FEVE Fluoropolymer Emulsions for Performance Improvement in Architectural Coatings
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1 FEVE Fluoropolymer Emulsions for Performance Improvement in Architectural Coatings Bob Parker, Applications Chemist SSCT Annual Meeting Sept. 26 Sept. 29, 2010
2 Outline Overview of FEVE resin technology Introduction of water-based FEVE emulsions Formulations using FEVE emulsions as blending resins: 1) Semi-Gloss House Paints a. White b. Dark Red 2) DTM Industrial Hi-Gloss Coatings a. White b. Black c. Dark Green d. Safety Yellow 1
3 FEVE Fluoropolymer Resins - FEVE is abbreviation for Fluoroethylene Vinyl Ether resins for coatings - Known for their high performance properties: 1) Exceptional resistance to UV degradation 2) Superior Chemical Resistance 3) Excellent Thermal Resistance - Known for their unique formulation properties: 1) Solvent soluble 2) Can be cured at ambient temperature with isocyanates 3) Can achieve high gloss formulations 2
4 Fluoroethylene Vinyl Ether (FEVE) Resins FLUORINATED SEGMENTS: Weatherability, durability, chemical resistance VINYL ETHER SEGMENTS: Gloss, solubility, crosslinking
5 Commercial Types of FEVE Resins: 1) Solvent soluble resins uses organic solvents for viscosity reduction; predominantly cured with isocyanates; available as resin solutions or as 100% solid resins 2) Water-based emulsions use vinyl ether macromonomers containing polyoxyethylene (EO) units to create stable emulsions 4
6 5 FEVE Water-borne Emulsions ************ FE-4300 FE-4500 Solids (Wt.) 50% 50% ph 7 to 9 7 to 9 Specific Gravity MFT 35 C. 28 C. Hydroxyl Value 10 13
7 6 White House Paint Formulation Properties Solids (Volume) 32% ph 9.0 to 9.5 TiO₂ Choice TiPure R-706 PVC 22 Thickeners both cellulosic and associative 60 Gloss Range VOC 150 g/liter
8 Testing procedure # 1 : 1) Blending of FEVE emulsions and 4 different acrylic emulsions to evaluate stability (3 weeks in 140 F. oven) 2) Manufacture of 3 White House Paint formulations for each acrylic emulsion: a. Binder = 100% Acrylic Emulsion b. Binder = 50% Acrylic Emulsion + 50% FE-4300 (FEVE Emulsion) c. Binder = 50% Acrylic Emulsion + 50% FE-4500 (FEVE Emulsion) 3) Stability testing of all formulations (6 weeks in 120 F. oven) 4) Preparation of test panels ( primed Al panels coated with 4 wet mils of coating) 5) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 7
9 8 Gloss Decrease - Acrylic #1 and 50/50 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 w/ FE /50 w/ FE-4500
10 9 Gloss Decrease - Acrylic #2 and 50/50 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 w/ FE /50 w/ FE-4500
11 10 Gloss Decrease -Acrylic #3 and 50/50 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 w/ FE /50 w/ FE-4500
12 11 Gloss Decrease - Acrylic #4 and 50/50 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 w/ FE /50 w/ FE-4500
13 12 Red House Paint Formulation Properties Solids (Volume) 36% ph 9.0 to 9.5 Pigment Choice Organic Red + Phthalo Blue (trace) PVC 6.5 Thickeners both cellulosic and associative 60 Gloss Range VOC 150 g/liter
14 Testing procedure # 2 : 1) Choose Acrylic Emulsion #3 as blending resin for Red HP formulation. 2) Manufacture of 6 Red House Paint formulations: a. Binder = 100% Acrylic Emulsion b. Binder = 50% Acrylic Emulsion + 50% FE-4500 (FEVE Emulsion) c. Binder = 60% Acrylic Emulsion + 40% FE-4500 (FEVE Emulsion) d. Binder = 70% Acrylic Emulsion + 30% FE-4500 (FEVE Emulsion) e. Binder = 80% Acrylic Emulsion + 20% FE-4500 (FEVE Emulsion) f. Binder = 90% Acrylic Emulsion + 10% FE-4500 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 4 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 13
