PROCESS ECONOMICS PROGRAM

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1 PROCESS ECONOMICS PROGRAM SRI INTERNATIONAL Abstract Process Economics Program Report No. 83A Menlo Park, California ADHESIVES (January 1986) This report reviews the technology and summarizes relevant patents relating to anaerobic, cyanoacrylate, epoxy, urethane, pressure sensitive, hot melt (including pressure sensitive hot melt and foamed hot melt), and reactive and aerobic acrylic adhesives. The process economics for the production of selected hot melt adhesives and reactive and aerobic acrylic adhesives are estimated. Summaries of patents on adhesive tapes, automotive adhesives, building and related adhesives, electronic and electroconductive adhesives, laminating adhesives, metal adhesives, radiation curable adhesives, and water-based adhesives are included. PEP'84 WSF

2 Report No. 83A ADHESIVES SUPPLEMENT A by WING SIEN FONG January 1988 A private report by the PROCESS ECONOMICS PROGRAM Menlo Park, California 94025

3 For detailed marketing data and information, the reader is referred to one of the SRI programs specializing in marketing research. The CHEMICAL ECONOMICS HANDBOOK Program covers most major chemicals and chemical products produced in the United States and the WORLD PETROCHEMICALS Program covers major hydrocarbons and their derivatives on a worldwide basis. In addition, the SRI DIRECTORY OF CHEMICAL PRODUCERS services provide detailed lists of chemical producers by company, product, and plant for the United States and Western Europe. ii

4 CONTENTS INTRODUCTION SUMMARY Technical Aspects... 4 Economics... 8 INDUSTRY STATUS ANAEROBIC ADHESIVES Chemistry Formulations Properties Uses CYANOACRYLATE ADHESIVES Chemistry Production of the 33 Formulations Properties Uses EPOXY RESIN ADHESIVES Chemistry Formulations Properties and Uses URETHANE ADHESIVES Chemistry Formulations Preparation Uses PRESSURE SENSITIVE ADHESIVES... Formulations.. Rubber Based... Acrylics... Silicones... Others... Radiation Curable Pressure Sensitive Adhesives : 77 iii

5 CONTENTS 9 HOTMELTADHESIVES... Hot Melt Adhesive Formulations... Base Polymers... Tackifiers... Waxes... Plasticizers... Antioxidants... Fillers... Hot Melt Adhesive Processes... Salient Features of Hot Melt kek;ei Pressure Sensitive Hot Melt Adhesives Fo&u;a;& Foamed Hot Melt Adhesives... Hot Melt Adhesives by a Continuous Extrusion Process Process Description... Process Discussion... Cost Estimates... Hot Melt Adhesives by a Eatch Process (Kneader-Extruder and a Kettle)... Process Description... Process Discussion... Cost Estimates : REACTIVE AND "AEROBIC" ACRYLIC ADHESIVES Formulations Application Method Advantages and Limitations Process Description Process Discussion Cost Estimates APPENDIX A DESIGN AND COST BASIS APPENDIX B SOME OF THE PERFORMANCE TESTS FOR ADHESIVES PATENTSUMMARYTABLES SUPPLEMENTARY PATENT SUMMARY TABLES CITED REFERENCES PATENTREFERENCES iv

6 ILLUSTRATIONS 9.1 Hot Melt Adhesives by a Continuous Extrusion Process Flowsheet EVA-Based Hot Melt Adhesives by a Continuous Extrusion Process Hot Melt Adhesives by a Batch Process Flowsheet Reactive and "Aerobic" Acrylic Adhesives Production V

