1 : sampling procedure 5 Sampling EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. Sample in accordance with FEFCO Testing Method N 1. 6 Conditioning 3 Principle Samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2 % r.h.). A test specimen of corrugated fibreboard is subjected to a uniformity increasing force applied perpendicularly to the surface by a compression tester having two flat and parallel platens, until the fluting collapses. The maximum force sustained by the specimen is recorded. 4 4.1. Type of flat crush tester A motor-driven type compression tester shall be used. If the tester operates on the principle of beam deflection the beam shall be such that the test results will occur within 20 % to 80 % of the normal range of deflection. 4.2. Platens Apparatus The platens must meet the following conditions : deviation from parallel not greater than 1:1000 lateral play not exceeding 0.05 mm size : 120 mm x120 mm to take 100 cm 2 or 50 cm 2 specimens. Note : the preferable size for beam tester is 50 cm 2. 7 Unless otherwise stipulated, at least ten specimens of the board shall be tested. They shall be free from converting machine marks, printing, or damage. 8 The testing shall be carried out in the standard atmosphere defined above in clause 6 unless otherwise stipulated. The test specimen shall be placed centrally on the lower platen, and the tester operated until the fluting collapses. The maximum pressure sustained by the specimen before collapse of the fluting will be recorded to the nearest 10 kpa (kn/m 2 ). 9 Preparation of test pieces Procedure Test report The test report will contain the following details : a Date and place of testing b Description and identification of the product tested c Results of individual tests to the nearest 10 kpa (kn/m 2 ) d Arithmetic mean and standard deviation of all the replicate test results e Number of specimens with leaning flutes f Details of any deviation from this testing method g Any other information which may assist in the interpretation of the test results. N 6-1

F E F C O T E S T I N G M E T H O D N 7 April 1986 (amended in1985, 1994, March 1997) Determination of water absorptiveness of corrugated fibreboard (Cobb test) 1 Scope 6 Sampling This testing method specifies the apparatus and the procedure for determining the water absorptiveness of corrugated fibreboard in 30 minutes (1800 sec.). The method is applicable to all types of corrugated fibreboard. For paper the EN 20 535 testing method should be used. 2 FEFCO testing method n 1 : sampling procedure. EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. EN 20 535 : paper and board - Determination of water absorptiveness - Cobb Method. 3 One specified side and a specified area of a corrugated fibreboard test piece is exposed to a defined column of water for 30 minutes. Its water absorptiveness is deducted from the difference of weightings immediately before and immediately after exposure to water. 4 Freshly distilled or deionized water at a temperature of 23 C ± 2 C. Soft blotting paper 250 g/m 2 ± 25 g/m 2 grammage. 5 5.1. 5.2. 5.3. 5.4. 5.5. References Principle Reagent and material Apparatus Rigid smooth finished cylindrical tank of either 100 cm 2 or 50 cm 2 internal cross sectional area, of sufficient depth to provide a head of at least 3 mm of water. When necessary to form an effective seal, the cylindrical tank, with its base possibly covered by a non-absorbent rubber ring of the same cross sectional area, may be fitted with a means of lightly clamping to the corrugated fibreboard test piece. Smooth stainless metal roller, 200 mm wide, 90 mm ± 10 mm diameter, 10 kg ± 0,5 kg mass. Analytical balance sensitive to 1 mg. Stop watch readable in seconds. Glass measuring cylinder to prepare aliquots of water. Sample in accordance with FEFCO Testing Method N 1. 7 The samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1C, 50 % ± 2% r.h.). 8 Prepare the test pieces in the same atmosphere as for conditioning the samples. From representative and undamaged areas of the samples, cut at least 3 test pieces for each specified condition (test on inner liner, or test on outer liner, unprinted or printed areas, etc.) with dimensions 10 mm greater than the external cross sectional area of the cylindrical tank. Avoid contact of bare hands on test pieces. 9 Carry out the tests in the same atmosphere as for conditioning the samples. Ensure before each test that the cylindrical tank is dry. Weigh the test piece to the nearest 1 mg (m 1). Apply the tank cylinder to the specified side and the specified area of the test piece. Pour the specified water in the cylindrical tank to form a head of at least 3 mm of water upon the test area of the test piece and start the stop watch immediately. After 30 minutes of exposure to water, quickly pour out the water, remove the cylindrical tank, place the blotting paper on the tested area of the test piece, roll the metal roller once forwards and once backwards with its axis parallel to the flutes, and weigh again the test piece to the nearest 1 mg (m 2 ). Renew the water and the blotting paper for the subsequent test pieces. 10 Conditioning Preparation of test pieces Procedure Expression of test results The water absorptiveness value A to the nearest g/m 2 of each test piece is : m 2 - m 1 A = S where : m 1 : mass of the test piece before exposure to water in g m 2 : mass of the test piece after exposure to water in g S : nominal cross sectional area of the cylindrical tank in m 2 For each test condition, calculate the arithmetic mean of the replicate test results to the nearest g/m 2. N 7-1/2

