Amy E. Frees Duke University Durham, NC TECHNICAL REPORT RDMR-WD And. October 2015

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TECHNICAL REPORT RDMR-WD-15-22 NEAR-FIELD TERAHERTZ TRANSMISSION IMAGING AT 0.210 TERAHERTZ USING A SIMPLE APERTURE TECHNIQUE Martin S. Heimbeck and Henry O Everitt Weapons Development and Integration Directorate Aviation and Missile Research, Development, and Engineering Center And Amy E. Frees Duke University Durham, NC 27708 October 2015 Distribution Statement A: Approved for public release; distribution is unlimited.

DESTRUCTION NOTICE FOR CLASSIFIED DOCUMENTS, FOLLOW THE PROCEDURES IN DoD 5200.22-M, INDUSTRIAL SECURITY MANUAL, SECTION II-19 OR DoD 5200.1-R, INFORMATION SECURITY PROGRAM REGULATION, CHAPTER IX. FOR UNCLASSIFIED, LIMITED DOCUMENTS, DESTROY BY ANY METHOD THAT WILL PREVENT DISCLOSURE OF CONTENTS OR RECONSTRUCTION OF THE DOCUMENT. DISCLAIMER THE FINDINGS IN THIS REPORT ARE NOT TO BE CONSTRUED AS AN OFFICIAL DEPARTMENT OF THE ARMY POSITION UNLESS SO DESIGNATED BY OTHER AUTHORIZED DOCUMENTS. TRADE NAMES USE OF TRADE NAMES OR MANUFACTURERS IN THIS REPORT DOES NOT CONSTITUTE AN OFFICIAL ENDORSEMENT OR APPROVAL OF THE USE OF SUCH COMMERCIAL HARDWARE OR SOFTWARE.

Form Approved REPORT DOCUMENTATION PAGE OMB No. 074-0188 Public reporting burden for this collection of information is estimated to average 1 hour per response, including the time for reviewing instructions, searching existing data sources, gathering and maintaining the data needed, and completing and reviewing this collection of information. Send comments regarding this burden estimate or any other aspect of this collection of information, including suggestions for reducing this burden to Washington Headquarters Services, Directorate for Information Operations and Reports, 1215 Jefferson Davis Highway, Suite 1204, Arlington, VA 22202-4302, and to the Office of Management and Budget, Paperwork Reduction Project (0704-0188), Washington, DC 20503 1.AGENCY USE ONLY 2. REPORT DATE October 2015 4. TITLE AND SUBTITLE Near-Field Terahertz Transmission Imaging at 0.210 Terahertz Using a Simple Aperture Technique 6. AUTHOR(S) Martin S. Heimbeck, Henry O. Everitt, and Amy E. Frees 3. REPORT TYPE AND DATES COVERED Final 5. FUNDING NUMBERS 7. PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) Commander, U.S. Army Research, Development, and Engineering Command ATTN: RDMR-WDI Redstone Arsenal, AL 35898-5000 8. PERFORMING ORGANIZATION REPORT NUMBER TR-RDMR-WD-15-22 9. SPONSORING / MONITORING AGENCY NAME(S) AND ADDRESS(ES) 10. SPONSORING / MONITORING AGENCY REPORT NUMBER 1 1. SUPPLEMENTARY NOTES 12a. DISTRIBUTION / AVAILABILITY STATEMENT Approved for public release; distribution is unlimited.. 12b. DISTRIBUTION CODE A 13. ABSTRACT (Maximum 200 Words) This report discusses a simple aperture useful for terahertz near-field imaging at.2010 terahertz (λ = 1.43 millimeters). The aperture requires no intricate fabrication techniques and connects easily to conventional terahertz output horns. Tests show that the near-field aperture is able to achieve a spatial resolution of λ/7. The aperture can be scaled with the assistance of machinery found in conventional machine shops to achieve similar results using shorter terahertz wavelengths. 1 4. SUBJECT TERMS Near-Field Imaging, Terahertz Imaging 15. NUMBER OF PAGES 14 16. PRICE CODE 17. SECURITY CLASSIFICATION OF REPORT UNCLASSIFIED 18. SECURITY CLASSIFICATION OF THIS PAGE UNCLASSIFIED 19. SECURITY CLASSIFICATION OF ABSTRACT UNCLASSIFIED 20. LIMITATION OF ABSTRACT NSN 7540-01-280-5500 Standard Form 298 (Rev. 2-89) Prescribed by ANSI Std. Z39-18 298-102 SAR i/ii (Blank)

