INGEDE Project PMV Entrance Quality Control of Recovered Paper Regarding Deinkability of Printed Products by FT-IR Spectroscopy
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1 INGEDE Project PMV Entrance Quality Control of Recovered Paper Regarding Deinkability of Printed Products by FT-IR Spectroscopy Project Leader: Dr.-Ing. Hans-Joachim Putz Dipl.-Chem. Antje Kersten 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 1 Content 1. Background 2. Status of Knowledge 3. Approach 4. Results IR Spectra - different fibres - newspapers - magazines - printed papers with and without varnish - printed packaging products with and without varnish 5. Summary 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 2
2 1. Background The quality of the paper products in paper mills with deinking stages is often influenced by some paper for recycling material with insufficient ink removal. These problems often originate from small amounts of papers with defined printing processes or special varnished products in the paper for recycling delivery. Simple and fast analytical technique for identification of difficult to deink print products is necessary. 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 3 2. Status of Knowledge - NIR measurement technique is used industrially since several years, for example in sorting of recyclable material as plastic or paper for recycling. - Successful application of the online NIR technology for continuous control of the composition of paper for recycling on the belt conveyor to a pulping unit has been published. - The idea is to detect and to control for example the input of varnished print products in a stock preparation line. With the obtained information the stock preparation process should be adapted to the conditions of the paper for recycling input. 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 4
3 Electromagnetic Spectrum Source: Bruker Optik Grundlagen der FT IR Spektrometrie 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 5 Comparison IR-NIR Spectroscopy Infrared IR Near Infrared NIR (Middle Infrared MIR) Kind of vibrations Fundamental vibrations Harmonics, Combination vibrations Origin of signals All functionalities Hydrogen functionalities Use for structural investigations Very good Poor Evaluation of spectra Directly evaluable Due to low peak intensity not directly evaluable; application of chemometric and other statistic algorithm necessary Quantitative analysis Very good Very good Absorptivity High Low Necessary sample thickness / Penetration depth Very thin (max. 100 µm); due to lower energy Signal-to-noise ratio < > Source: Siesle, H. W.; Ozaki, Y.; Kawasata, S.; Heise, H. M.: Near Infrared Spectroscopy, Wiley VCH Verlag, Weinheim, 2002 High (up tp several mm); due to higher energy 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 6
4 IR Spectrum of n-hexane 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 7 Source: Bruker Optik Grundlagen der FT IR Spektrometrie IR Spectrum of Acetone 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 8 Source: Bruker Optik Grundlagen der FT IR Spektrometrie
5 Identification of Unknown Substances 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 9 Source: Bruker Optik Grundlagen der FT IR Spektrometrie IR Frequences Assignment Table 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 10 Source: Bruker Optik Grundlagen der FT IR Spektrometrie
6 Identification of Unknown Substances 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 11 Source: Bruker Optik Grundlagen der FT IR Spektrometrie 3. Approach - Collection of results from spectroscopic FT-IR analysis of print products as well as of deinkability tests of the same samples in a data base. - By linking the FT-IR analysis with the deinking results the data base will be built up in a way that unknown print products can be allocated to not, poor or good deinkable print products. - In an ideal case also the problems in terms of dirt specks, discolouration or luminosity losses should be predictable from an unknown print product. 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 12
7 (M)IR-ATR-Measuring Device Platinum-ATR-Measuring device with ATR-Diamond-Module Manufacturer: Bruker Optik GmbH, Ettlingen, Germany 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 13 Figure: Bruker Optik Grundlagen der FT IR Spektrometrie 4. Results Repeatability (Chemical Pulp) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 14
8 Flexo Printed Newspapers in Comparison to Offset Printed Newspapers Flexo Daily Mail Flexo la Republica Flexo La Stampa Flexo (Sample K & N) Offset Neue Zürcher Zeitung 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 15 Results Newspaper Handelsblatt (Digitally Printed with UV Different Colours) CaCO3 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 16
9 Offset Printed Samples (Full Surface Printed, 2 differ. Print Densities) Back sides (2 samples) - unprinted Front side offset printed (cyan) high load Front side offset printed (cyan) high load 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 17 Offset Printed Samples (Full Surface Printed, Usual Print Density) black cyan magenta yellow 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 18
10 Sample Solid InkJet (Schmelzfarben InkJet) PE 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 19 Cosmopolitan with and without Printing and UV Varnish Unprinted, without varnish CaCO3 Printed, without varnish Printed, with UV varnish Acrylat 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 20
11 Wohnträume with and without Printing and UV Varnish Unprinted, without varnish CaCO 3 Printed, with UV varnish Acrylate 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 21 Results KCTL 100 g Sheet Fed Offset with Varnish Back side (unprinted) Front side (printed and varnished) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 22
12 Results KCTL 100 g Flexo Printed with Varnish Front side (flexo printed, different colours, without varnish) Back side (unprinted) Back side (unprinted, without varnish) Front side (printed Flexo printed with varnish and varnished) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 23 Results KCTL 100 g Flexo Printed with Varnish: Spectra Search 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 24
13 CEWE Photo Book PE 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 25 Cardboard Samples with UV Offset Print and/or UV Varnish (Fa. Weig) GD 2 with gloss varnish GC2 Cardboard GC 2 with gloss varnish 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 26
14 Packaging Printing with Varnishes; Sample Asiabox (1) PET 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 27 Packaging Printing with Varnishes; Sample Asiabox (2) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 28
15 Packaging Printing (UV printing with UV varnish); Sample Kaffeefilter (1) Acrylate 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 29 Packaging Printing (UV printing with UV varnish); Sample Kaffeefilter (2) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 30
16 Packaging Printing; Sample Broccoli Inner side Frozen PMV 4 PE 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 31 Library Information table 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 32
17 5. Summary Several printed products can be identified by using IR technology: Some kind of digitally printed products, all kind of paper products with a film forming printing ink Almost all varnished printed products can be identified: Polyethylene (PE), polyethylene terephthalates (PET), Polyacrylates Role of CaCO 3 signal Not detectable: Offset printed newspaper, flexo printed newspaper and all other paper products manufactured by printing processes where ink dries by absorption into the paper Database has to be completed (Information about printing product, IR spectra, deinking results) 24 February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten February 2016 Chair of Paper Science and Mechanical Process Engineering Antje Kersten 34
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