11 Test report The test report shall contain at least the following informations : a Date and place of the testing b Reference to this FEFCO testing method c Complete identification and description of the material tested d Duration of exposure to water, if not 30 minutes e Nominal cross sectional area of the cylindrical tank f Number of replicate test for each test condition g Replicate test results and arithmetic mean for each test condition h Details of any deviation from this testing method i Any information which may assist in the interpretation of the test results j Name and signature of the operator N 7-2/2

F E F C O T E S T I N G M E T H O D N 8 1982 (amended in 1989, 1994, March 1997) Edgewise crush resistance of corrugated fibreboard 1 The edgewise crush resistance of corrugated fibreboard is the maximum compressive force that a test piece will sustain before being crushed, the test piece standing on one edge and the force being applied to the opposite edge under specified conditions. The edgewise crush resistance of corrugated fibreboard can be very much affected by conversion of board into packaging. It is also affected when the packaging is in use. It is therefore important that the origin of the sample being tested is fully identified under 10. Test report. 2 To define the apparatus and test procedure used to determine the edgewise crush resistance of corrugated fibreboard. This method is applicable to all types of corrugated fibreboard. 3 FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 4 Definition Scope References Principle A rectangular specimen of the corrugated fibreboard is placed between the platens of a crush tester with the flutes perpendicular to the platens, and is subjected to an increasing compressive force until failure occurs. The maximum force sustained by the specimen is recorded and the edgewise crush resistance calculated. Platens The platens must meet the following conditions : size large enough to take test specimens of 100 mm length deviation from parallel not greater than 1:1000 lateral play not exceeding 0.05 mm flat with at most 0.1 mm deviation from the median plane. 5.3. Compression speed The tester operates with one fixed platen, the other having a direct positive drive, the rate at which the platens approach each other shall be 12.5 mm/mn ± 2.5 mm/min. Cutting equipment Cutting equipment designed to give rectangular test pieces with parallel, clean, straight edges. The cutting shall be done perpendicularly to the flutes in one operation for instance by single bevelled knives which have a thickness of about 0.5 mm, used not more than 50 times or by a high speed rotary saw. Guide blocks Two rectangular, smooth finished, metal blocks, 20 mm x 20 mm, and at least 100 mm in length, to support the test piece and keep it perpendicular to the platens. 6 Sample in accordance with FEFCO Testing Method N 1. 7 5.2. 5.4. 5.5. Sampling Conditioning Samples shall be conditioned accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2 % r.h.) The corrugated board has to be conditioned before cutting, and to be kept conditioned throughout the test. 5 Apparatus 8 Preparation of test pieces 5.1. Crush tester A power driven crush testing machine with horizontal platens designed to measure compressive force, shall be used. For testing machines operating on the principle of beam deflection, see note. 8.1. 8.2. From the corrugated board to be tested, strips 100 mm ± 0.5 mm wide will be cut in the direction of the glue lines. Out of these strips, perpendicularly to the glue lines, test pieces of 25 mm ± 0.5 mm nominal height will be cut. The maximum difference between any two dimensions having the same nominal value must not exceed 0.2 mm. N 8-1/3

8.3. Unless otherwise stipulated, 10 test pieces of the board shall be tested. 8.4. When converted board is tested, test pieces should be free from converting machine marks, printing and any damaged areas. 9 Procedure The test piece shall be placed centrally on the platen with its shorter edges perpendicular to the platens and supported by the guide blocks. By operating the tester, the load is increased until the test piece collapses. The maximum load sustained is rounded to the nearest 10 N. Calculate the edgewise crush resistance R, in kilonewtons per metre according to the equation below, where F is the maximum load, in newtons. L is the length of the test piece in millimetres (here L = 100). F R = kn/m L 10 Test report The test report shall contain the following details : a Date and place of testing b Reference to this FEFCO Method c Description and identification of the product tested d Results of individual tests to be stated in kn/m e Arithmetic mean and standard deviation of all the replicate test results f A specific statement that a testing machine working on the principle of beam deflection has been used if relevant g Details of any deviation from this testing method h Any other information which may assist in the interpretation of the test results i Name and signature of the operator Note: when a tester operating on the principle of beam deflection is used, results are valid only if they occur between 20 % and 80 % of the maximum range of deflection, that can be measured with the beam and dial in question. N 8-2/3