15 14 Gloss Decrease of Acrylic #3 and FE-4500 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 10% FE % FE % FE-4500
16 15 Gloss Decrease of Acrylic #3 and FE-4500 Blends Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 40% FE % FE-4500
17 16 White DTM I/M Paint Formulation Properties Solids (Volume) 38% FEVE Emulsion FE-4300 ph 9.0 to 9.5 TiO₂ Choice TiPure R-706 PVC 18 Thickeners associative-type 60 Gloss Range VOC 100 g/liter
18 Testing procedure # 3 : 1) Choose 3 different acrylic emulsions from 2 manufacturers as blending resins for White DTM I/M Formulation. Blend these acrylic emulsions with the FE emulsions and run oven stability tests. 2) Manufacture of 2 White DTM I/M Paint formulations: a. Binder = 100% Acrylic Emulsion b. Binder = 50% Acrylic Emulsion + 50% FE-4300 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 4 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 17
19 18 Gloss Decrease of Acrylic #5 and FE-4300 Blend Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 BLEND w/ FE-4300
20 19 Gloss Decrease of Acrylic #6 & FE-4300 Blend Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 BLEND w/ FE-4300
21 20 Gloss Decrease of Acrylic # 7 and FE-4300 Blend Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 50/50 BLEND w/ FE-4300
22 21 Black DTM I/M Paint Formulation Properties Solids (Volume) 36% FEVE Emulsions FE-4300 and FE-4500 ph 9.0 to 9.5 Pigment Choice Tint-Ayd CW5331 Masstone Black PVC 2.7 Thickeners associative-type 60 Gloss Range VOC 100 g/liter
23 Testing procedure # 4 : 1) Choose Acrylic Emulsion # 5 and Acrylic Emulsion # 6 as blending resins for Black DTM I/M Formulation. 2) Manufacture of 3 Black DTM I/M Paint formulations for each Acrylic: a. Binder = 100% Acrylic Emulsion b. Binder = 50% Acrylic Emulsion + 50% FE-4300 (FEVE Emulsion) c. Binder = 50% Acrylic Emulsion + 50% FE-4500 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 8 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 22
24 100 Gloss Decrease of Acrylic #5 and 50/50 LUMIFLON Blends (BLACK FORMULA) 60 Gloss Decrease (%) ,000 Hours in QUV Weatherometer 100% Acrylic 50/50 w/ FE /50 w/ FE
25 Gloss Decrease of Acrylic #6 and 50/50 FEVE Blends (BLACK FORMULA) 60 Gloss Decrease (%) , % Acrylic 50/50 w/ FE /50 w/ FE-4500 Hours in QUV Weatherometer
26 Testing procedure # 5 : 1) Choose Acrylic Emulsion # 5 and Acrylic Emulsion # 6 as blending resins for Black DTM I/M Formulation. 2) Manufacture of 3 Black DTM I/M Paint formulations for each Acrylic: a. Binder = 100% Acrylic Emulsion b. Binder = 80% Acrylic Emulsion + 20% FE-4300 (FEVE Emulsion) c. Binder = 80% Acrylic Emulsion + 20% FE-4500 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 8 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 25
27 26 60 Gloss Decrease (%) Gloss Decrease of Acrylic #5 and FE-4300 Blends (DTM BLACK FORMULATION) Hours in QUV Weatherometer 100% Acrylic 20% FE-4300
28 27 Gloss Decrease of Acrylic #5 and FE-4500 Blends (DTM BLACK FORMULATION) Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic 20% FE-4500
29 28 Test Formulation: 100% Acrylic Emulsion #5 as total binder
30 29 Test Formulation: 80% Acrylic emulsion #5 and 20% FE-4300 FEVE Emulsion as total binder