7 TABLES Process Economics for Hot Melt Adhesives, and Reactive and "Aerobic" Acrylic Adhesives Estimated Adhesives Markets in the United States and Western Europe for The Hot Melt Adhesives Market in Great Britain The 1982 Adhesives Consumption and Adhesives and Sealant Markets in the United States The 1983 Hot Melt Adhesives Market in the United States The 1983 Structural and Specialty Adhesives and Sealants Markets in the United States Predicted Growths for Some Adhesives in the United States The Percentages of Water-Based, Hot Melt, and Solvent-Based Adhesives Used in Packaging, Nonrigid Bonding, and Tapes in 1983 in the United States Estimated Production and Demand of Adhesives in Japan Anaerobic Adhesives Patent Summary Cyanoacrylate Adhesives Patent Summary Physical Properties of Alkyl Cyanoacrylates Physical Properties of Some Commercial Cyanoacrylate Adhesives Bond Strength of Cyanoacrylate Adhesives Epoxy Resin Adhesives Patent Summary Effect of Temperature on the Tensile Shear Strength on an Epoxy Resin Adhesive Bond Formed with Various Hardeners vii

8 TABLES 7.1 Urethane Adhesives Patent Summary Pressure Sensitive Adhesives Patent Summary Performance Properties of Rubber-Based, Acrylic-Based, and Silicone-Based Pressure Sensitive Adhesives Typical Properties and Uses of Silicone Pressure Sensitive Adhesives Hot Melt Adhesives Based on Copolymers of Ethylene and Vinyl Acetate, Polyamides, Polyesters, Polyolefins, Rubbers, and Other Materials Patent Summary Hot Melt Pressure Sensitive Adhesives Patent Summary Hot Melt Adhesives Raw Material Flow Rates Hot Melt Adhesives by a Continuous Extrusion Process MajorEquipment Hot Melt Adhesives by a Continuous Extrusion Process Utilities Summary Hot Melt Adhesives by a Continuous Extrusion Process Total Capital Investment Production of a Hot Melt Adhesive Based on an EVA Copolymer by a Continuous Extrusion Process Production Costs Production of a Hot Melt Adhesive Based on a Mixture of Two EVA Copolymers by a Continuous Extrusion Process Production Costs Production of a Hot Melt Adhesive Based on a LDPE by a Continuous Extrusion Process Production Costs Production of a Hot Melt Adhesive Based on a Styrene Block Copolymer by a Continuous Extrusion Process Production Costs Viii

9 TABLES 9.11 Hot Melt Adhesives by a Batch Process (KneaderExtruder and Kettle) Formulation and Cycle Time Hot Melt Adhesives by a Batch Process Major Equipment Hot Melt Adhesives by a Batch Process Utilities Summary Hot Melt Adhesives by a Batch Process Total Capital Investment Combined Production of Two EVA Based Hot Melt Adhesives by a Batch Process Production Costs Hot Melt Adhesives by a Batch Process Production Costs for the Individual Products in the Product Mix Combined Production of a Styrene Block Copolymer Based and an EVA Based Hot Melt Adhesive by a Batch Process Production Costs Reactive and "Aerobic" Acrylic Adhesives Patent Summary Formulation and Cycle Time for a Reactive Acrylic Adhesive Reactive and "Aerobic" Acrylic Adhesives Production Major Equipment Reactive and "Aerobic" Acrylic Adhesives Production Utilities Summary Reactive and "Aerobic" Acrylic Adhesives Production Total Capital Investment Production of a Reactive Acrylic Adhesive Production Costs ix

10 TABLES 10.7 Production of a Heat Resistant Reactive Acrylic Adhesive Production Costs s Production of an "Aerobic" Acrylic Adhesive Production Costs s.l Adhesive Tapes Summary of Some Recent Patents s.2 Automotive Adhesives Summary of Some Recent Patents s.3 Building and Related Adhesives Summary of Some Recent Patents s.4 Electronic and Electroconductive Adhesives Summary of Some Recent Patents s.5 Laminating Adhesives Summary of Some Recent Patents S.6 Metal Adhesives Summary of Some Recent Patents s.7 Radiation Curable Adhesives Summary of Some Recent Patents S.8 Water-Based Adhesives Summary of Some Recent Patents

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