TA Instruments RSA-G2 Dynamic Mechanical Analyzer

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1 The new RSA-G2 is the most advanced platform for mechanical analysis of solids from the world s leading supplier of DMA instrumentation. This new highperformance instrument represents the fourth generation of dual head mechanical analyzers, featuring a new force convection oven for precise and accurate temperature control, extensive array of geometries to accommodate the widest range of sample shapes and stiffness and immersion testing capability. In addition, the RSA-G2 doubles as a Dielectric Analyzer, DEA, for stand-alone or simultaneous measurements. The separate motor and transducer technology of the RSA-G2 insures the purest mechanical data through independent control of deformation and measurement of the stress. Unrivaled accuracy, flexibility, and ease-of-use are realized through improved specification, a new environmental system, expanded test modes, and new intuitive TRIOS Software. RSA-G2 Specifications N (High-range)) Minimum Force N(Low-range) 35 N (High-range) Maximum Force 3.5N (Low range) Force Resolution N Dynamic Displacement Range ± to ± 1.5 mm Displacement Resolution 1 Nanometer Modulus Range 10 3 to 3 x Modulus Precision ± 1% Tan delta Sensitivity Tan delta Resolution Frequency Range 2 x 10-5 to 100 Hz Temperature Control Force Convection Oven Temperature Range -150 to 600 C* Heating Rate 0.1 to 60 C/min. Cooing Rate 0.1 to 60 C/min. Isothermal Stability ± 0.1 C *Note: Standard sample clamps are for use to a maximum temperature of 500 C. Optional tooling are required for testing to 600 C.

2 RSA-G2 Sample Clamps The RSA-G2 features a variety of sample clamps that provide multiple modes of deformation to accommodate a wide range of sample stiffness. The RSA-G2 can easily characterize, films, fibers, soft foams, thermoplastic or thermoset bar samples, high modulus composites, metals, and even medium to high viscosity polymer melts in shear sandwich. All sample clamps are constructed from 17-4 PH steel for maximum rigidity. The RSA-G2 also features the popular Immersion System for testing solid materials immersed in liquids to a maximum temperature of 150 C. Standard Clamping systems for use in Forced Convection Oven to 500 C *Note: Standard sample clamps are for use to a maximum temperature of 500 C. Optional stainless steel sample clamps required for testing to 600 C are available upon request. Immersion System; includes tension, compression and three point bending

3 RSA-G2 New Features and Options TA Instruments RSA-G2 Dynamic Mechanical Analyzer Forced Convection Oven (FCO) Environmental Control The FCO is an air/n2 gas convection oven designed for optimum temperature stability, extremely rapid heating and cooling, and ease of use over the temperature range of -150 to 600 C. The maximum controlled heating rate is 60 C/min. Obtaining the -150 C minimum temperature requires an optional liquid nitrogencooling device. The FCO provides superior temperature stability through the use of twin element heaters, which produce counter rotating airflow into the oven chamber. The FCO can be mounted on either side of the test station, and comes standard with long life internal LED lamp and window viewing port. The FCO can be fitted with an optional cameral viewer option for capturing real time images during experiments. Touch screen and Keypad A color touch screen user interface mounted on the front of the test station. This graphical interface adds a new dimension in ease-of-use. Interactive activities such as geometry zeroing, sample loading, and setting temperature can be performed at the test station. Important instrument status and test information, such as temperature, gap, force and motor position are displayed. The touch-screen also provides easy access to instrument settings and diagnostic reporting. New Electronics Separated from Test Station The RSA-G2 is equipped with new high-sped electronics with digital signal processing for transducer measurements and motor s control. The test station is isolated from electronics box which houses the main power supply and any electronics cooling fans. While many manufactures try to cut costs by fully integrating the test station and electronics into a single box, the separate electronics approach by TA Instruments isolates the precision measurements from heat and vibration, and ensures the best sensitivity and data quality from the test station.