Cutting Head - with two parallel blades Emery Cloth Test-piece Counter Pneumatic Cylinder End Stop Fig. 1 Edge Crush Sample Cuttier Cutting Head Specification Locating Pin Details of Cutting Blades N 8-3/3

F E F C O T E S T I N G M E T H O D N 9 July 1985 (improved version of 1968) Determination of the water resistance of the glue bond of corrugated fibreboard by immersion 1 Scope To define the apparatus and test procedure used to determine the water resistance of the glue lines of corrugated board. This method is applicable to all types of corrugated board for which a high degree of bond strength is required to resist the influence of wet conditions. 4.8. 4.9. A 250 g copper weight for each test specimen. Each of these weights shall be provided with a hook. A time control device. 2 FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 3 The water resistance of the glue of corrugated fibreboard is expressed by the length of time during which a predetermined combination of glue lines, immersed in water, resists the pull of a suspended weight in the plane vertical axis of the board, at a right angle to the glue lines. 4 4.1. References Principle Apparatus A water tank, preferably glass, for easy observation, large enough for the free suspension of the required number of test specimens. The depth of the tank shall be at least 25 cm. The bottom of a glass tank may be lined with a rubber sheet to prevent damage. 5 Sample in accordance with FEFCO Testing Method N 1. 6 The samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2% r.h.). 7 7.1. Sample Individual samples must be large enough to permit the cutting of test pieces, size 20 mm ± 1 mm by 150 mm approximately, with the flutes at right angles to the length of the specimen. Except for routine production control tests, the corrugated board to be tested should generally be at least three days old to allow it to develop its water resistance properties. The time will be dependent on temperature and adhesive formulation. 7.2. Preparation of test pieces Test specimens Sampling Conditioning 4.2. 4.3. 4.4. 4.5. 4.6. 4.7. A number of rods or bars with hooks. These to be placed across the tank for suspension of the test specimens. Means for proper identification of test specimens shall be provided. A soft rubber stamp to mark the sample corrugated board with outlines and other details for cutting the test specimens. The design to be imprinted on the corrugated board is shown in fig.1. A knife with a sharp, thin blade. A straight edge. Punch pliers. Eyelet pliers, and eyelets. The test specimens shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2% r.h.). To guide the operator in preparing the test pieces, the corrugated board sample will be marked by means of the rubber stamp (clause 4.3.). The specimens to be tested are picked at least 50 mm away from a crease, edges and finger lines and also from small local defects in the paper. Not more than one specimen should be cut out of an area approx. 1/2m 2. Unless otherwise specified test pieces have to be free from all irregularities or damage, especially by water, mechanical stress (e.g. finger lines). Two holes shall be punched into the pieces, their centres being at a distance of 10 mm from either end and side, respectively. Eyelets are inserted into these holes and clenched. N 9-1/4

