University of Groningen. Fundamental limitations of THz and Niobiumnitride SIS mixers Dieleman, Pieter

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University of Groningen Fundamental limitations of THz and Niobiumnitride SIS mixers Dieleman, Pieter IMPORTANT NOTE: You are advised to consult the publisher's version (publisher's PDF) if you wish to cite from it. Please check the document version below. Document Version Publisher's PDF, also known as Version of record Publication date: 1998 Link to publication in University of Groningen/UMCG research database Citation for published version (APA): Dieleman, P. (1998). Fundamental limitations of THz and Niobiumnitride SIS mixers Groningen: University of Groningen Copyright Other than for strictly personal use, it is not permitted to download or to forward/distribute the text or part of it without the consent of the author(s) and/or copyright holder(s), unless the work is under an open content license (like Creative Commons). Take-down policy If you believe that this document breaches copyright please contact us providing details, and we will remove access to the work immediately and investigate your claim. Downloaded from the University of Groningen/UMCG research database (Pure): http://www.rug.nl/research/portal. For technical reasons the number of authors shown on this cover page is limited to 10 maximum. Download date: 02-01-2019

Fundamental Limitations of THz Niobium and Niobiumnitride SIS Mixers Pieter Dieleman

The cover picture is taken the morning after the 1953 flood disaster in the province of Zeeland, the Netherlands. Clearly visible are the holes in the sea dike through which the water flows with great force. Apart from the devastating effects, the apparent huge stream of water through these holes provides an expressive analoge to the effects of pinholes in tunnel barriers as described in this thesis. (Copied with permisson from De watersnood in Zeeuws-Vlaanderen, by G. Sponslee and E. Steyns, van Geyt productions, Hulst, the Netherlands). The reading committee for this thesis consists of Prof.Dr.Ir. J.E. Mooij, Prof.Dr. M.J. Feldman, and Prof.Dr. K.H. Gundlach. This thesis is typeset in Times Roman with L A TEX. This work was performed at the Department of Applied Physics of the University of Groningen and the Space Research Organization of the Netherlands (SRON) as part of the research program of the Stichting voor de Technische Wetenschappen (STW), with financial support from the Nederlandse Organisatie voor Wetenschappelijk Onderzoek. This work is also supported by the European Space Agency (ESA) under contract no: 7898/88/NL/PB(SC) and 11653/95/NL/PB.

Rijksuniversiteit Groningen Fundamental Limitations of THz Niobium and Niobiumnitride SIS Mixers Proefschrift ter verkrijging van het doctoraat in de Wiskunde en Natuurwetenschappen aan de Rijksuniversiteit Groningen op gezag van de Rector Magnificus Dr. F. van der Woude in het openbaar te verdedigen op vrijdag 24 april 1998 des namiddags te 1.15 uur. door Pieter Dieleman geboren op 24 mei 1970 te Kommerzijl.

Promotor: Prof. Dr. Ir. T.M. Klapwijk Referent: Dr. M.W.M. de Graauw

Preface This thesis describes the use of superconducting niobium and niobiumnitride tunnel junctions as heterodyne mixing elements in the submillimeter frequency range from 600 to 1000 GHz. In this frequency range Nb as well as NbN layers exhibit significant absorption of submillimeter radiation, making them unsuitable as impedance matching embedding structures. This brings about the inclusion of normal metals in the design of these detectors. The frequency range obtainable with these hybrid detectors as well as the attainable ultimate sensitivity are the main topics of this thesis. Ch. 1 is an introduction to the work presented in the thesis, and describes the historical development and the basic principles of operation of heterodyne receivers based on superconducting tunnel junctions. The fabrication, materials properties and their effect on the electrical characteristics of Nb and NbN tunnel junctions are discussed in Ch. 2 as well as the fabrication related RF radiation losses in superconductors and normal metals. The operation of the receiver as a whole and the junction in particular will be illustrated in Ch. 3 by means of a case study of a Nb junction with aluminum circuitry. Measured data are compared in detail with the quantum theory of mixing. An interesting observation when employing aluminum embedding is an improved transport of the heat generated by Joule heating of the device when operated as a detector. The cooling efficiency of aluminum vs. niobium embedding of the junction is investigated in Ch. 4. Using the simulation developed in Ch. 3 the effect of this enhanced heat transport is on the mixing properties is investigated. Ch. 5 deals with the feasibility of NbN junctions in the frequency range of 600 to 1000 GHz, in which an analysis method is employed similar to that in Ch. 3. The NbN junctions exhibit a significantly enhanced shot noise which dominates the performance of the device. The physical mechanism behind this is described in Ch. 6. The same noise enhancement mechanism is found to be present in high v

vi critical current density Nb junctions as well. This observation, described in Ch. 7 answers a long-standing question on the discrepancy between the noise measured and theoretically expected. Appendix A discusses the lay-out of the used waveguide mixers and the experimental methods used to determine the physical properties of the devices. A summary of the work performed and the implications of the results for the feasibility of superconducting tunnel junctions in the THz regime is given in Ch. 8. The thesis ends with a summary both in English and Dutch.