TABLE OF CONTENTS Page I. INTRODUCTION... 1 II. THEORY AND EXPERIMENT... 1 III. RESULTS... 4 IV. CONCLUSION... 6 REFERENCES... 7 LIST OF ABBREVIATIONS, ACRONYMS, AND SYMBOLS... 8 iii

LIST OF ILLUSTRATIONS Figure Title Page 1. Diffraction Limited Terahertz Imaging Setup... 2 2. Near-Field Aperture Horn... 2 3. Near-Field Imaging System... 3 4. 1951 USAF Resolution Target... 3 5. Diffraction Limited Image... 4 6. Near-Field Image at 0.210 Terahertz... 5 7. Cross Sections of Near-Field Image... 5 8. Near-Field Image Showing Locations of Cross Sections in Figure 7... 6 iv

I. INTRODUCTION Terahertz radiation has recently gained attention for its usefulness in nondestructive imaging [1]. Terahertz radiation is used to see through nonmetallic objects such as plastic, dry paper, and cloth. [2, 3, 4]. The radiation s unique properties and low photon energy make terahertz imaging a promising alternative to current technologies in security, quality control, and medical diagnostics. However, the long wavelength severely limits the obtainable resolution of traditional diffraction limited terahertz imaging systems [5, 6]. In the case of imaging thin objects in transmission geometries, studies have shown that near-field microscopy can be used to improve the obtainable diffraction limited spatial resolution of terahertz imaging to subwavelength resolution [5]. Terahertz subwavelength imaging was first demonstrated in 1998 when a subwavelength spatial resolution of λ/4 using a terahertz time-domain system and a conical aperture was achieved [7]. Reference 8 discussed that a spatial resolution of λ/85 with the use of a complex near-field probe and a terahertz time-domain system was achieved in 2001. Unlike diffraction limited systems which can at best resolve objects on the size of a few wavelengths, near-field imaging resolution is mainly limited by the ability to machine subwavelength apertures that focus and transmit radiation in the form of an evanescent wave efficiently enough to be detected several wavelengths after it passes through the aperture [9]. Applying near-field techniques with terahertz radiation creates the potential for high-resolution, nondestructive imaging of transmissive objects that are several wavelengths thick. II. THEORY AND EXPERIMENT By using simple aperture fabrication techniques, the spatial terahertz output can be inexpensively modified from a continuous wave terahertz source to obtain images with subwavelength resolution. In order to quantify the resolution improvements over conventional transmission imaging techniques, compare diffraction-limited and near-field terahertz imaging of a standard 1951 United States Air Force (USAF) resolution target at a terahertz output frequency of 0.210 terahertz. The resolution limit of diffraction-limited imaging systems is given by the well-known Rayleigh criterion [10]: RR = 1 1.22 λλ ff/# (1) where, R is the resolution, λ is the wavelength, and f/# is the object space f-number of the optical system. For this report, radiation at 0.210 terahertz was used, corresponding to a wavelength of 1.40 millimeters. The optical system can be characterized by f/# = 1, meaning that the diffraction-limited Airy disk radius and resolution are 1.71 millimeters and 0.59 millimeters minus 1, respectively. The terahertz source is a solid-state amplifier multiplier chain, which outputs about 2 milliwatts at 0.210 terahertz with a line width on the order or hertz. Its diagonal output horn diameter is approximately 6 millimeters. Figure 1 shows the setup of the diffraction limited system. The terahertz beam is focused onto the USAF resolution target, which is rasterscanned through the focused spot. The detector is located a few millimeters behind the target. 1