31 30 Test Formulation: 80% Acrylic emulsion #5 and 20% FE-4300 FEVE Emulsion as total binder
32 31 Test Formulation: 80% Acrylic emulsion #5 and 20% FE-4500 FEVE Emulsion as total binder
33 32 Test Formulation: 80% Acrylic emulsion #5 and 20% FE-4500 FEVE Emulsion as total binder
34 60 Gloss Decrease (%) Gloss Decrease of Acrylic #6 and FE-4300 Blends (DTM BLACK FORMULATION) Hours in QUV Weatherometer 100% Acrylic 20% FE
35 34 Gloss Decrease of Acrylic #6 and FE-4500 Blends (DTM BLACK FORMULATION) 60 Gloss Decrease (%) Hours in QUV Weatherometer % Acrylic 20% FE-4500
36 35 Test Formulation: 100% Acrylic Emulsion #6 as total binder
37 36 Test Formulation: 80% Acrylic emulsion #6 and 20% FE-4300 FEVE Emulsion as total binder
38 37 Test Formulation: 80% Acrylic emulsion #6 and 20% FE-4300 FEVE Emulsion as total binder
39 38 Test Formulation: 80% Acrylic emulsion #6 and 20% FE-4500 FEVE Emulsion as total binder
40 39 Test Formulation: 80% Acrylic emulsion #6 and 20% FE-4500 FEVE Emulsion as total binder
41 40 Dark Green DTM I/M Paint Formulation Properties Solids (Volume) 32.7% FEVE Emulsions FE-4300, FE-4500, and FE4400 ph 9.0 to 9.5 TiO₂ Colorant (Evonik 896 line) Phthalo Green Colorant (896 line) Tint-Ayd CW5317 (Elementis) Pigment Choice PVC 8.7 Thickeners associative-type 60 Gloss Range VOC 150 g/liter
42 41 FEVE Water-borne Emulsions ************ FE-4400 Solids (Wt.) 50% ph 7 to 9 Specific Gravity 1.13 MFT 55 C. Hydroxyl Value 49
43 Testing procedure # 6 : 1) Choose Acrylic Emulsion # 5 as blending resin for Dark Green DTM I/M Formulations 2) Manufacture of 4 formulations: a. Binder = 100% Acrylic Emulsion b. Binder = 80% Acrylic Emulsion + 20% FE-4300 (FEVE Emulsion) c. Binder = 80% Acrylic Emulsion + 20% FE-4500 (FEVE Emulsion) d. Binder = 80% Acrylic Emulsion + 20% FE-4400 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 8 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 42
44 100.0 Gloss Decrease of Avanse MV-100 and 80/20 LUMIFLON Blends (Dark Green FORMULA) 60 Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic w/ 20% FE-4300 w/ 20% FE-4500 w/ 20% FE
45 44 Color Change of Avanse MV-100 and 80/20 LUMIFLON Blends (Dark Green FORMULA) 12 Color Change ΔE Hours in QUV Weatherometer 100% Acrylic w/ 20% FE-4300 w/ 20% FE-4500 w/ 20% FE-4400
46 Testing procedure # 7 : 1) Choose Acrylic Emulsion # 5 as blending resin for Safety Yellow DTM I/M Formulations 2) Manufacture of 3 formulations: a. Binder = 100% Acrylic Emulsion b. Binder = 80% Acrylic Emulsion + 20% FE-4300 (FEVE Emulsion) c. Binder = 60% Acrylic Emulsion + 40% FE-4300 (FEVE Emulsion) 3) Preparation of test panels ( primed Al panels coated with 8 wet mils of coating) 4) QUV Weatherometer Exposure (UVA 340 Bulbs used) a. Test Cycle = 8 hours UV 60 C. + 4 hours 50 C. 45
47 Gloss Decrease of Acrylic #5 and LUMIFLON Blends (Safety Yellow FORMULA) 60 Gloss Decrease (%) Hours in QUV Weatherometer 100% Acrylic w/ 20% FE-4300 w/ 40% FE-4300
48 47 18 Color Change of Acrylic #5 and LUMIFLON Blends (Safety Yellow FORMULA) Color Change ΔE Hours in QUV Weatherometer 100% Acrylic w/ 20% FE-4300 w/ 40% FE-4300
49 48 Conclusion: Inclusion of FEVE emulsions in architectural coating formulations can increase gloss retention, color retention, and the overall durability of the dry film. These characteristics will prolong the aesthetic properties and the protection properties of these coatings, thereby increasing the time frame between recoats.
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