4 Other Unique Features of the RSA-G2 TA Instruments RSA-G2 Dynamic Mechanical Analyzer Fully Integrated ultra-high Speed Data Acquisition Fully integrated high speed data acquisition for transient (up to 8000Hz) and oscillation (up to 15000Hz) measurements. Such high speed data sampling provides superior resolution of magnitude and phase of the measured signals, and allows much better higher harmonic resolution for automatic analysis during the oscillation test or post Fourier transformation analysis after the oscillation test. Higher Harmonics and Fourier Transformation Rheology Thanks to the ultra-high speed data acquisition, the purest applied deformation and the minimum inertia effect in the measured force, RSA-G2 provides the most accurate higher harmonic analysis up to 9th not only harmonic intensity ratio but also its corresponding phase. With optional Fourier Transformation Rheology software package, a wide range of non-linear Rheology parameter can be obtained like Fourier coefficients, Chebyshev coefficients, Minimum-strain and Large-strain modulus. Real-time Waveform Display and Image storage Waveform of oscillation can be displayed in real-time and saved with each data point for replay later. TTRIOS Software An important feature of RSA-G2 is the level of testing freedom and flexibility. Trios software is an integrated package for instrument control, test programming and data analysis. Superior Creep recovery Measurement New stress control algorithm of RSA-G2 provides a very high quality creep-recovery measurement without inertia effect which is unavoidable in other DMA designs. Flexible Axial Force Control New axial force control of RSA-G2 can be operated in both FRT (stiff) and Spring (soft) modes, that makes RSA-G2 can handle a wide range of materials with non-compromised high quality data.

5 New RSA-G2 Dielectric Thermal Analysis Option, DETA DETA, or Dielectric Thermal Analysis, is a material characterization technique similar to dynamic mechanical analysis except that an oscillating electrical field (AC field) is used as opposed to a mechanical force (stress) and the oscillating strain is a stored charge (Q) in the sample. The sample basically behaves like a capacitor. Q is measured as its derivative dq/dt = AC current. When the oscillating electric field is applied to a material, random dipoles in the material will orient with the field. DETA measures the degree to which the sample is storing a charge (capacitance) or passing the charge (conductance) through its bulk. The RSA-G2 DETA includes a special set of parallel plates which are connected directly to a dielectric bridge (LCR meter) which imposes a signal at a certain voltage and frequency/ies. It is a very powerful technique for characterizing polar materials such as PVC, PVDF, PMMA, and PVA. It is also very powerful for monitoring curing kinetics of materials such as epoxy and urethane systems. The wide range of frequencies available in DETA (20 Hz to 1 MHz and higher depending on the bridge) also extends the measurement range over traditional dynamic mechanical analysis (typically below 200 Hz). The combination of DETA with a high precision RSA-G2 DMA allows for the simultaneous collection of rheological and dielectric information. In addition, dielectric measurements can be run independently of rheological measurements and still benefit from the RSA-G2 test platform. This is because DETA measurements are conducted on a material sandwiched between parallel plates, with some normal force applied to ensure good surface contact, and surrounded an oven for temperature control. The permittivity, or dielectric constant, is measured by the ratio of capacitance with the sample in the plates to the capacitance with the same air gap. As temperature changes and expansion of the plates occurs, the gap changes and the accuracy of the permittivity suffer. The RSA-G2 FCO (forced convection oven) temperature control, axial force control with gap temperature compensation capability, and software for interface, all lead to more accurate DETA measurements. RSA -G2 DETA Specifications Attribute Geometry Temperature System Compatibility ARES to DE Bridge Interface Specification 25 mm PP FCO, Force Convection Oven IEEE Internal to Instrument Temperature Range -160 to 300 C Bridge Compatibility Agilent Models 4284A, 4285A, E4980A DE Frequency Range w/ Depends on Bridge Selection: See table DE Bridge Potential Depends on Bridge Selection: See table Agilent LCR Meter Model 4285A ARES-G2 and Bridge Compatibility Agilent LCR Meter Model 7980A

6 Dielectric Bridge (LCR Meter) Frequency AC Test Signal (potential) Agilent 4284A (Discontinued) 20 Hz to 1 MHz to 20 Volts Agilent 4285A 75 khz to 30 MHz to 10 Volts Agilent E4980A 20 Hz to 2 MHz to 20 Volts

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