Figure 1. Diffraction Limited Terahertz Imaging Setup Image resolution can be greatly improved by the use of near-field imaging. The Rayleigh criterion does not apply, and objects separated by less than the system s Airy disk can be distinguished. The system resolution is instead limited by the size of the aperture where radiation is emitted as well as the aperture to object plane separation. The high resolution spot expands approximately as 2π steradians immediately after passing through the aperture. Therefore, in order to be able to take advantage of the high resolution due to the aperture, the sample has to be thin and placed directly in front of the aperture. For this report, a circular aperture was fabricated with an output diameter of 0.3 millimeters, which was placed in contact with the resolution target. This aperture is an inexpensive, easily reproducible near-field imaging aperture alternative to complex near-field apertures requiring intricate fabrication techniques. The near-field aperture is a conical horn that was rolled up from a sheet of standard aluminum foil. The diameter of the base is approximately 12 millimeters. This allows the conical horn to be directly attached to the source output horn previously described. Figure 2 shows the aperture specifications, and Figure 3 shows the nearfield imaging setup. Figure 2. Near-Field Aperture Horn 2

A 1951 USAF resolution target was imaged using both diffraction-limited and near-field terahertz transmission imaging. The target is a 3-by-3 inch glass plate with a thin coating of chrome. The chrome-coated plate is opaque at 0.210 terahertz, and shows different size line pairs that were edged out of the chrome layer. These line pairs correspond to a variety of spatial resolutions. Figure 4 shows a picture of the 1951 USAF resolution target. Figure 3. Near-Field Imaging System Figure 4. 1951 USAF Resolution Target 3

III. RESULTS The system resolution is determined by observing the smallest well-defined set of line pairs. It is important to note that the chrome layer is orders of magnitude thinner than the terahertz wavelength. Furthermore, the tip of the near-field aperture is in contact with the chrome layer. Therefore, assume that the measured resolution is a best-case scenario and that it represents the maximum achievable resolution for the given aperture. For both the diffraction-limited and near-field tests, radiation was maintained at a frequency of 0.210 terahertz. An XY scanning stage was used to raster scan the resolution target laterally across the beam focus or the tip of the aperture. First, the resolution target was imaged using the diffraction-limited transmission imaging system, as shown in Figure 1. The resulting image is shown in Figure 5. The smallest line set that could be resolved with conventionally focused terahertz radiation at 0.210 terahertz was Element 1 of Group 2. The line set is located inside of the white circle in Figure 5. This line set represents a resolution of 0.250 line pairs/millimeters and corresponds to a resolution of 1 line pair in 4 millimeters, or 1 line in 2 millimeters. Therefore, this imaging setup could, at best, resolve a 2-millimeter object. These experimental data match the previously calculated resolution (Airy disk radius) well. For the near-field imaging experiment, the conical aperture with a circular tip of 0.3 millimeters in diameter was attached to a 0.200- to 0.300-terahertz conical source output horn. The 1951 USAF resolution target was then imaged using the setup shown in Figure 3. Figure 6 shows the terahertz image of the same 1951 USAF resolution target when acquired in the near-field setup. Figure 5. Diffraction Limited Image 4

Figure 6. Near-Field Image at 0.210 Terahertz The smallest line set resolved with near-field imaging was Element 3 of Group 1 and represents a resolution of 2.52 line pairs/millimeters. This corresponds to a resolution of 5 lines/millimeters or a 0.2-millimeter object. The improved resolution is evidenced by the terahertz image in Figure 6. For this report, a resolution of λ/7 was achieved, compared to diffraction-limited ratio of λ/0.8. It is interesting to note that the vertical line pairs are better resolved than the horizontal line pairs. This can be explained by a slightly elliptical aperture tip, with is major axis in the horizontal direction and minor axis in the vertical direction. This departure from a perfect circular aperture tip is only apparent for structures that are just resolved. Figure 7 shows three cross sections of the resolution target imaged in the near-field setup. Figure 7. Cross Sections of Near Field Image 5