Contents 1 Submm radiation detection 1 1.1 Understandingtheuniverse... 1 1.2 Atmosphericresearch... 2 1.3 RadiationdetectionatTHzfrequencies... 3 1.3.1 Detectorrequirements... 3 1.3.2 Couplingofradiationtothedetector... 4 1.3.3 Submmradiationdetectionmodes... 6 1.4 Heterodyne detectors.... 9 1.4.1 Schottky-barrierdiode... 9 1.4.2 SISjunctions... 9 1.4.3 HEBjunctions... 10 1.5 SIS heterodyne detectors...... 11 1.6 FrequencyrangeofSISoperation... 13 1.6.1 Tuningcircuitcharacteristics... 13 1.6.2 Junctionfrequencyrangelimitations... 14 1.7 Conclusions... 15 2 Materials aspects and SIS characteristics 17 2.1 FabricationofSISmixerstructures... 17 2.1.1 Nb tunnel junction fabrication... 19 2.1.2 NbN tunnel junction fabrication......... 20 2.2 I-V characteristics vs. barrier structure... 27 2.2.1 Aluminumoxidegrowth... 27 2.2.2 Dependence of electrical properties on J c... 28 2.2.3 Current transport in pinholes.... 33 2.3 InfluenceofMARonTHzradiationmixing... 36 2.3.1 EffectofmicrowaveradiationonMAR... 36 vii

viii Contents 2.3.2 Radiation modifies MAR modifies mixing properties... 37 2.4 Integratedtuningstructures... 38 2.4.1 Transmissionlineoperation... 38 2.4.2 Low-lossradiationcoupling... 41 2.5 Surface resistance of metals and superconductors.... 42 2.5.1 Nbsurfaceimpedance... 44 2.5.2 Alsurfaceimpedance... 44 2.5.3 NbNsurfaceimpedance... 45 2.6 Conclusions... 46 3 Performance analysis of Nb junctions at 800 1000 GHz 51 3.1 Introduction......... 51 3.2 Receiver configuration... 52 3.3 Heterodyne measurements..... 53 3.4 Receiver noise analysis... 55 3.4.1 RF components... 56 3.4.2 Mixercharacteristics... 56 3.5 Discussionandconclusions... 58 4 DC heating in SIS junctions 63 4.1 Introduction......... 63 4.2 Junction layout....... 64 4.3 Heatflow... 64 4.4 Heatrelaxationmechanisms... 65 4.5 Thermalhealinglength... 66 4.6 Influenceonmixerperformance... 68 4.7 Conclusions... 69 5 Performance limitations of NbN SIS junctions 71 5.1 Introduction......... 72 5.2 Junctioncharacteristicsandmeasurementsetup... 72 5.3 Shotnoisemeasurementsandmodeling... 73 5.4 Receiver noise measurements.... 77 5.5 Conclusions... 79

Contents ix 6 Observation of Andreev reflection enhanced shot noise 83 6.1 Introduction......... 84 6.2 Sample layout and characteristics...... 85 6.3 Shotnoisemeasurement... 85 6.4 ShotnoiseinNbNjunctions... 87 6.5 Chargeclustercalculation... 88 6.6 Conclusions... 91 7 Shot noise beyond the Tucker theory in niobium tunnel junction mixers. 95 7.1 Introduction......... 95 7.2 Junctioncharacteristics... 96 7.3 Measurementsetup... 97 7.4 Noisemeasurements... 99 7.5 Shotnoisecalculation... 99 7.6 Implicationsforthenoisetemperature... 99 7.7 Effects on the receiver characteristics....101 7.8 Conclusions...101 8 Summary and discussion 105 8.1 Integratedtuningstructures...105 8.2 Nbjunctionresults...106 8.3 NbNjunctionresults...107 8.4 FuturedevelopmentofTHzdetectors...108 A Performing heterodyne measurements 111 A.1 Junctionperformancetesting...111 A.2 Receiver layout.......113 Samenvatting 115 Dankwoord 121 List of publications 123

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