Alternatively a suitable clamp may be used to suspend the test specimen from the rod. A cooper clamp may be used at the lower end to suspend the weight. This clamp and any additional copper weight shall not exceed a total of 250 g. Determination of the glue lines to be tested The shearing stress is concentrated on five lines to be tested within zone M (see fig. 1). These glue lines shall be isolated by cuts through the components as may be necessary to achieve this object, as exemplified in fig. 2 for single wall, fig. 3 for double wall board. 8 7.3. Procedure Five test pieces of each set of glue lines to be tested (standard number), with their ends loaded with weight (see 4.8), are suspended in the tank, which be filled with neutral water (distilled, deionized, demineralized, hydrant) that all M zones (clause 7.3.) of the specimens remain immersed 25 mm below the surface of the water throughout the test period. Care should be taken to avoid the inclusion of air bubbles in the flutes. 10 Interpretation of the test results The board can be considered as «water resistant» : if for every test specimen the time of resistance is at least 24 hours without a dropped weight (standard : 5 test pieces of each cutting type). should there be one early failure per sample type within a period of 24 hours under load, the test will have to be repeated with the corresponding sample type with the full number of specimens (standard : 5 test pieces). In this case the test will also be considered as successful, if in the repeated test all specimens remain resistant for at least 24 hours. in all other cases (more than one early failure per sample below 24 hours in the first test round, as well as one more early failure in the repeated testing), then the test will be considered as not successful. Sporadical weak spots in the paper being technically unavoidable, are not taken into consideration in respect to moisture-proof bonding. (Sporadical impurities do not influence the acceptance but systematical ones in the paper may be a reason for rejection). Individual test pieces will not be used to test more than one set of five glue lines between the selected lines and its fluting. 11 Notes 8.1. Test temperature The temperature of the water shall be 23 C ± 1 C. 8.2. Timing The immersed specimens will be checked for failure at 24 hour or such shorter intervals as may be suitable. An automatic time control device is recommendable. Water resistance of the manufacturer s joint of a box. (Only valid for joints, made with an adhesive or taping band, which can be reactivated with water). This is also a very good method to test the water resistance of the manufacturer s joint of a box. In this case 2 cm wide strip cuts across the manufacturer s joint are tested according the prescribed method for ordinary board specimens. The whole glued zone has to remain under water. The evaluation of test results has to be done as described in clause 10. 8.3. Failure Failure of a specimen is shown by complete separation of the five bonds on the same liner side, which will cause the weight to drop. 9 Test report The test report will contain the following details : a Date and place of testing b Description and identification of the product tested c Identification of each specimen tested d Number of specimens tested and number of failures at each set glue lines at the chosen test intervals. State intervals. e Statement whether after rupture : * fibres adhere to the glue * glue predominates on the fibre surface. f Details of any deviation from this testing method g Any other information which may assist in the interpretation of the test results. N 9-2/4

F E F C O T E S T I N G M E T H O D N 9 Diagrams Cut. Test zone 5 flute tips Cut. Fig. 1 Rubber stamp Fig. 2 Diagram showing suspension arrangement and typical cuts in s.w. board N 9-3/4

Diagrams showing typical cuts in D.W. board to isolate the five glue lines, to be tested Cut. Cut. Zone Cut. Cut. A flute/liner Fig. 3 A flute/centre B flute/liner Fig.4 B flute/centre N 9-4/4

F E F C O T E S T I N G M E T H O D N 1 0 July 1985 (improved version of 1968) Determination of the basis weight of the component papers of corrugated fibreboard after separation 1 Scope 5 Sampling To define the apparatus and procedure used to determine the basis weight of the individual papers from which corrugated fibreboard has been made. This method is applicable to all types of corrugated fibreboard. 2 References FEFCO testing method n 1 : Sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. EN ISO 536 : paper and board - Determination of grammage FEFCO testing method n 6 : Determination of the flat crush resistance of corrugated fibreboard. Sample in accordance with FEFCO Testing Method N 1. 6 Samples shall be conditioned accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2 % r.h.). 7 Conditioning Preparation of test pieces Individual samples of board of sufficient size to provide the test pieces shall be cut from the corrugated fibreboard to be tested. The surfaces of the fibreboard shall be free from any damage which may affect the results. Test specimens shall preferably be taken from nonprinted and noncoated board. After conditioning the test specimens, cut test pieces of board, each of 100 cm 2 area minimum using cutting device specified at 4.3. The cut edges shall be clean and perpendicular to the faces of the board. 3 Test specimens of corrugated fibreboard are treated so that the individual components can be separated. The component papers are then dried and conditioned, and subsequently used for the determination of their basis, in accordance with EN ISO 536. 4 Principle Apparatus 8 8.1. Procedure Separation of components papers Test specimens shall be immersed long enough in water to cause the component sheets of paper to separate spontaneously or with an extremely light pull. Care shall be taken, in separating the papers that no fibres be removed from a surface and adhere to the adjoining one. To accelerate the process, and to separate corrugated board whose glue bond is more or less moisture resistant, hot water may be used. 4.1. A tank of sufficient size for immersion of the board specimens, to contain cold or hot water. 8.2. Removal of adhesive showing on the surface of the paper 4.2. 4.3. 4.4. Means for drying the test specimens when separated, to contain cold or hot water. A cutting instrument having a circularly guided knife to cut test pieces with an area of 100 cm2 (diameter 113 mm ± 0.5 mm) shall preferably be used. (see FEFCO Test Method N 6, para 4.4.). Alternatively a sharp knife and straight edge may be used. A balance with sensitivity of 0.01 g or better over the entire measuring range (this will make it possible to determine from test pieces of 100 cm 2 area their grammage to a precision of 1 g/m 2 ). Adhesive which has not been absorbed by the paper may be removed, while wet, by lightly scraping the surface. Complete removal of the absorbed adhesive cannot be expected. 8.3. Drying of the separated papers The individual papers shall be dried in a temperature not exceeding 125 C and conditioned. 8.4. Weighing fluting medium After cleaning and conditioning the fluting medium shall be flattened and recut to give an area of 100 cm 2. N 10-1/2