The locations of each cross section are indicated in Figure 8. The arrow in Figure 7 identifies Element 3 of Group 1. The three peaks show that the three lines are just resolved. The next smaller pair (Element 4 of Group 1) immediately to the right is no longer resolved. Figure 8. Near-Field Image Showing Locations of Cross Sections in Figure 7 IV. CONCLUSION Our preliminary test has shown the effectiveness of an easily fabricated aluminum foil aperture in obtaining terahertz images with subwavelength resolution. A resolution of λ/7 was obtained for a near-field scan at 0.210 terahertz. The method eliminates the need for complex and laborious fabrication techniques while maintaining comparable high resolution quality. 6

REFERENCES 1. Kawase, K. et al., Non-Destructive Terahertz Imaging of Illicit Drugs Using Spectral Fingerprints Optics Express, Volume 11, pp. 2,549-2,553, 2003. 2. Mittleman, D. M.; Jacobsen, R. H.; and Nuss, M. C., T-Ray Imaging, Institute of Electrical and Electronics Engineers (IEEE) Journal of Quantum Electron, Volume 2, pp. 679-692, 1996. 3. Thrane, L. et al., THz Reflection Spectroscopy of Liquid Water, Chemical Physics Letters, Volume 240, pp. 330-333, 1995. 4. Kindt, J. T. and Schmuttenmaer, C. A., Far-Infrared Dielectric Properties of Polar Liquids Probed by Femtosecond Terahertz Pulse Spectroscopy, Journal of Physical Chemistry, Volume 200, pp. 10,373-10,379, 1996. 5. Lecaque, R. et al., THz Near-Field Optical Imaging by a Local Source, Optics Communication, Volume 262, pp. 125-128, 2006. 6. Adam, A. J. L. et al., THz Near-Field Measurements of Metal Structures, Comptes Rendus Physique, Volume 9, pp. 161-168, 2006. 7. Hunsche, S. et al., Thz near-field imaging Optical Communications, Volume 150, pp. 22-26, 1998. 8. Mitrofanov, O. et al., Collection-Mode Near-Field Imaging With 0.5-THz Pulses, Institute of Electrical and Electronics Engineers (IEEE) Journal of Selected Topics in Quantum Electronics, Volume 7, pp. 600-607, 2001. 9. Betzig, E. et al., Near-Field Scanning Optical Microscopy (NSOM), Biophysical Journal, Volume 49, pp. 269-279, 1986. 10. Geary, J., Introduction to Lens Design, Center for Applied Optics, Willmann-Bell, Inc., Richmond, Virginia, 2002. 7

LIST OF ABBREVIATIONS, ACRONYMS, AND SYMBOLS mm THz USAF millimeter terahertz United States Air Force 8

INITIAL DISTRIBUTION LIST Copies Defense Systems Information Ms. Jessica Owens Electronic Analysis Center jessica.owens@dsiac.org SURVICE Engineering Company 4695 Millennium Drive Belcamp, MD 21017 Defense Technical Information Center Mr. Jack L. Rike Electronic 8725 John J. Kingman Rd., Suite 0944 jackie.l.rike.civ@dtic.mil Fort Belvoir, VA 22060-6218 AMSAM-L Ms. Anne C. Lanteigne Electronic hay.k.lanteigne.civ@mail.mil Mr. Michael K. Gray Electronic michael.k.gray7.civ@mail.mil RDMR RDMR-CSI Electronic Electronic RDMR-WDI Mr. Wayne E. Davenport Electronic wayne.e.davenport2.civ@mail.mil Dr. Henry O. Everitt Electronic henry.o.everitt.civ@mail.mil Dr. Michael S. Richman Electronic michael.s.richman.civ@mail.cil RDMR-WDI-WSD Mr. Martin S. Heimbeck Electronic/Hardcopy martin.s.heimbeck.civ@mail.mil Dist-1/Dist-2 (Blank)