8.5. Individual tests The weighing shall be carried out in the standard atmosphere (specified at Clause 6). Each specimen of component papers is to be weighed individually to the nearest 0.01 g. 8.6. Number of individual determinations Unless otherwise specified, the component papers of five specimens of corrugated board shall be tested. 9 Test report The report will contain the following details : a b c d e f g h Date and place of testing Description and identification of the corrugated board tested Description and identification of the individual papers Number of test pieces Results of the individual tests in g/m 2 Arithmetic mean of the individual tests Details of any deviation from this FEFCO Testing Method Any other information which may be essential for the interpretation of the results. N 10-2/2

F E F C O T E S T I N G M E T H O D N 1 1 July 1985 (improved version of 1971) Determination of the adhesion strength of the glue bonds of corrugated fibreboard (pin method) 1 Scope 4.2. Cutting equipment To define the apparatus and procedure to be used to determine the strength of the adhesion between the flutes and liners of corrugated board. This method is applicable to all types of corrugated fibreboard. This shall ensure that the cut edges are clean, straight and perpendicular to the facings of the board. 4.2.1. A bandsaw or knife and cutting jig may be used. 2 FEFCO testing method n 1 : sampling procedure EN 20 187 : paper, board and pulps - Standard atmosphere for conditioning and testing and procedure for monitoring the atmosphere and conditioning of samples. 3 Two assemblies of metal pins are introduced into spaces between the flutes of the adhesive joints to be tested, in such a way that by means of a holder and a crush tester the sets of joints are separated by the application of a force applied perpendicularly to the surface of the board. The force needed to separate the liner from the fluting is measured and reported. 4 4.1. Crush tester [1] References Principle Apparatus A power-driven type crush tester shall be used. (When a tester operating on the principle of beam deflection is used, results are valid only if they occur between 20 % and 80 % of the normal range of deflection). 4.1.1. Platens The platens must meet the following conditions : deviation from parallel not greater than 1:1000 lateral play not exceeding 0.05 mm minimum size large enough to take test specimens of 100 mm length. 4.1.2. Compression speed The relative speed of the two platens shall be 12.5 mm ± 2.5 mm per minute (with testers working on the principle of beam deflection this is equivalent to an increment of force of 67 N/s ± 23 N/s when the platens are in contact with each other). [1] As an alternative to the crush tester specified at 4.1., other suitable apparatus operating at the speed given at 4.1.2. and meeting the requirements of clause 3 may be used. Full particulars of alternative apparatus used shall be reported under 9. Pin holder assemblies The apparatus to be used shall be of any suitable type permitting the perpendicular force to be applied selectively to the liner/flute lines to be tested. Annexe 1 shows the points at which the pins shall be inserted to enable the test to be effected on the selected liner and fluting. The pins shall be sufficiently rigid so that they are not bent during the test and of a diameter and arrangements that will not distort or deform the flute profiles of the board tested. Unless otherwise specified it is recommended that a combination of 6 and 7 pins shall be used. The following pin diameters are normally suitable : A flute = 3 mm B flute = 2 mm C flute = 2.5 mm 5 Note: Flute distance may vary with corrugator manufacturer. Thus, to make appropriate apparatus use pin diameter and tolerance for each flute size, and adjust pin spacing (distance between pins). Sample in accordance with FEFCO Testing Method N 1. 6 Samples shall be conditioned in accordance with EN 20 187 (i.e. 23 C ± 1 C, 50 % ± 2% r.h.). 7 4.3. 7.1. Preparation of test pieces Sample Sampling Conditioning The samples must be taken from board of sufficient area to permit the cutting of the required number of test specimens which shall be free from machine marks, or other damage. N 11-1/2